, i .i \ j Vl."'. I L. LVV I U, L;}I'\IYI 10"'1O:!'1=-:c::::::-:::-_____LPST ID No.: ... Site Name: "'E"'xx"'o"'n"'RI,..S":""6-0"""27L,SL-_____Facility ID No.:,--<2"'6"'32""3'--______ Site Address: 4191 Beltline Road Addison (Dallas County), Texas This checklist must accompany all correspondence submitted to the RPR Section and should be affixed to the front ofyour submittal as a cover page. Please check the appropriate box for the type of correspondence which you have submitted to the RPR Section. Check all boxes that apply ifyou are submitting more than one type of correspondence. If you cannot find an appropriate category, please complete the "other" section. Initial Abatement Excavation (3) Waste Treatment (4) 0 Site Assessment (5) 0 Aquifer Testing (6) o LPST Case Questionnaireo 0 VES/Sparge Testing !7) 0 Qtrly. GW Monitoring (8) 0 􀁃􀁾􀁐􀁲􀁥􀁰􀀮􀀨􀀹􀀩􀀠0 GW Extrac,fTreatment (10) 0 Soil Vapor Extrac. (11) 0 Operation & Main. (12) 0 Site Closure (13) 0 Plan A Risk Ass, (14) 0 Plan B Risk Ass. (15) 0 Semi-annual GW Mon, (16)" 0 Annual GW Mon. (18) 0 Product Recovery (19) 0 Other proposal o Product Recovery Report Form (TNRCC-OOI6) • Release Report Form (TNRCC-0621) o Site Closure Request Form (TNRCC-0028) o Monitoring Event Summary and Status Report (TNRCC-0013) o Final Site Closure Report Form (TNRCC-0038 o Priority 4 LPST Case Closure Request Form (TNRCC-046I) o Other form o O&MlPerformance Mon. Plan B Risk Assessment 0 CAP InstallationIModification o Property DivestiturelPhase I ESA 0 Corrective Action Plan (CAP) 0 AquiferlPilot Test Results o Off-site access assistance o Deadline Extension Request o Tank tightness test results o Request for State-Lead o Request for LPST Waste Code o Class V Reinjection Request o Notice to Owner/Operator for CAS Services o Petroleum-Substance Waste Manifest o Notice ofContinuation of Groundwater Monitoring o Underground Storage Tank Registration Form o Notice of of Continuation of Operation and Maintenance 0 Aboveground Storage Tank Registration Form • Other (anything that does not fit into one of the categories above) 􀁦􀁵􀀡􀁕􀁾􀁾􀁬􀀺􀁬􀀡􀁬􀀡􀀱􀁬􀀱􀁾􀁑􀀡􀀱􀁩􀀲 􀀡􀀺􀁨􀀲􀁬􀁬􀁬􀁬􀁬􀁩􀀩􀁲􀁊􀀲􀁾􀀾􀀡􀀡􀁲􀁀􀁬􀀡􀁌􀀭􀀭􀀭􀀱􀀠* The proposal for semi-annual monitoring and annual report (proposal Activity 17) has been discontinued. For monitoring. use Proposal Activity 16. RELEASE DETERMlNAnON REPORT FORM Owners and operators must report releases by pbone to the appropriate TNRCC Region Office within 24 bours of confmnalion. The owner and operator sbould use this form to comply with the reporting requirements in Title 30, Texas Administrative Code D334.77(b). Submit the completed form within 20 days after release confirmation. EXCEPT IN EMERGENCIES, TIlE TNRCC WILL INITIATE ACTiON ON THIS CASE ONLY WHEN TIlE COMPLETED FORM IS S1.lBMrITED. Submit copies of this form with attachments to both the appropriate TNRCC Regional Office and to the Central Office in Austin. DO NOT MODIFY TIDS FORM IN ANY WAY. Complete all applicable blanks. Incomplete forms will be retumed without review. All proposals for the next appropriate corrective action activity must be submitted by a CAS and PM in the format outlined in the guidance document entitled PreapprovalJor Corrective Action Activities (RG-lll). SUMMARY Based on the information obtained during the release determination and by comparing the contaminant levels to the stated action levels, check one of these items as appropriate: o This was a suspected release. No contamination was detected. '" This site is an LPST site. Contaminant levels exceed action levels. o This site is Dot an LPST site. Contaminant levels do not exceed action levels. o This site is not an LPST site. No Contamination was detected (and none of the other criteria applies). IF THIS SITE IS AN LPST SITE, COMPLETE TIlE REMAINDER OFTHIS FORM (except Section B). If this site is not an LPS'!: site, stop here and complete Sections A, C and G (and Section B if applicable) of the attached form. o Check here ifthis site is an existing LPST case and this Release Detennination Report is being submitted only as the tank removal·fromservice documentation. Answer the following questions in this Summary Section if the CAS and PM sign the form in Section G. Tbis section is to be completed by a CAS and PM only. Ifthe form is completed by someone nther than a CAS and PM, leave the rest of this Summary Section blank and go to Section A. Is this case eligible for reimbursement of necessary corrective actions? 0 YES I NO If 􀁮􀁯􀁾􀀠appropriate corrective action in accordance with applicable rules and guidance ntay continue without specific direction or approval from the PST Division. however. coordination with the PST Division is recommended. If the site is eligible for reimbursement, all corrective action 􀁡􀁣􀁴􀁩􀁶􀁩􀁴􀁩􀁥􀁳􀁾􀀠with the exception of NAPL recovery and emergency abatement activities, must be preapproved prior to initiation. The next appropriate step fur this site, if it is an LPST site. is (check one only): o Case cIQSUI'C If checked, attach Site Closure Request Fonn (TNRCC-0028). Please be sure the site meets all requirements for closure prior to submitting the Site Closure Request Fonn. Are there costs associated with case closure? 0 YES 0 NO If YES, and ifthe site is eligible for 􀁲􀁥􀁩􀁭􀁢􀁵􀁲􀁳􀁥􀁭􀁥􀁮􀁾􀀠attach proposal with the Sit. Closure Request Fonn. o Risk-Based Assessment The risk-based assessment is needed only when the existing assessment data is not an adequate basis for site closure. Please critically evaluate the need for additional assessment before selecting this option. Refer to pamphlet RG·175 for guidance on conducting the risk·besed assessment. Attach a detailed workplan and proposal if the site is eligible for reimbursement. A proposal must be submitted with this form if the RP is financially able to undertake necessary corrective actions o Corrective action other tluln risk-based assessment Attach a detailed workplan and proposal ifthe site is eligible for reimbursement and the RP is financially able to undertake necessary corrective actions. Is the responsible party financially able to complete the next appropriate step? [1 YES 0 NO If Yes, attach proposal as specified above. If No, contact the PST Division at 5121239-2200 to request information on the State-Lead option. Financial ability determination forms must be I, completed and submitted to document that the RP is finanCially unable tocontinue necessary corrective actions. TNRCC·0621 (2-1·96) Page 1 of 15 A. GENERAL INFORMATION LPST ID No.: NA TNRCC Region: 04 Priority:(II mown) (see pages 12-14) Facility ID No.: 002632J o Required unless one of the following applies: 0 Check her iftank registration is not required for this site (per 30 TAC §334.7), and check one of the following as applicable: 0 the tank(s) are partially excluded Or exempted from jurisdiction under 30TAC Chapter 334. Speciry type Or usage oftank(s):_ 0 the tank( s) were pennanently removed from the ground before May 8, 1986 (provide date of removal ); 0 the tanks(s) remained in the ground but were emptied, cleaned and filled with inert substance before January 1, 1974 (provide date ofactivities ); 0 the tanks(s) were out of operation, their existence was unknown, and they were permanently removed from service within 60 days of their discovery (provide date of discovery : . Describe method of diseovery : ) Prior to this release incident, was this site an LPST site? v YES or 0 NO Ifyes, provide LPST ID number: 109104 Tank Owner: Exxon Mobil COT(lpration Tank Owner Mailing Address: P.O. Box 4552, Room # KT-1270 Tank Owner City: Houston State: Texas Zip: 772104552 Tank Owner Contact Person: Dale Gomm Phone: (7131656·9219 Fax no.: (7131656-9191 Tank Operator (If different from tank owner): Same as owner Tank Operator Mailing Address: Tank Operator Cltv: State:__ Zln: Tank Operator Contact Person: Phone: Fax no.: Land Owner (if different from tank owner and operator): Same as tank Q)!!ner , Land Owner Mailing Address: Land Owner City: State: Zip: Land Owner Contact Person: Phone: Fax no.: Ifthis site is all LPST site, which of these parties will oversee the corrective actions at this site? V Tank Owner 0 Tank Operator 0 Land Owner o Other (not the contractor or conSUltant): Name Address: City: State: Zip: Contact person: Phone: Fax: A representative of the party overseeing the corrective action must sign this form in Section G. Please note that no matter which party conducts corrective action, the tank owner and the tank operator are jointly responsible for the necessary corrective actions. , ! ! TNRCC·0621 (2-1-96) Page 2 of 15 I I : Facility Name: Exxon 6-0275 Facility Physical Address: 4121 Be/tline Road i Facility City: MrIisfIll County: Dallas County Code (see p. 15): 220 INDICATE TYPE OF RELEASE: (check one) D Suspected o Confirmed but below aClion levels (not an LPST site) ,; Confirmed and above action levels (LPST sile) o No evidence of contamination ! Please refer to flowchart and Title 30 Texas Administrative Code, 0334.71 -334.77 for descriptions and procedures fur suspecled and confinned reJeases. Were copies of this COMPLETED form (Excluding pages I through 5) AND APPROPRIATE ATTACHMENTS, including a proposal (ifRP is ! financially able), sent to both tile TNRCC Central Office and to tile Region Office? /YES o NO (IF COPIES ARE NOT SENT TO BOTH OFFICES, TIllS DOCUMENT WILL BE RETURNED WrrnOUT REVIEW). Indicate nurnberoftanks currently and formerly loealed at this sile (attach pages as necessary): 􀁔􀁾(UST/ASTI ProductTme Size 􀀨􀁡􀁾􀁒􀁲􀁯􀁾􀀮􀀠gal) Current: i , Date RemQved frQm Service Former: UST Unl,aded. regular ga,mline 10,000 10126&1 UST Unleaded fllus gasoline 10,000 lQ{l6lO1 illir. Unleaded SUl2.reme 􀁧􀁡􀁾􀁯􀁬􀁩􀁮􀁥􀀠10,00Q 10126101 􀀡􀁾􀁔􀀠Diesel 8000 lQ{l(i/Ol B. SUSPECTED RELEASE INFORMATION ! Complete only Ibis SOftion and seetions E through G as appropriate when the situation ofa suspected release has occurred and it was documented that a relea.. had not occurred, Date suspected release discovered: Reason release suspected: i Date suspected release reported to rnRCC: Reported to: Possible souree(s) of release: (check all that apply) Tanks: DUSTs 0 ASTs o Piping o Overfills/spills o Unknown o Other: i Type of substance(s) suspected released: (cheek all tIlalapply) o Gasoline o Diesel o Used Oil o Aviation Gasoline io Jet Fuel (type: ) o Alcohol-blended fuel (Type and percentage ofalcohol: ) o Other: (be :Were USTIAST system tank andlor line tightness tcsts pcrformed? 0 YES or 0 NO (check one) If yes, attach test data and results. Did tile tests indicate tIlal all tanks and piping were Ught? 0 YES or 0 NO (check one) IfNo, specify tile portion of tile tank syslem(s) tIl.1 were ! found not to be tiehl: i Were any repairs conducted on the tank system(s)? 0 YES or 0 NO (check one) Ifyes, describe type(s) and location of repairs: ! Were tightness tests perfonned after repairs were conducted? 0 YES or 0 NO (check one) If yes, attach test data and results. :Did the tests indicate thal tile repaired items were tight? 0 YES or 0 NO If No, specify the portion of the tank syslem(s) tIlat were found not to be tight: Were any soil confinnation samples collected? G YES or 0 NO (check one) If yes, were all potential source areas investigaled? i o YES or 0 NO If samples were collected, attach descriptions of sample locations, collection methods, and laboratory results. i Were any groundwater confU1Jllltion samples collected? 0 YES or 0 NO (check one) If yes, were all potential source areas investigated? DYES ! orONO If samples were coHected. attach descriptions of sample locatIons, collection methods, aquifer name, and laboratory results. (Groundwater sampling is not required at this point unless there is reasonable suspicion of impact.) : i C, CONFIRMED RELEASE INFORMATION I: TNRCC·0621 (2-1,96) Page30f15 Complete this section only if a release was confirmed. Date release confirmed: 11/23/01 Date release reported to TNRCC:,-'-N."'A'-______ Reported 􀁴􀁯􀁾􀀺________ Is this the first release from a UST or AST discovered at this site? 0 YES "NO Is there any other contamination or potential impacts to human health from any source other than the IJlnk systems at this site? DYES ,; NO Ifyes, indicate type and location of contamination:,_________________________ Reported to TNRCC by: 􀁾􀁎􀀮􀀬􀀭􀀬􀁁􀀬􀀭􀀬􀀭_______ Representing: 􀁟􀀭􀀢􀁎􀀮􀀧􀀭􀀧􀁁􀁾___________ Method of release discovery: o Samples collected during tank removal-from-service activities 0 Impact to utility line o Samples collected during other tank system construction activities 0 Impact to surface water o Samples collected during release determination investigation 0 Impact to water well 􀁾Other: Monitor well installation for a Divestment Assessment. Method of release confirmation: (check all that apply) " Soil samples ,; Groundwater samples 0 Surface water samples 0 DocumenMion of presence ofNAPL Source(s) of release: (check all that apply) Tanks: 0 USTs 0 ASTs 0 Piping 0 Overfills/spills ,; Unknown o Other' SubslJlnce(s) released: (check all that apply) " Gasoline o Diesel o Used Oil o Aviation Gasoline o Alcchol-blended fuel (Type and percentage oOcl:'ra'I':obol:________________________--.-J) o Jet Fuel (type:,_____________---1) 0 Other: (be specific),________________ Amount of product released: CASII:_______ (for hazardous substances) Were any soil confirmation samples collected? ,; YES or 0 NO (check one) Ifyes, attach descriptions of sample locations, collection methods and laboratory results. Type of native soil: (check one) ,; Clay or silt ,; Sand, gravel or rock Were any groundwater confirmation samples coIlected? ,; YES Or [] NO (check one) Ifyes, atlJ!ch descriptions of sample locations, collection methods, aquifer name, and laboratory results. Known Jmpact(s): (check all that apply) ,; Soil ,; GW 0 Surface Water 0 Subsurface Utilities -tvDe'JI":,____________ o Buildings 0 Water wells 0 Other sensitive receptors: ____________________________ Was the land owner (if different from the IJ!nk owner) notified of the contamination? 0 YES or 0 NO (check one) If Yes, attach copy of the letter which provided the notification, IfNo, documentation that notification was provided must be submitted within 30 days from the date the impact is discovered, NIA Possibly Threatened: (check all that apply) 0 GW 0 Surface Water 0 Subsurface Utilities -tvo'J""e:,_______________ o Buildings 0 Water wells 0 Other sensitivereceptors: ____________________________ Was NAPL detected (greater thaD 0.01 feet)? 0 YES or'; NO (check one) Ifyes, describe how and where it was detected, the thickness detected, and the recovery actions lJ!ken: __________________________________ TNRCC-0621 (2-1-96) Page 4 of 15 D. ABATEMENT MEASURES Were abatement measures initiated to stop the release or to recover the released substance? oYES or I NO (check one) If yes, describe the abatement andlor recovery measures taken and the dates and duration of the activities: Were UST/ASTsystem tank andlor line tightness tests performed? 0 YES or 0 NO (check one) Ifyes, attach test results. Did the tests indicate that all tanks and piping were tight? 0 YES or o NO IfNo, specify the portion of the tank system(s) that were found : not to be tight: Were any repairs conducted on the tank system(s)? :::J YES or 0 NO (check one) If yes, describe type(s) and location of repairs: Were tightness tests performed after repairs were conducted? 0 YES or 0 NO (check one) Ifyes, attach test results. Did the tests indicate that the repaired items were tight? 0 YES or 0 NO IfNo, specify the portion of the tank system(s) that were found not to be tight: N{-5 E. F1REIOTHER OFFICIALS Were any other officials notified? o YES 0 NO (check one) IfYes, indicate: Name Representing Phone number Daters) Notified ! Were any directives issued by the fire or other officials? 0 YES 0 NO If Yes, describe directives and actions taken in response to the -_. F. WASTE DISPOSITION Indicate the status of all wastes and other materials generated: Type of wlljlte (soil. water. product) Quantity Current location Method and location ofdisposal or treatment 5oi£eugs 1 uti swckiUtlonsile 􀁾􀁤qfat 'Wast RErn!!Im fRIlII: EXXON _ USA. I I I I I I , I > 􀁾􀀠iI!m!IIC!lJ !ROIl: 􀁾_ USA. 􀁾􀀠􀀭􀀭® EA ENGINEERING, SCIENCE. AND TECHNOLOGY _III 􀁾􀁉􀁉􀁉􀀠lAH 1lI.1E IP!IOJIl:T NO. 11-26-01 50802.75 P!IOJIl:T IiGR TF S('JL£ If"KlIIRE 1" 􀁾􀀠40' I 3 EXXON 4191 SITE MAP Il1.USTRATING6-0275 LOCATION Or MONITOR WELlS BELT LINE ROAD AND ELEVATIONS MEASURED ON NOVEMBER IS, 2001ADDISON, 1'£XAS I EA Engineering, Science, and Technology APPENDIXB SOn. ASSESSMENT Divestment Assessment I FIELD BOREHOLE LOG I1420 Valwood Plllkway. . BOREHOLE NO.: MW-I0Suib:l170 Carrollton. Texas 75006 I TOTAL DEPTH: 15' 972-484-1420 PROJECT INFORMATION DRILLING INFORMATION PROJECT: 6-0275 DRILLING CO.: Total Support Services SITE LOCATION: 4191 Belt Line DRILLER: Dan JOB NO.: 50802.75 RIG TYPE: CMC 45 ! LOGGED BY: Mark S. Lach METHOD OF DRILLlNG:CFA 1()...15 NO <50 127 132 I PROJECT MANAGER: Mark S. Lach DATES DRILLED: 11114/01 BOREHOLE DIAMETER: 8" NOTES: MW-IO cleared to 2.0' t w o SOIL DESCRIPTION 'w ...J a. :i! SAMPLING METHODS: Hand auger at clearing sz Water level during drilling Page 1 of2 '" Water level in completed well ><:0-:J:E BORING WELL0'[;;59 his, I-s, wa. a.Cl. COMPLETION DETAILS-Cl. 􀁡􀀮􀁾􀀠o I=r=I. CL gray, 0-2 6204.3 <50 170 <50 31 2"PVC 2.5' blank 12.5' screen 0.010" Slots 20/40 Sand -1 -2tH -2 1420 Valwood Parkway, Suite 170 FIELD BOREHOLE LOG I BOREHOLE NO.: MW-ll BARngina.aing, Science. Carrollton. Texas 75006 TOTAL DEPTH: 15' adTecbnology.lDc. 972-484-1420 I .. PROJECT INFORMATION DRILLING INFORMATION DRILLING CO.: Total Support Services! PROJECT: (i..0275 . SITE LOCATION' 4191 Belt Line DRILLER' Dan RIG TYPE: CMC 45 METHOD OF DRILLlNG:CFA ! SAMPLING METHODS: Hand auger at clearing BOREHOLE DIAMETER: 8" :sz Water level during drilling Page 1 of2 '"' Water level in completed well !w I ·'..ISOIL DESCRIPTION 'Q. BORING ! WELL ,,::lE COMPLETION, DETAILS I, « 0 I CO 􀁾􀁉􀀠AV: Dark "!own to oar!< gray,molsi:soft to firm ......... ! 6<50NO 2" PVC ND <50 31 2.5' blank 12.5' screen 0.010" Slots 20140 Sand -10-I 10-15 <50 12770.3I I -15-,-''--l.-j LS 132 -20-25JOB NO.: 50802.75 LOGGED BY: Mark S. Lach PROJECT MANAGER: Mark S. Lach DATES DRILLED: 11/14/01 'NOTES: MW-ll cleared to 2.0' i ! wet. HOUSTON LABORATORY 8a80 INTERCHANGE DRIVE HOUSTON, TEXAS 77054 (713) 660-0901 RECEIVED ExxonMobii NOV Z 9 2001 Certificate of Analysis Number: EA ENGINEERING01110599 Report To: EA Engineering Mark Lach 1420 Valwood Parkway Suite 170 Carrollton TX 75006ph: (972) 484-1420 fax: Project Name: 5080275 Site: 6-{)275,21 044479 Site Address: PO Number: LWRN21045007 State: Texas State Cert. No.: Date Reported: 11/21/01 This Report Contains A Total Of 14 Pages Excluding This Page And Chain Of Custody 11121/01 Date HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Case Narrative for: ExxonMobii Certificate of Analysis Number: 01110599 Report To; EA Engineering MarkLach 1420 Vatwood parkway suite 170 Carrollton TX 7S006Project Name: 5000275 Sile: 6--!l275,21044479 Site Address: PO Number: LWR#21Q45007 Texas Stale Cart. No.: L _____________ph, (972) 484-1420 fax: .___ _􀁟􀁌􀁟􀀭􀀽􀁄􀀽􀀮􀀽􀁬􀁥􀀽􀁒􀀽􀁥􀀽􀁰􀁯􀀽􀁲􀁴􀀽􀁥􀁤􀀽􀀺􀀽􀀭􀀮􀀮􀀮􀀮􀀮􀀺􀀮􀀮􀁬􀁬􀁾􀁉􀀲􀁾􀀮􀁉􀁾􀀯􀁏􀁾􀁬􀁾_________-.J Matrix spike (MS) and matrix spike duplicate (MSD) sample. are chosen and tested at random 'rom an analytical batch of 'like' mall1x to check for possible matrix effect. The MS and MSD Will provide site specific matrix data onty for those samples Which are spiked by the laboratory. Since the MS and MSD are chosen at random from an analylcal batch, the sample chosen for spike purposes mayor may not have been a sample submitted in this sample delivery group. The validity of the analytical procedures for Which data Is reported in this analytical report Is determined by the Laboratory Control Sample (LCS) and the Method Blank (MS). The Laboratory Control Sample (LCS) and the Method Blank (MB) are processed with the samples and the MSIMSD 10 ensure methOd crneria are achieved throughout the entire analylcat process. Any other exceptions associated with this report will be fOOfflOted In Ihe analylcal resull page(s) or the quality control summary page(s). Please do not hesitate to contact us if you have any questions or comments pertaining to this data report. Please reference the above Certificate of Analysis Number. This report shall not be reproduced except 10 full, without the written approval of the laboratory. The reported results are only representative of the samples submitted for testing. SPL. Inc. Is pleased to be of service to you. We anticipate working with you in fulfilling all your current and future analytical needs. 01110599 Page 1 11121/01􀁾􀁾􀁡􀁌􀀭􀁌􀀠Date Senior Project Manager HOUSTON LABORATORY 8880 INTERCHANGE ORIVE HOUSTON, TX nOM (713) 660-0901 ExxonMobiJ Certificate of Analysis Number: 01110599 􀁒􀁾􀁧􀁯􀁲􀁴􀁔􀁯􀀺􀀠EA Engineering Protect Name: 5080.275 Mark Lach 1420 Valwood Parkway Suite 170 Carronton Site: Site Address: 6-0275,21044479 TX PO Number: LWRII21045007 75006ph: (972) 484-1420 fax: (972) 247-7220 􀁾􀀠Slate C!!!l. No.: Texas Fax To: Date Regorted: 11121/01 k.: Client Sample ID MW·l00-2 I Lob Sample 10 I I 01110599-01 I Matri. Soil Date Collected 111910111:15:00 AM Date Received 11115101 10:00:00 AM COCIO HOLD 1J MW·l02-4 MW·l0 10-15 MW-l10-2 01110599-03 01110599-04 I I Soil sell Soil 11114/019:20;OOAM 11/14101 9:45:00 AM 1119/01 10:45:00 AM 11115101 10:00:00 AM 11115101 10:00:00 AM 11/1510110:00:00 AM 0 0 0 IMW'11 3·6 􀁾􀁗􀀮􀁬􀁬􀀱􀀰􀀭􀀱􀀵􀀠01110596-05 01110599·06 ................ I I Soil Soil , I 11/14/01 8:40:00 AM 111141018:55:00AM I 11/1510110:00:00 AM I 11/1510110:00:00AM 0 0 Sonia West Date Senior Project Manager Joel Grice Laboratory Director Ted Yen Quality Quality Assurance Officer 01110599 Page 2 11121/011:24:63 PM 11121/01 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 66()"OOOl Client Sample 10 MW-10 0-2 Collected: 1119/01 11:15:00 SPL Sample 10: 01110599-01 Site: 6-0275,21044479 Analyse.lMethod Result Rep,Umit 011, Factor QUAL Dale Analyzed Analyst Seq. # 􀁾􀁐􀁾􀁕􀁾􀁒􀁇􀁾􀁅􀁾􀁁􀁾􀁂􀁾􀁌􀁾􀁅􀁾􀁁􀁾􀁁􀁾􀁏􀁾􀁍􀁾􀁁􀁾􀁔􀁾􀁉􀁃􀁾􀁓􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀁾􀁾􀁾􀀽􀀽􀁾􀁾􀁾􀁾MCL SW8021B Units: ug/Kg Benzene .B.3 1 11/1610123:36 TM 913690 Elhylberzene 140 1 11/16101 23:36 TM 913690 Methyl tert-butyl ather 1.9 1 11/16101 23:36 TM 913690 Toluene ND 1 1111610123:36 TM 913690 Xyl enes,Total 56 1 11116101 23:36 TM 913690 SUIT: 1,4--Difluorobenzene 102 % 59-127 11/1610123:36 TM 913690 Surr: 4-Bromofiuorobenzene 297MI % 48-156 11/1610123:36 TM 913690 TPH TEXAS 100S 􀁾􀀱􀀲􀀠916336 >C12-C28 916336 >C28-C35 916336 Tola! TPH (C6-C35) 916336 Surr: 1-Chlorooctane 916336 :Preo Date TNRCC 1005 111151200113:16 􀁾􀁾􀁕􀀲􀀮􀁣􀀮􀀿􀁾􀀠SoniaWesl ----------------------Project Ma:,:na:190=r______________________________________ QuaJifJers: NDIU -Not Detected at the Reporting Limit >MCL -Resutt Over Maximum Contamination Llmll(MCL) B -An.lyle detected in !he associated Method Blank D -Surrogate Recovery Unreport8ble due to Dilution • -Surrogate Recovery OUtside Advisable QC Limits MI -Mallix Interierence J Estimated Value between MOL end POL 01110599 Page 3 11/21/011:25:11 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 000-0901 Client Sample ID MW-l0 2-4 CQllected: 11/14101 9:20:00 SPl Sample ID: 01110599-02 Site: 6-6275,21044479 AnalysesIMelhod Result Rep.Urnit Dil. Factor QUAL Date Analyzed Analyst Seq. # PURGEABlE AROMATICS Benzene 13 5 MCl SW8021B 5 Units: ugIKg 11/17101 0:04 TM 913691 Ethylbenzene 22 5 5 11117101 0:04 TM 913691 100 5 5 11117101 0:04 TM 913691 66 5 5 111171010:04 TM 913691 69 5 5 11/17101 0:04 TM 913691 135MI % 59-127 5 11117/01 0:04 TM 913691 109 % 48-156 5 11117101 0:04 TM 913691 TPH TEXAS 1005 Mel TNRCC1005 Units: mg/Kg C6-CI2 ND 50 I 11120101 1:40 AM 916337 >C12-C28 ND 50 1 11/201011:40 AM 916337 >C28-CS5 ND 50 1 11/201011:40 AM 916337 To1al TPH (C6-C35) ND 50 111201011:40 AM 916337 Surr. 1-Chlorooctane 104 % 70-130 11120101 1:40 AM 916337 Surr: 0-Terphenyl 101 % 70-130􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀻􀀻􀀺􀁾􀀭􀀻􀀻􀀻􀁩􀁟􀀺􀀻􀀻􀀻􀀭􀁾􀀻􀁟􀀭􀀭􀀭􀀭􀀭􀀭􀁟􀀻􀁟11120101 1:40 AM 916337 Prep Method ,.prep Date Prep Initials: TNRCC 1005 1111512001 13:16 􀁊􀀽􀁦􀁾􀁾􀁟􀂷􀀠Sonia West Proleot Manager Qualifiers: NDIU -Not Detected at the Reporting Limit >MCl -Result Over Maximum Contamination Llmlt(MCL) B -Analyte detected in the associated Method Blank D -Surrogate Recovary Unreportable due to Dilution • -Sunroga1e Racovery Outside Advisabla QC Limits MI -Matrix Interference J -EsUmated Value be1ween MDl and POL 01110699 Page 4 11121101 1:25:14 PM HOUSTON LABORATORY OOSO INTERCHANGE DRIVE HOUSTON, TX 77054 (l13) 000-0901 Client Sample ID MW-10 10·15 Collected: 11/14101 9:45:00 SPL Sample 10: 01110599·03 Site: 6-0275,21044479 AnalysesIMelhod ResuEt Rep.Limit Oil. Factor QUAL Date Analyzed Analyst Seq. # Units: 􀁵􀁧􀁬􀁬􀀨􀁾􀀠Benzene 11117/010:32 TM 913692 PURGEABLE AROMATICs ___--;:o;:;-___􀀭􀀺􀀻􀀭􀁟􀀭􀀽􀀽􀁾􀁟􀀮􀀺􀀺􀀺􀁓􀀻􀀮􀀺􀁗􀀢􀀧􀀸􀀢􀀧� �􀀲􀀢􀀢􀀱􀀢􀀧􀁂􀀧􀀭􀁟􀀻􀀢􀀻􀀧􀀻􀀺􀀻􀀻􀀻􀀷􀀬􀀧􀀻􀀷􀀻􀀧􀀺􀁾...: Ethylbenzene 11/17/010:32 TM 913692 Methyl tert-bulylether .. ______-',=-_ 11117101 0:32 TM 913692 Toluene 11117/01 0:32 TM 913692 Xylenes,Total 11117/010:32 TM 913692 11117/01 0:32 TM 913692Surr.l,4-DiHuorobenzenc:e______􀁾􀀬􀀻􀀻􀀺􀀮􀀮􀀻􀁾􀁟􀀺􀀺􀁟􀁟􀀧􀀻􀀺􀀺􀁟􀀺􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀀭􀀭􀀭􀁟􀀺􀁣􀁾􀁾􀁟􀀷􀁟􀀺􀀷􀁟􀁟 􀀽􀀭􀀺􀀺􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀺􀀺􀀭􀀽􀀽􀀠SUIT: 4-Bromofluorobenzene 11/17/010:32 TM 913692 Unit!;: mgIKg TPH TEXAS 1005 .. __􀁾􀁾􀁾􀁟􀀭􀀻􀀭􀀻􀀻􀀻􀁾􀁾􀁟􀀭􀀺􀀺􀀺􀀺􀀺􀁟􀁾􀀽􀀧􀀺􀀮􀀮􀀮􀀮􀀭􀀭􀀬􀁔􀀢􀁎􀀢􀁒􀀻􀀭􀀮􀁃� �􀀢􀀢􀀭􀀬􀀭􀀱􀀰􀀢􀀬􀀰􀀬􀀬􀀬􀀵􀀬􀁟􀀭􀀽􀀽􀁾􀀠􀁾􀀲􀀠1 11120101 I:SO AM 916338 􀀾􀁃􀁬􀁾􀁃􀀲􀁾􀀸􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀀭􀀭􀀭􀀭􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁉􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀁾􀁾􀁾􀁾􀀭􀀭􀀭 􀀭􀁾􀁾􀁾11/201011:80 AM 916339 >C28-C38 1 11/201011:80 AM 916338 Total TPH (C6-C38) 1 111201011:50 AM 916338 Surr. I·Chlorooctane 11120101 1 :50 AM 916338 Surr. o-Terphenyl 11/20101 1 :50 AM 916938 prep Method prep Date TNR<;C 1005 11/151200113:16 􀁾􀁾LL.//dZ=;;; SOnia West ------------------------------------Project Ma=n:;:."'9:.:er:......_______________________________________ ___ Qualifiers: NDIU -Not Detected at the Reporting Umit >MCL· Resull Over Maximum Contamination Umit(MCL) B • Analyte aetactea in the associated Method Blank o . Surrogate Recovery Unraportable due to Dilution •• Surrogata Recovery OUtside Advisable OC Limits MI-Matrix Interference J . EsUmated Value between MOL and POL 01110599 Page 5 11121/01 1:25:16 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON. TX 77054 (713) 660-0901 Client Sample ID MW-11 0-2 Collected: 11/9101 10:45:00 SPl Sample ID: 01110599-04 Site: 6-ll275,21 044479 AnalysesIMethod Result Rep.Llmlt Oil. Factor QUAL Date Analyzed Analyst Seq. II PURGEABlE AROMATICS MCl SW8021.EL Units: IIg1Kg Benzene NO 1 1 11/171011:00 TM 913693 Ethylbenzene NO 11117/01 1:00 TM 913693 Methyl tert·butyI ether NO 1 11/17/01 1:00 TM 913693 Toluene NO 1 11/17/011:00 TM 913693 Xylene.,Total ND 1 111171011:00 TM 913693 􀀭􀀭􀁳􀁷􀁲􀀮􀂷􀁾􀁬􀁾􀀮􀁾􀀽􀁏􀁾􀁩􀁦􀁾􀁬􀁵􀁯􀀭􀀭􀁲􀁯􀁾􀁢􀀭􀁥􀁮� �􀁺􀀭􀁥􀀭􀁮􀁥􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀷􀀭􀁾􀁾􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀀽􀀽􀁾􀁾􀁾􀁾􀀭􀀭􀀭􀀭􀁾􀁾􀁾90.1 % 59·127 1 11/17/011:00 TM 913693 SUIT: 4--Bromofluorobenzene 94.3 % 48·156 1 11/17101 1:00 TM 913693 TPH TEXAS 1005 MCl TNRCC1005 Units: mglKg C6-C12 ND SO 11I20I01 2:01 AM 916339 >CI2·C28 NO SO 11120101 2:01 AM 916339 >C28·C35 ND SO 11/20101 2:01 AM 916339 Total TPH (G8-C35) NO 50 1 11/20101 2:01 AM 916339 Surr: l·Chlorooctane 106 % 70·130 1 11/20101 2:01 AM 916339 916339Surr: 0-Terphenyl 104 % 70·130 1 11120101 2:01 AM Prep Method Pmp Date Prep Initials 􀁾􀁔􀁾􀁎􀁾􀁒􀁾􀁃􀁃􀁾􀀮􀀱􀀺􀁾􀁾__􀁾􀁾􀀱􀀱􀁾􀀯􀁬􀁾􀁓􀁉􀀲􀁾􀀰􀀰􀀱􀁾􀀱􀀳􀁾􀀺􀀱􀁾􀀶____ J_F 􀁾􀁾U2 <;;?<=.:;;;: Sonia West Project Menage, Qualifiers: ND/u -Not Detected at the Reporting Limit B • An.lyle detected in the associated Method Blank , • Surrogate Recovery Outside Advisable QG limits J . Estimated Value between MDL and POL 01110599 Page 6 >MCl -Result OVer Maximum Contamination Limit(MCL) o -Surrogate Recovery Unreportable due to Dilution MI -Matrix Interference t1/211011:25:18 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 􀁾􀁾􀀷􀀠(713) 880-0901 Client Sample 10 MW-l1 3·6 Collected: 11/14101 8:40:00 SPl Sample 10: 01110599·05 Site: 6-0275,21044479 AnalysesIMethod Result Rep.Limit DII. Faclor QUAL Date Analyzed Analyst Seq. It PURGEABLE AROMATICS MCl SWB021B 􀁕􀁮􀁩􀁬􀁾􀀺􀀠ug/KS Benzene NO 1 11117/011:28 TM 913694 Elhylbenzene. NO 1 111171ll11:28 TM 913694 Methyl tert-bulyl ether NO 1 111171011:28 TM 913694 Toruene NO 11117101 1:28 TM 913694 Xylenes,TotaI NO 11/171011:28 TM 913694 Surr: 1.4-Difluorobenzene 93,0 % 59·127 1 11/171011:28 TM 913694 Surr: 􀀴􀁾􀀸􀁲􀁯􀁭􀁯􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠98.8 % 48·156 1 11/17/011:28 TM 913694 TPH TEXAS 1005 MCl TNRCCJ005 Ullits: mg/Kg C6-C12 NO 50 11120101 2:11 AM 916340 >C12-C28 NO 50 1 11120101 2:11 AM 916340 >C28-C36 NO 50 1 l1f20101 2:11 AM 916340 Total TPH (C6-C36) NO 50 1 11/20101 2:11 AM 916340 SUff: l·Chlorooctane 107 % 70-130 1 111201012:11 AM 916340 SUIT: 0-Terphenyi 102 % 70·130 1 11120101 2:11 AM 916340 􀁾􀁾􀁟£..<:/& d:::L::::::= Sonia West -------------------------Project Manager Qualifiers: NDIU • Not Detected althe Reporting Limit >MCL -Result OVer Maximum Contamination Llmit(MCL) B • Analyle detected in the associated Method Blank o-Surrogate Recovery Unreporlable due to DilUtion •• Surrogate Recovery Outside Advisable OC Limits MI -Matrix Interference J. Estimated Value between MOL and POL 01110599 Page 7 11/211011:25:21 PM HOUSTON LABORATORY SS80 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample ID MW-11 10-15 Collected: 11/14/01 8:55:00 SPl Sample ID: 01110599-06 Site: 6-6275,21044479 AnalysesIMelllod Resull Rep.Llmit Oil. Factor QUAL Dete Analyzed Analyst Seq. # MCl SW8021B Units: uglKg Benzene 15 1111610122:13 TM 913687 􀁐􀁕􀁒􀁇􀁅􀁁􀁂􀁌􀁅􀁁􀁒􀁏􀁍􀁁􀁔􀁉􀁃􀁾􀁓􀁾______􀁾______􀁾____===-__􀁾􀁾􀁾􀁾􀁾 􀁾􀁾􀁾􀁾􀁾____􀁾􀁾􀁾􀀠Ethylbenzene 22 1 1111610122:13 TM 913687 Methyltert-butyl . ..:eth=er'-____ Toluene 52 11 1 1 11/1610122:13 1111610122:13 TM TM 913687 913SS7 Xyienes.Tolal 22.3 1 1111610122:13 TM 913687 Surr: 1.4>-Difluorobenzene 127.09MI % 59-127 • 1111610122:13 TM 913687 Surr: 􀀴􀁾􀁡􀁲􀁯􀁭􀁯􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠138 % 48-156 1111610122:13 TM 913687 TPH TEXAS 1005 C6-C12 ND 50 MCl TNRCC 1005 Units: mgIKg 111201012:22 AM 916341 >C12-C28 ND 50 11120101 2:22 AM 916341 >C28-C35 ND 50 11120101 2:22 AM 916341 Tola! TPH (CS-C35) ND 50 11/20101 2:22 AM 916341 Surr: 1-Chlorooctane 106 % 70-130 11/20/01 2:22 AM 916341 Surr: 0-Terpllenyl 103 % 70-130 11120/01 2:22 AM 916341 :Prep Method Prep Date :Prep Initialsi TNRCC 1005 1111512001 13:16 J F b􀁾􀁾U ?<=;;;: Sonia West -----------------------Projeel Manager Qualifiers: ND/U -Not Detected at the Reporting Limit >MCL -Result OVer Maximum Contamination Umlt(MCL) B -Analyle detected in the associated Method Blank D -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery outside Advisable QC Umlls MI -Matrix Interference J -Estimated Value between MDL and PQL 01110599 Page 8 11121/01 1:25:24 PM Quality Control Documentation 01110599 Page 9 11/21101 1:25:25 PM HOUSTON lABORATORY aaao INTERCHANGE DRIVE HOUSTON, TX n054 Quality Control Report (713) 660-0901 ExxonMobil 5080275 Analysis: TPH Texa. 1005 WorkOrder: 01110599 Method: TNRCC 1005 Lab BatCh 10: 16237 Method Blank Samples In Analytical Batch: RunlD: HP_B.011120A-916330 Units: mg/Kg Lab Samili. 10 􀁃􀁉􀁩􀁾􀁮􀁬􀀠Samille 10 Analysis Date: 1112012001 0:37 Analyst: AM 01110599-01A MW-l0 0-2 Preparation Date: 111151200113:16 Prep By: J_F Method TNRCC 1005 01110599-02A MW-l02-4 01110599-03A MW-l0 10-15 01110599-Q4A MW-ll0-2 01110599.Q5A MW-l1 3-6 01110599-00A MW-l110-15 Analyte C6-C12 I (C6-C351 Surr. ,. , Suit 10 Result 'Rap Llmll NI 70-130 , 102: 70-130 Laboratory Control sample (LeS) RunlD: HP _B_011120A-916331 Units: mglKg Analysis Date: 1112012001 0:48 Analyst: AM Preparation Date: 11115/200113:16 Prep By; J_F Method TNRCC 1005 Analyte Spike Result Percent Lower Upper Added RecoII&ry Uml! Umit >C12-G28 500 550 110 70 130 C6-C12 500 480 97 70 130 ITotal TPH (C6-C3S) I 1000 1030 1031 70 130 􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁍􀀻􀀺􀀺􀁡􀀺􀀺􀁴􀁲􀀢􀁩􀁸􀀺􀁣􀁓􀀻􀀻􀀺􀀺􀁰􀀺􀀭􀀺􀀭􀁬􀁫􀀢􀀮􀀺􀀭􀁦􀀻􀀻􀀮􀁦􀁩􀁉􀀻􀀻􀀮􀁓􀁾􀁬􀀭􀀻􀁉􀀭􀀻􀀻􀀻􀁍� �􀀺􀀺􀁡􀁴􀀻􀀺􀀭􀁲􀀻􀀺􀀭􀁬􀁸􀀺􀁣􀁓􀀻􀀻􀀺􀀺􀁰􀀺􀀭􀀺􀀭􀁩􀁫􀁥􀀽􀁏􀀻􀁃􀁵􀀭􀀮􀁰􀁉􀁬􀁣􀁭􀀭􀁥􀀭􀁦􀁍􀀭􀁓􀀭􀁐􀀩􀀧􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭Sample Spiked: 01110596-01 RunlD: HP_B_011120A..g16334 Units: mgIKg Analysis Date: 11/2012001 1:00 Analyst: AM Preparation Date: 111151200113:16 Prep By; J_F Method TNRCC 1005 Analyte Semple MS , Result SpikeI Added 120 500􀁾􀀲􀀸􀀠MS Rasult MS% Recovery 680 112 MSD% ' RPD MSD MSD Result RPD Low iHigh' Spike Limit UmilRecovelY Limit Added 500 700 3,95 20117 70 C6-C12 Total TPH (C6-C35) 100, 500 220: 1000, 580 96.2 500 590 1260 104 1000 1290 96.9 0.769 107 2.841 20 70 130 20 70 130 aualifiers: NDIU -Not Datacted at the Reporting Limit MI -Matrix Inleltarsnce B -Analy!e detected In 1I1e associated Melhod Blank D -RecoII&ry Unraportable due to Dilution J -Estimated value between MDL and POL • -Recovery OutSide Advisable QC Limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01110599 Page 10 rounding, the reported RPD may differ from the displayed RPD values but is correci as reported. 11tz1l011:27::16PM 130 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054􀂣􀁲􀁾􀀷􀀠(713) 660·0901Quality Control Report ExxonMobil 5080275 Analysis: Purgeable Aromatics WorkO,der: 01110599 Method: SWB021B Lab Batch 10: R47940 Method Blank Samples in Analytical Batch: RunlD: HP_fl-Ol1116B·913686 Units: uglKg Lab sam!!l. 10 Client Sam!;!le 10 Analysis Date: 111161200121:45 Analyst TM 01110599·01 A MW·l0 0-2 01110599·02A MW·l0 2·4 01110599-D3A MW·l0 10-15 01110599-04A MW·ll 0-2 Analyle Result Rep Limit 01110599-05A MW·ll 3-61,0:Benzene I ND , 0111 059{)'05A MW·l110·151.01NO􀀧􀁅 􀁴􀁨􀁹􀁬􀁢􀁥􀁮􀁺􀁾􀁡􀁥􀀠1.0,NO:Melhvt tert-buM etMr ND 1.0:Toluene 􀁭􀀮􀁄􀁾􀁘􀁙􀀡􀁥􀁮􀁥􀀠NO 1.0 1.0: Total aTEX NO􀁾􀀩􀀨􀁹􀁬􀁥􀁮􀁡􀀠1.0NO ,1M2nes.Total NO 1.0 ..... Sun: 1 4-DlfJuorobenzene 1IT.7 70·130 Surr: 4wBromofIUOrobenzenf) 923 70-130 Laboratory Control Sample (LCS) RunlD: HP..A.Dl1116B-913M2 Units: uglKg Analysis Dale: 111161200118:59 Aralyst: TM Analyle Spike Percent Lower UpperResull Added Recovery Limit limit :Benzene 50 70 12453 106 Ethylbenzene 50 52 104 78 128 Methyl tslt·butyl ether 13050 53 107 70 Toluene 50 105 70 12853 m,p·Xylene 100 100 103 71 130 71krXyfane 105 12950 53 71IXylenas, Total 15C 153 102 130 .. Matrix Spike (MS: 1 Matrix Spike Duplicate (MSDl Sample Spiked: 01110599·03 RunlD: HP_R_011116B-914287 Units: uglKg Analysis Date: 111171200116:48 Analyst TM ! Aralyle I Sample MS ! MS Resull I MS % MSO ! MSO Resull! MSD % RPD Result Spike Recovery Spike I I 'RecoveryAdded , ! Added RPD Limit Low High Limit Limit Qualifiers: NDiU • Not Detected at !he Reporting Limit MI • MalJix Interference B • Analyle detected in the associated Method Blank o • Recovery Unreportable due to Dilution J • Estimated value _aen MOL and POL •• Recovery Outside Advisable QC Limits The percent recovelies for QC samples are correct as reported. Due 10 significant figures and 01110599 Page 11 rounding, Ihe reported RPD may differ from the displayed RPD values but is correct as reported. 111211011:27:50 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON. TX 77054 Quality Control Report (713) 66Q-090l 􀁾􀁊􀁬􀁬􀀡􀀡􀁊􀁃􀀷􀀠ExxonMobil 8080275 Analysis: Purgeable Aromatics WorkOrder: 01110599 Method: SW8021B Lab Batch ID: R47940 Matrix Spike (MS) I Matrix Spike Duplicate IMSDI Sample Spiked: 01110599-03 AunID; HP_R...0111169·914287 Units; ugIKg Analysis Date: 111171200116;48 Analyst: TM , Benzene Ethylbe1llene Analyte Sample MS MS Result I MS% MSD II MSD Result MSO% Result Spike Spike Recovery Added : Recovery Added i NO: 20 20 97.3 20 19 94.2 NO 20 17 82.9 20 16, 78.8 Methyl tart·butyl e.ther 4.8 20 23 92.5 20 23 89.2 ,To!uene 􀁾􀀠'm,p-Xylene ",Xylene Xylenes,T oIal NO 20. NO 40 NO, 201 ..--... NO 601 .....􀁾􀀮􀀭22 104 20 19 34, 85.7 40 33 17' 79.4 20 16, 51 i 85.0 80 491 93.4 82.7 78.3 81.7 RPO RPO Umit , 􀁾􀀠34 5.03 35, 3.66 22! 11.2 28 3.52 381 1.47 571 4.00 381 Low High 􀁕􀁭􀁾􀀠Umit 35 139 31 137 27 196 31: 137 19 144 251 139 19 144 Qualifiers: NDIU • Nol Detected at the Reporting limit MI • Matrix Interference B • Anatyie detected in the associated Method Blank D • Recovery Unreportable due 10 Dilution J . Estimated value between MOL and POL •. Recovery Outside Advisable QC Limits The percent recoveries tor QC samples are correct as reported. Due to significant fjgures and 01110899 Page 12 rounding, the reported RPD may diHer from the displayed RPD values but Is correct as reported. 11/21/011;27:51 PM Sample Receipt Checklist And Chain of Custody 01110599 Page 13 11121101 1:2:7:52 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Sample Receipt Checklist Workorder. 01110599 Received By: DS Date and Time Recefved: 11115101 10;00;00 AM Carrier name: FedEx Temperature: 3 Chilled by: Water Ice 1. Shipping container/cooler in good condition? Yes 􀁾􀀠No Not Present 0 2. Custody se.ls intact on shlppping container/cooler? Yes 0 NoD Nat Present 􀁾􀀠3. Custody seals intact on sample bottles? Yes 0 No Not Present 􀁾􀀠4. Chain of custody present? Yes 􀁾􀀠No 5. Chain of custody signed when relinquished and received? Yes 􀁾􀀠NoD 6. Chain of custody agrees with sample labels? Yes 􀁾􀀠NoD 7. Samples in proper container/boffie? Yes 􀁾􀀠NoD 8. Sample containers intact? Yes 􀁾􀀠NoD 9. Sufficient sample volume for indicated test? Yes 􀁾􀀠NoD 10. All .amples received within holding time? Yes 􀁾􀀠NoD 11. ContajnerlTemp Stank temperature in compJiance? Yes 􀁾􀀠NoD 12. Water· VOA viais have zero head.pace? Ye. 0 NoD Nat Applicable 􀁾􀀠13. Water -pH acceptable upon receipt? Yes No[] No[] Not Applicable 􀁾􀀠________________􀁾SPL Representative: Contact Date & TIme:1L-Client Name contacted:"1 ============i Non 􀁣􀁯􀁮􀁦􀁯􀁾􀀺􀁾􀀺􀀺􀀺􀀠Ciient 'not, 􀀧􀁾􀁴􀁬􀁮􀁮•• :====================================i 01110599 Page 14 11/21/01 1:27:53 PM '" UII I U5.GfCJ EXXON COMPANY, USA. ISouthweot&WBshlngtonl!-''','' Exxon 􀁅􀁾􀁨􀁥􀁥􀁲􀀺􀀠,0'hJ [:0: 1M Phone: 7(t 􀁲􀁏􀀺􀁾􀁾􀁥􀀷􀀿J9 Consultan! Co. Name ;;:; /;; IV 􀁾􀁾􀀠Contact , "Address: l(..\ 􀁾Ur:: ! 􀁍􀁣􀀩􀀢􀁾􀀠Fax: 1M.. S L I'Ji? & ItE S:riP" ",..oN OF CUSTODY RECORD NO. Page -Lof -f-ANALYSIS REQUEST: OTHER(CHECK APPROPRIATE BOX) m" " 0 i 0 0 . 􀁾􀀠::l 0 >􀁾􀀠􀁾􀀠0liS 􀁾􀀠􀁾􀀠0 􀁾0 0 z o 􀁴􀁾􀀠􀁾􀀠0 􀁾􀀠􀁾􀀠g 0 i50 􀁾􀀠􀁾􀀠􀁾􀀠'" m f? 'I I? o § 􀁾􀀠g " 0 a: x 􀁾􀀠0 􀁾􀀠.,; 􀁾􀀠g!iJ 􀁾􀀠r fi ;1; N 0 I 􀁾􀀠0 0" ;5􀁉􀁾􀀢􀀠􀁾􀀠" 0 0 N I 􀁾􀀠&i w ;:! 􀁾􀀠lIJ § 􀁾􀀠I '"0 0 0 0"' i M 0 􀁾􀀠􀁾􀀠0 0 " z lSI 􀁾􀀠r '" 0 " i x w 􀁾􀀠(I) 􀁾􀀠􀁾􀀠􀁾􀀠" 8 Ii! 􀁾􀀠􀁾􀀠􀁾􀁾􀀠􀁾􀀠ill f 􀁾􀀠0 -II 0 ;; I? 􀁾􀀠0 0 0 􀁾􀀠., "z 􀁾􀀠r 􀁾􀀠􀁾􀀠I '"' I 'l' .,., 5' i iiiu.. 􀁾􀀠􀁾􀀠􀁾􀀠" w 0 " o 􀁾􀀠􀁾􀀠.J 􀁾􀀠Ie ;5 g 􀁾􀀠d a: :t: l? 0 " 􀁾􀀠if iI!: " w􀁺􀁡􀀬􀀬􀀬􀁾􀁉􀀡􀀺􀀺􀀺􀁬􀀠> ., .. 􀁾􀀠" w RAS 􀀣􀀺􀁾􀁯"d-'1 C; Facility/Slate 10 # (TN Only): ---::-=:-r,----:::-=-:--::;-o-_---,-.-,.-___ConsuU nl rojecl#::.sr>S3 0),7S-Loca . . 􀁾(, N (Cily) (State) '/)( E DC;'''' 􀁏􀁾􀀠􀁾􀀺􀀻􀁾􀀠􀁾􀀻􀁯􀁾􀀠􀁒􀀮􀁜􀀺􀀧􀀻􀀻􀁾􀀬􀀭r l 􀁾􀀠􀁾􀁾􀀨􀁴􀀬􀀠,1.0. I DATE ITIME 1<::6MRIGRAB I r¥sTRI¥. I"'" ",,0 SOIL AIR '1.j '1-rr;?1'0􀁺􀀭􀀺􀁪􀁲􀁾􀁾􀁦􀀠IJIItil IifI \ I'n ff lIT 111111111111111 􀁉􀁐􀁷􀁲􀁾􀁾􀀵􀂣􀀠􀁉􀁾􀁦􀁦􀀠111 W1IIl1111IJt 􀁉􀁪􀁬􀁬􀁬􀁬􀁬􀀡􀁾􀁾􀁩􀁦􀁬􀁬􀁩􀁬􀁬􀀠.i TAT 24 HR. 48 HR. 72HR. 􀁾􀀮􀀧􀀠96HR. r. Rg;'; I [) t,:Jj(rrTbt5 rb·T'[ I " ,/EXXON UST I {' 0 (,6 SPECIAL DETECTION LIMITS (Specily) 8 Business 􀁾􀁃􀁯􀁮􀁴􀁡􀁤􀀠US Prfor to SMdlr'Ig Sample CONTRACT NO, I-S:::PE=C:-:-IAL:-:::RE:::P:::O:::R=TI::-:N:::G-=R=EQ:::UC;:I:::RE::M:::E"'N"'TS;:-;::(S'-pe-cily:7.7")----t""'LA"B;:-;;cUS"'E::O" "N"L;;Y LOt # . ...... Slo"'ll" Location Other C41483 􀁾􀀠2.,VPDF 0 0 EDD )h) u QAlQC L.,..t I OV-􀁩􀀻􀀬􀀢􀀧􀁾Standard 0 CLP 0 Olh., 0 n FAX 0 0 FAX c-o.c WIREPORT WORK ORDER #: ()J tV;:::;,r11 LAB WORK RELEASE #: Relinquished: Date Time I I I -":::y Triplicate: Original' WhHe lab's Copy' Green Client Copy. Yellow • I EA Engineering, Science, and Technology APPENDIXC GROUNDWATER ASSESSMENT Divestment Assessment HOUSTON lABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660·0901 ExxonMobii '-;-:--;--;-;-:--:-----Certificate of Analysis Number: 01110658 Report TO': EA Engineering Mark Lach 1420 Valwood Parkway Suite 170 Carrollton TX 7!iIl06· ph (972) 484-1420 ''''': Proiect Name: 5080275 Sito: 6-0275,21044479 Site Address: PO Number; LWR#21045043 State: Texas State Cert. Ne.: Date Reported: 1217/01 This Report Contains A Total Of 14 Pages Excluding This Page 12110101 Date I HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON. TX 77054 (713) 660-0901 Case Narrative for: ExxonMobii -...--.--􀀭􀀭􀀭􀀭􀀭􀀭􀀺􀀺􀀭􀀭􀀽􀀭􀀭􀀺􀀭􀀭􀀽􀁾􀀭􀀭􀀺􀀭􀀭􀀺􀀺􀀭􀀭􀀭􀀻􀀭----------Certificate of Analysis Number: 01110658 Report To: EA Engineering Mark Lach 142.0 Valwood Parkway Suite 170 Carrollton TX 75006ph: (972)484-1420 fax: Project Name: 5080275 Site: 6-0275.21044479 Site Address: PO Number: lWR#21045043 􀁾􀀠Texas State Celt. No.: Date Reported: 1217101 Matrix spike (MS) and matrix spike duplicate (MSD) samples are chosen and tested at random from an analytical batch of "liken matrix to check ror possible matrix effect. The MS and MSD will provide site spedfic matrix data only for those samples which are spiked by the laboratory. Since the MS and MSD are chosen at random from an analytical batch. the sample chosen for spike purposes mayor may not have been a sample submitted in this sample delivery group_ The validity of the analytical proceCI2-C28 >C28..cas Total TPH (C6-C35)SUIT: 􀁬􀀭􀁃􀁨􀀷􀀱􀀰􀁲􀀰􀀰􀁣􀀭􀁾􀁉􀁡􀀭􀁮􀁥􀀭􀀭SUIT: 0-Terphenyl NO NO ND ND 113 109 % % 5 5 5 5 70-130 70-130 MCl TNRCC 1005 1 1 1 1 Units: mgll 11119101 21:08 AM 11119/01 21:08 AM 11/19/01 21:08 AM 11119/0121:08 AM 11119101 21:08 AM 11119101 21:08 AM 916361 916361 916361 916381 916381 916381 : Prep Method Prep Date Prep Initials ,TNRCC 1005 111161200115:10 J F 􀁾􀁾􀀻􀁣􀀺􀀻􀀧􀁲􀀮􀀻􀀺􀁾􀁾􀀭􀀭􀁾􀁌􀀯􀁾􀀭􀁤􀀧􀀭􀁚􀀽.Sonia West Qualifiers: NDJU -Not Detected at the Reporting limit >MCL -Result Over Maximum Contamination Umit(MCL) B -Analyte detected in the associated Method Blank D -Surrogate Recovery Unreportable due to Dilution ., -Surrogate Recovery Outslde Advisable QC Limits MI -Matrix Interference J. El!fimated Value between MOL and pQl 01110658 Page 3 12110;01 11;54:18 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, 'IX 77054 (713) 660.0901 Client Sample 10 MW-4 Collected: 11115101 12:20:0 SPL Sample 10: 01110658-02 Site: 6-0275,21044479 AnalyseS/Method Result Rep. Limit DiI, Factor QUAL Date Analyzed Analyst seq. # PURGEABLE AROMATICS MCL SW8021B Units: ug/L Benzene ND 1 11120101 5:04 DL 917720 Ethylbenzen. ND 11120101 5:04 DL 917720 Toluene NO 11120/01 5:04 DL 917720 11120/01 5:04 DL 917120Methyl tert-butyl .th....r_______-:17..2:;.--___-:_______...;...____􀀻􀀮􀀻􀀺􀀻􀀺􀁾􀁾􀁾􀀻􀁟􀀻􀀺􀀮􀀻􀀺􀀭􀀭􀀭􀁾􀀽􀀻􀀠Xylen••,Total ND 11120101 5:04 DL 917120 Surr: 4-Brornoftuorobenzene 93.3 % 48-156 11120101 5:04 DL 917120 Surr: 􀀱􀀬􀀴􀁾􀁏􀁩􀁦􀁩􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠96.4 % 􀀷􀀲􀁾􀀱􀀳􀀷􀀠111201015:04 DL 917720 MCL TNRCC 1005􀁔􀁐􀁈􀁔􀁅􀁘􀁁􀁓􀀬􀀱􀁾􀁏􀁾􀀰􀀵􀁾__________􀁟􀁟􀀺􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀀭􀁾􀁾􀀭􀀭􀁾􀀠Units: mglL C6-C12 ND 5 11/1910121:40 AM 916384 >C12-C28 ND 5 .1111910121:40 AM 916384 >C28-C35 ND 5 11119101 21 :40 AM 916384 ND 5 11119/01 21 :40 AM 916384 109 % 70-130 1111910121:40 AM 916384 106 % 70-130 1111910121:40 AM 916384 :P Method Prep Dale Prep Initials: '"T",NR",C",C"",1005='--_l'1 ..11=161200_1_15_:1,0 J_F $oniaWest Project Manager Qualifiers: ND/U -Not Detected at the Reporting limit >MCL -Result Over MaximUm Contamination Umit{MCL) B -Analyte detected in the associated Method Blank D· Surrogate Recovery Unreportable due to D{lution ,. -Surrogate Recovery Outside Advisable QC Umits MI -Matrix Interference J -Estimated Value between MOL and pal 01110658 Page 4 12110l0111:54:19 AM HOUSTON LABORATORY 8BSO INTERCHANGE DRIVE HOUSTON. TX 77054 (713) 660-0901 Client Sample ID MW-l0 Collected: 11/1510112:30:0 SPl Sample ID: 01110658-03 Site: 6·0275,21044479 AnalysesiMethod Result Rep.Limit Oil. Factor QUAL Date Analyzed Analyst Seq.# PURGEABlE AROMATICS MCl SW6021B Units:ugll Benzene 1.1 1 1 11120101 5:29 DL 917723 11120/01 5:29 DL 917723Ethylbenz.n. __-'N;::D;-___-;__ _____-7____􀁾􀁾􀁾􀀻􀀽􀀮􀀻􀀻􀀻􀁟􀀻􀁣􀀮􀀺􀀺􀀭􀀭􀀭􀀭􀀭􀁟􀀻􀀻􀀮􀀻􀁟􀀺􀀻􀀺􀀻􀀬􀁾􀀠Toluene 1.8 1 11120/01 5:29 DL 917723 Methyl tert-butyl ether 140 1 11120/01 5:29 DL 917723 Xylenes,Total ND 1 11120/01 5:29 DL 917723 % % 48-156 72-137 11120/01 5:29 DL 11120/01 5:29 DL 917723 917723 C6-C12 >CI2-C28 >C28-C35 NO ND NO 5 5 5 MCl IIIIRc:;C 1005 1 Unils:mgll 11/19/01 􀀲􀀱􀀺􀁾􀀠AM 􀀱􀀱􀀯􀀱􀀹􀀯􀁯􀀱􀀲􀀱􀀺􀁾􀀠AM 11/19/01 􀀲􀀱􀀺􀁾􀀠AM 915385 915385 915385 Total TPH (C6-C35) Surr: 1-Chlorooctane Surr: 0-T erphenyl NO 110 108 % % 5 70-130 70-130 1 11/19/01 21:50 11/19/01 21:50 11/19/01 21:50 AM AM AM 915385 915385 915385 prep Method TNRCC 1005 1005 Preo Dale 111161200115:10 ,Prep Initials :J_F 􀀧􀀺􀀻􀀻􀀭􀀮􀁾􀀬􀁣􀀺􀀺􀀺􀀧􀀠""'J!-MCL -Result Over Maximum Contamination Llmlt(MCl) D -Surrogate Recovery Unreportab!e due to Dilution MI 􀁾􀀠Matrix lnterference 01110658 Page 5 12/10f(l111:54:19AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE . HOUSTON, TX 77054 (713) 660-0001 Client Sample ID MW-11 Collected: 1111510112:10:0 SPl SamplelD: 01110658-04 Site: 6-0275,21044479 Analys.slMelhod Result Rep.Limit Oil. Factor QUAl Date Analyzed Analyst Seq. II 􀁐􀁕􀁒􀁇􀁅􀁁􀁂􀁬􀁅􀁁􀁒􀁏􀁍􀁾􀁁􀁔􀁾􀁉􀁾􀁃􀁾􀁓______􀁾􀁾____􀁾􀁾__􀁾􀁾__􀁾􀁾􀁾􀁾􀁾SW8021B Units: uSll Benzene 50 11120101 5:54 Dl 917726 􀁅􀁴􀁨􀁹􀁬􀁾􀁥􀁮􀁺􀁥􀁮􀁥􀀠50 11120101 5:54 DL 917726 Toluene 50 11120101 5:54 OL 917726 250 1112010116:58 DR 918281 50 11/20/01 5:54 DL 917126 50 11120101 5:54 OL 917726 250 1112010116:58 OR 918281 SUIT; 􀀱􀀮􀀴􀁾􀁄􀁩􀁦􀀱􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠50 11120/015:54 OL 917126 Surr: 1.4-Dffiuorobenzene 250 11120101 16:58 OR 918281 TPH TEXAS 1005. C6-C12 6.8 5 Mel TNRCC 1005. Unlls:mc/l 11/19101 22:01 AM 916386 >C12-C28 ND 5 11/1910122:01 AM 916386 >C26-C35 Total TPH (CB-C35) Surr: 1-ChtorooClane --surf: 0-Terphenyl ND 6.8 110 107 % % 5 5 70-130 70-130 1 1 11/19/01 22:01 11119/0122:01 11/19/0122:01 11119101 22:01 AM AM AM AM 916388 916386 916386 916386 'prep Method Prep Date Prep Initials ;J FITNRCC 100",5,-_",1",1/:..:1.::6/2::.0", 0:..:1..:1.::5::..:1::.0___-",;:,􀀭􀀢􀀢􀁾􀀠􀀬􀁾􀀭􀁣>"';u:. .=.-􀁃􀀻􀁌􀁾􀁲􀀭􀀺􀀼􀀺􀀷􀀧􀀭􀀭􀀭􀀭􀀺􀀺Sonia West ------------------------Project Manager Qualifiers: ND/U • Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Limit(MCL) B 􀁾􀀠Analyte detected jn the associated Method Blank D 􀁾􀀠Surrogate Recovery Umepor1able due to Dilution • -Surrogate Recovery Outside Advisable QC Limits MI 􀁾􀀠Matrix Interference J -Estimated Value between MDL and POL 01110658 Page 6 1211010111:64:19 AM Quality Control Documentation 01110658 Page 7 􀀱􀀲􀁦􀀱􀀰􀀡􀀰􀀱􀀱􀀱􀁾􀀵􀀴􀀺􀀲􀀵􀀠AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobil 5080275 Analysis: TPH Texa. 1005 WorkOrder: 01110658 Method: TNRCC1005 Lab Batch 10: 16268 Method Blank Samples in Analytl<:al Batch: RunJD: 􀁈􀁐􀁟􀁂􀁟􀀰􀀱􀀱􀀱􀀱􀁧􀁥􀁾􀀹􀀱􀀶􀀳􀀷􀀹􀀠Units; mgll lab Sample JO Client Sample 10 Analysis Date: 1111912001 20;47 Analyst; AM 01110658·018 6-0275 MW·3 Preparation Date: 111161200115:10 Prep By; J_F Method TNRCC 100S 01110658·026 MW-4 01110658-036 MW·10 01110658-046 MW·l1 Analyte i>C26-C35 􀁣􀁡􀀭􀁃􀀱􀁾􀀠Result IRep Limil I , laboratory Control Sample (leS) RunlD: HI'-"_S_01111S8..s16380 Units: mglL Analysis Date: 111191200120:58 Analyst AM Preparation Date: 11/16/200115:10 Prep By: J_F Method TNRCC 100S I ! 􀀭􀀭􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀮􀀮􀀺􀀺􀀻􀀺􀀻􀀺􀀺􀀭􀀻.....􀀭􀀭􀁾􀀭􀀺􀀭􀀺􀀺􀀭􀀺􀀺􀀭􀀭􀀭􀀺􀀺􀀭􀁾􀁾􀀽􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾MattiX);tpike (MS) I Matrix Spike Duplicate {MSO} Sample Spiked: 01110658-01 RunlD; HP_B_011119M16382 Units: mglL AnalYSis Date: 111191200121:19 Analyst: AM Preparation Date: 111161200115:10 Prep By: LF Method TNRCC 100S Analyte Spike Added Result Percent Recovery lower Limit Upper limit >(;12-G28 50 49 98 70 130, CB-CI2 50 48 95 70 1301 Tolal TPH (C&-C35) 100-97 97 70 1301 .... _-..---;:--;-:;--.------,--;::::-:::::;:-...,--;-;;;;--,-=:-;;--7 ."""'1-;-:;:;-,;-;--.......􀀻􀀻􀀺􀀻􀀻􀀻􀀺􀀭􀁾􀀻􀁣􀁾􀀽􀀻􀀻􀁟􀁲􀀽􀀺􀀺􀁟􀀻􀀺􀀻􀁟􀁟􀁟􀁟􀁲􀀬􀀺􀀻􀀻􀀢􀀢􀀢􀀽􀀺􀁟􀁲􀀮􀀺􀀮􀀮􀀮􀀮􀀬􀁟􀀻􀀺􀁟􀀺􀀺􀁟􀀷􀀱 Analyte Sample MS Result Spike Added MS Resul! MS % MSD ,: MSD Result MSD % RPD RPO Low ,High Recovery Spike Recovery limit Limit: Limit Added : >CI2·C28 C6-G12 ND 50 ND 50 SO, 99.7 50 50 1000.345 20 70 130 48' 95.5 50 46 95.3 0.192 20, 70 130 􀁌􀀺􀁾􀀺􀁣􀀺􀁏􀁉􀁡􀀽􀀻􀁩􀀺􀁩􀁔􀁐􀁾􀀽􀀺􀁈􀀭􀀻􀀭􀀧􀀨􀀻􀀻􀁃􀁾􀁂􀀭􀀺􀀮􀀺􀀢􀀧􀁃􀀻􀁦􀀧􀀳􀀺􀁟􀀺􀀵􀀧􀁦􀀮􀀩-:::-:::_..􀀭􀀺􀀺􀀺􀀭􀀺􀀺􀀺􀀭􀀺􀀺􀀺􀂷􀀽􀀭􀀺􀀺􀀺􀀭􀀺􀀺􀀺􀀭􀀺􀁣􀁾􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀀭� �􀀭􀀭􀁴􀁎􀁴􀁄􀀧􀁴􀀭􀀽􀀭􀀭􀀭􀀭􀀻􀁣􀀬􀀰􀁾􀀰􀀱􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀹􀁾􀀸􀀽􀁩􀀽􀀽􀀽􀁩􀀹􀀸􀁾􀀮􀀰􀁾􀀽􀀽􀁬􀀺􀀱􀀻􀀻􀀺􀀰􀀰􀀧􀁴􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀁾􀀹􀀸􀀧􀁴􀁾􀁾􀀭􀀽􀀭􀀭􀀽􀀭􀀭􀀽􀀭􀀱􀀹􀀻􀀻􀀻􀀸􀀽􀀺􀀺􀀻 􀀬􀀮􀁯􀁬􀀮􀀺􀀮􀀺􀀮􀀠"'01-,--..."'20"'01-'::70;;r-"';'13;;;;10....:.:....c Qualifiers: NDIU -Not Detected at the Reporting limit MI -MatriX Interference B -Analyte detected In the associated MethOd Blank D -Recovery Unreportable due to Dilution J -Estimated value between MDL and POL '" ¥ Recovery Outside Advisable QC Limits The percenl·recoveries for QC samples are correct as reported. Due to significant figures and 01110658 Page 8 rounding, the reported RPD may djffer from the displayed RPD values but is correct as reported. 12J10J01 11:54:32 AId HOUSTON LABORATORY 8880 INTERCHANGE ORIVE HOUSTON, TX 77054 (713) 660-0901Quality Control Report ExxonMob!1 5080275 Analysis: PurgeabJe Aromatics WorkOrder: 01110658 Metl1od: SW8021B Lab Batch 10: R48183 MetI10d Blank Samples in Analytical Satch: RunlD: 􀁖􀁁􀁒􀁅􀁾􀀰􀀱􀀱􀀱􀀱􀀹􀁁􀂷􀀹􀀱􀀷􀀶􀀱􀀱􀀠Units: ug/l lab Sample 10 Client Sample 10 Analysis Date: 1111912001 16:19 Analyst: DL 01110658-01A 6-0275 MW·3 01110658-02A MW-4 01110658·03A MW·l0 01110658·04A MW·l1 􀁁􀁮􀁡􀁬􀁹􀁴􀁾􀀮􀀠Result Rep limit Benzene NO 1.0 Elhvlbenzene NO 1.0' Methvl 􀁴􀁥􀁲􀁴􀁾􀁴􀁶􀁴􀀠ether ND 1.01 Toluene ND 1.0: 􀁾􀁥􀁮􀁥..TOlar' NO 1.0: Surr: 1.4·Oilluorobenzene 103.6· 􀀷􀀲􀁾􀀱􀀳􀁑􀀠Surr. 4-aro!flof'lUorobenzeoo 00.2 70-130 Laboratorv Control Sample (LeSl RuniC: VARE_011119A-917604 Units: ug/l Analysis Date: 1111912001 14:58 Analyst: DL ..-Analyte Spike Lower UpperResult IPercent limit I llmitAdded Recovery Benzene 53. 107 7050 130, 70 130.􀁅􀁴􀁨􀁹􀁬􀁢􀁥􀁮􀁺􀀺􀁾􀁮􀁥􀀠50 541 109 Methyl tart·butyl ether 70 130.50 531 106 Toluene 551 109, 70 70 130150 Xylenes,Totai 150 1641 1091 70 130 Matrix Spike (MSJ JMatrix Spike DUPlicate rMSO) Sample Spiked: 01110657-05 RunlD: VARE_011119P.-.S11622 Units: ugJL Analysis Date: 111191200116:48 Analyst: DL Analyle Sample MS MS Result MS% MSD MSD Result Result Spike Recovery Spike Added Added Benzene 17 20: 41 120 20 35 Ethylbenzene 6.6 20 27 102 20 27 Methyl tert-butyl ether 4.8: 20 24 97.4 20 23 Toluene 171 20 38 105 20 37 ,.,..,.... Xylenas,Total 221 60 85 105 60 83 MSD% 􀁾􀀠RPD Recovery ; 91.6 6.5 .. 102: 0.324: 92.4 5.26 104 0.139' 101: 3.24 RPD ILow, IHigh!Umit : Umit Umit i i : : 21 32 164 19· 52 142 20 39. 150 20 381 159 18 53 144 aualifiers: NO/U • Not Detected at the Reporting lrmlt MI -Matnx Interference B -Analyte detected in the associated Method Blank 0-Recovery Unreportable due to Dilution J -Estimated value between MOL and PQL .. -Recovery Outsfde Advisable QC limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01110658 Page 9 founding, the reported RPO may differ from the displayed RPD values but is correct as reported. 121100111:54:32AM HOUSTON LABORATORY M80 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobU 5080275 Analysis: Purgeable Aromatics WorkOrder: 01110658 Method: SW8021B Lab Batch 10: R48183 -_··_--:c:::-::-:-::-c-:-.,--,-,-:-:;--:=---c:-Qualifiers: NON -Not Detected at the ReportIng Umit MI -Matrix Interference 8 -Analyte detected in the associated Method Blank D -Recovery Unreportable due to D1Iutloo J -Estimated value between MOL and POL " -Recovery Outside Advisable QC Limits The percent recoveries for QC samples are correct as reported. Due to signifICant figures and 01110658 Page 1Q rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 12110/01 11:54:32 AM HOUSTON lABORATORY 8880 INTERCHANGE DRIVE HOUSTON. nc 77054 (713) 660-0901 ExxonMobil Certificate of Analysis Number: 01110658 Report To: EA Engineering Mark lach 1420 VaJwood Parkway Suite 170 Carrollton TX 75006· ph (972)484-1420 fax: Project Name: 5080275 Sit.: 6·0275.21044479 SUe Address: PO Number: LWRtI21045043 St.te: Texas State Cort. No.: pate Reported: 1211101 This Report Contains A T olal Of 14 Pages Excluding This Page Date 12110101 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HqUSTON, TX 77054 (713) 660-0901 Case Narrative for: ExxonMobii Certificate of Analysis Number: 01110658 ReoortTo: Project Name: 5080275I Site: 6.()275,21044479EA Engineering Mark lach SHoAddress: 1420 Valwood Parkway Suit. 170 Carrollton PO Number; LWRfI21045043 TX Stalo: Texas 7500S-State 􀁾􀁥􀁲􀁴􀀬􀀠No.: ph: (972) 484-1420 fax: Date Reported: 1211101 Matrix spike (MS) and matrix spike duplicate (MSD) samples are chosen and tested at random from an analytical batch of "like" matrix to check for possible matrix effect. The MS and MSD will provide site specific matrix data only for lhose samples which ara spiked by the laboratory. Since the MS and MSD are chosen at random from an analytical batch, the sample ChOsen for spike purposes mayor may not have been a sample submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this analytical report is delennined by the Laboratory Control Sample (LCS) and the Method Method Blank (MB). The Laboratory Control Sample (LCS) and the Method B!ank (MB) are processed with the samples and the MSJMSD to ensure method criteria are achieved throughout the entire analytical process. Any other exceptions associated with this report will be footnoted in the analytical result page(s} or the quality control summary page(s). Please dQ not hesitate to contact us if you haye any questions or comments pertaining to this dala report. Please reference the above Certificate of Analysis Number. This report shall not be reproduced except in full, without the written approval of the laboratory. The reported results are only representative of the samples submitted for testing. SPL, Inc. is pleased to be of service to you. We anticipate working with you in fulfilling all your current and future analytical needs. 01110658 Page 1 Sonia West Dale Senior Project Manager 12110101 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 ExxonMobil Certificate of Analysis Number: 01110658 Regon-To: EA Engineering Project Name: 5080275 Mark l.ach 1420 V.lwood Parkway Suite 170 Site: Site Address: 6·0275,21044479 Carrollton TX PO Number: LWR#21045043 7500(;ph: (972) 484-1420 fax: (972) 247·7220 .§li!!!!;. State Cert. No.: Texas Fax To: Date 􀁒􀁥􀁾􀁯􀁲􀁴􀁥􀁤􀀺􀀠12fT/01 Client Sample 10 Lab Sample ID Matrix 1 Date Collected Date Received COCIO HOLD 1 :6-0275 MW-3 01110658-01 Water I 11115/0112:00:00 PM 11/16101 10:00:00 AM [J MW·4 01110658-02 Water 1111510112:20:00 PM 11/16/01 10:00:00 AM 0 i MW·10 01110658·03 Water 11111510112:30:00 PM 11116101 10:00:00 AM 01 MW·l1 01110658·04 Water I 1111510112:10:ooPM 1111610110:00:00 AM 0 􀁾􀁺􀂣􀀡􀁣􀀭􀀻􀁲􀁺􀁌􀀭􀁃􀁾􀀠􀁾􀁾______ .._____..__ 121...,10=-10.,..1 Sonia West Date Senior Project Manager Joel Grice Laboratory Director Ted Yen Quality Assurance Officer 01110658 Page 2 121lO/011j;$1:11 AM HOUSTON LABCltATORY 8880 INTERCHAI'IlE DRIVE HqUSTON, TX17054 (713) 66().0lIl1 Client Sample 10 6-{)275 MW-3 Collected: 11/15/0112:00:0 SPl SamplelO: 01110658-01 Site: 6-0275,21044479 Anafyses/Method Result Rep.Limit 011. Factor QUAL Date Analyzal Analyst Seq_II PURGEABlE AROMATICS SW8021BMCl ._-_._-_... Unils:ag/l Benzene 14 111201014:411 DL 917714 Ethylbenzene 2.7 1 11/20/01 4:>111 DL 917714 .._-_. Toluene 1.2 1 11/201014:41 DL 917714 Melhyl tert-butyl elher ______-"-=_ ._-_..._-_140 11120101 4:411 DL 917714 .. Xylenes,Total 1.5 1 11/20/01 4>11 OL 917714 SUrT: 4-Bromofluorobenzene 92.9 % 48-156 111201014:41 OL 917714 114 % 72-137 11/20101 4:41 OL 917714􀁾􀁲􀁲􀀮􀁟􀀮􀁟􀁬􀀬􀁟􀀴􀁾􀁾􀀽􀁩􀁦􀁬􀁾􀁕􀁾􀁯􀁾􀁲􀁯􀁾􀁢􀁥􀀽􀁮􀁺􀁥􀁾􀀽􀁮􀁥􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽� �􀁾􀀽􀀽􀁾􀁾􀁾􀁾􀀽􀀽􀀽􀀽􀀽􀀽􀁾􀀽􀀽􀀽􀀽􀁾􀁾􀀽􀀽􀀽􀀠TPH TEXAS 1005 MCl TNRCC 1005 Unilsang/l C6-C12 NO 5 1 11119101 21:C1t AM 916381 >CI2.-C28 NO 5 1 11/19/01 21:01 AM 916381 >C28-C35 NO 5 1 11/19/0121:01 AM 916381 Tolal TPH (C6-C35) NO 5 1 11/19/o121:C1t AM 918381 SUIT: 1-1-Chlorooctane 113 % 70-130 11119/0121:01 AM 918381 􀁾􀀮􀀿􀀭􀁔􀁥􀁲􀁰􀁨􀁥􀁮􀁹􀀲􀀠109 % 7()'130 11/19/0121:01 AM 916381 Sonia West Project Manager. .__.._-----Qualifiers: NO/U -Not Detected at the Reporting Limil >MeL Result Over Maximum Contamination Limit(MCL) B -Analyte detected in the asSOCiated Method Blank D -Surrogate Recovery Unreportable due to Dilution " -Surrogate Recovery Outside AdvJsable QC Limits MI -Matrix Interference J -Eslimated Value between MOL and POL 01110658 Page 3 12J,0J0111:54:1SAM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 􀁾􀁾􀀷􀀠(713) 660-0901 Client Sample ID MW4 Collected: 11115/01 12:20:0 SPL Sample ID: 0111Q658-02 Site: 6-0275,21044479 AnalysesfMethod Result Rep.limlt Oil. Factor QUAL Date 􀁁􀁮􀁡􀁬􀁾􀁥􀁤􀀠Analyst Seq. If PURGEABLE AROMATICS MCl SW8021B Units: uglL Benzene ND 1 11120101 5:04 DL 917720 Ethylbenzene Toluene ND NO 1 1 11120101 5:04 11120101 5:04 DL OL 917720 917720 Methyl tert-butyl ether Xyienss,Total Surr; 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀁴􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠Surr. 1,4-Dif1uorobenzene 1.2 NO 93.3 96.4 % % 48-156 72-137 1 11120101 5:04 11120101 5:04 11120101 5:04 11120101 5:04 OL OL Ol OL 917720 917720 917720 917720 TPH TEXAS 1005 C6-C12 NO 5 MCL TNRCC 1005 1 Units: mgll. 11119101 21:40 AM 916384 >CI2-C28 NO 5 1111910121:40 AM 916354 >C28-C35 NO 5 1111910121:40 AM 916384 Total TT'H (C6-C35) NO 5 1 11119/0121:40 AM 916354 Surr: 􀀱􀁾􀁃􀁨􀁬􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀁥􀀠109 % 70-130 1 11119101 21;40 AM 916384 1 1111910121:40 AM 916384SUfT: trTerphenyl 106 % 70-130 i I I 􀁾􀀠/'./.) ./:; .'􀀧􀁾..c 􀁾􀀷􀂷􀀺􀁴􀀭􀁥􀀺􀀻􀀮􀁾􀀬􀁟􀁾􀂷􀀠􀁾􀀮􀀼􀀭􀀭􀀭􀀮􀁾􀁾􀀢􀀼􀀮􀀮􀀮􀀮􀀮􀀭􀀮􀀠Sonia West ----------------------.Project Manag=o:=-,___ Qualifiers: ND/U -Not Detected at the Reporting Limit >MCL -Result OVer Maximum Contamination Limit(MCL) B -Anatyte detected in the associa.ted Method Blank D -Surrogate Recovery Unreportabte due to Dilution '" -Surrogate Recovery Outside Advisa.ble QC Limits MI -Matrix Interference J -Estimated Value between MDL and POL 01110656 Page 4 12J1010111:54:19AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HCUSTON. TX 77054 (713) 660·0901 Client Sample ID MW-l0 Collected: 1111510112:30:0 SPl Sample ID: 01110658·03 Site: 6-0275,21044479 Analyses/Method Result Rep.limit 011. Factor QUAL Date Analyzed Analyst Seq.# PURGEABlE AROMATICS Benzene Ethylben_e 1.1 ND MCl SW8021 B 1 1 Units: ugll 11/20101 5:29 Dl 917723 􀀱􀀱􀀯􀀲􀁾􀁾􀁾􀀰􀀱􀁾􀀵􀀺􀀷􀀲􀀹􀁾􀁾􀁄􀀽 􀁬􀀭􀀭􀀭􀀭􀀭􀀭􀀹􀁾􀀱􀁾􀀷􀁾􀀷􀀽􀀷􀀲􀀳􀀠Toluene Methyl tert·butyl ether 1.8 140 1 􀀱􀀱􀀯􀀲􀀰􀀱􀁾􀀰􀀮􀀺􀀮􀀱􀁾􀀵􀀺􀁾􀀲􀀹􀁾􀁾􀁄􀀽􀁬􀀭􀀭􀀭􀀭􀀭􀀭􀀹􀀺􀀺􀀮􀀱􀁾􀀷􀀷􀁾􀀲􀀽􀀷􀀳􀀠􀀱􀀱􀀱􀀲􀁾􀀰􀀱􀀠5:29 DL 917723 Xylenes.Total ND 11I20I01 5:29 Dl 917723 Surr:: 93.3 % 48·156 1 11120/01 5:29 􀁄􀁌􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀹􀀱􀁾􀀷􀀷􀁾􀀲􀀽􀀷􀀳􀀠TPH TEXAS 11)1)5.. MCl______________= ______-:;--__-==__..:.T:..:N.:.:R "'C"'Cc,;1"'0""05 Units: mgll C6·C12 NO 5 1111910121:50 AM 916385 >C12·C28 NO 5.=-____-'---:;.____________7-_____ 􀀱􀀱􀀱􀀱􀀹􀀯􀀰􀀱􀀲􀀮􀀻􀀺􀀱􀀺􀀺􀀺􀀺􀀵􀀰􀁾􀁁􀁾􀁍􀁾􀀭􀀭􀀭􀀮􀀻􀀹􀀮􀀺􀀺􀀱􀀶􀁾􀀳􀀺􀀺􀀻􀀻􀀸� �􀀠>C2S-C35 ND 5 11119/0121:50 AM 916385 Total TPH (C6.C35) SUIT: 1-Chlorooctane Surr: 0-T erphenyl ND 110 108 % % 5 70·130 70·130 1 1 11119/0121:50 1111910121:50 11119/0121:50 AM AM AM 916385 916385 916385 Prep Method TNRCC 1005 IPrep Date '111161200115:10 iPrep Initials J F 􀁾􀁾􀁾􀁾􀁌􀀮􀁾􀁾􀁾􀀠􀁾􀁾__________________________________ Sonia West Project Manager Qualifier'S: ND/U -Not Detected al the Reporting Limit >MCL -Result Over Maximum Contamination LJmit(MCL) B -Analyte detected in the assoclated Method Blank o -Surrogate Recovery Unreportable due to Dilu1ion • 􀁾􀀠Surrogate Recovery Outside Advisable QC Llmits MI 􀁾􀀠Matrix Interference J 􀁾􀀠Estimated Value between MOL and POL 01110658 Page 5 12110f()111;54:19 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054􀁾􀁾􀀷􀀠(713) 66(l·0901 Client Sample 10 MW-11 Collected: 1111510112:10:0 SPl Sample 10: 01110658-04 Site: 6-0275,21044479 Analyses/Method Result Rep.limit DII. Factor QUAL Dale Analyzed Analyst Seq. # PURGEABlE AROMATICS MCl SW8021B Units: ua/l Benzene 390 50 50 111201015:54 Dl 917726 Ethylbenzene NO 50 50 11120101 5:54 Dl 917726 Toluene 980 50 50 11120101 5:54 Dl 917726 Methyl tert·butyl elher .. Xylenes,Tota.! 43000 152 250 50 250 50 1112010116:56 11120101 5:54 D_R DL 916261 917726 Surr: 4-8romofluorobenzene 91.8 % 411-156 50 111201015:54 OL 917726 Surr: 4-8romofluorobenzene 90.2 % 411-156 250 1112010116:56 DR 918281 SUIT: 1.4-Difluorobenzene 108 % 72·137 50 11120101 5:54 OL 917726 Surr; 1,4-Dinuorobenzene 210MI % 72·137 250 11120101 16:56 DR 916261 TPH TEXAS 1005 MCl TNRCC 1005 Units: mall C6-C12 >CI2-(;28 >028-C35 6.8 NO NO 5 5 5 11/19/01 22:01 11119/01 22:01 11/1910122:01 AM AM AM 916386 916366 916386 Total TPH (C6-C35) 6.8 5 1111910122:01 AM 916386 Sun: 1-Chlorooctane 110 % 70-130 1111910122:01 AM 916386 SUIT: 0-Terphenyl 107 % 70-130 11/19/01 22:01 AM 916386 Sonia West Project Manager Qualifiers: NDIU • Nol Detected at the Reporting Urnit >MCl-Resull Over Maximum Contamination limit(MCL) B -Analyte detected in (he associated Method Blank D -Surrogate Recovery Ur'I(eportable due to Dilution .. -Surrogate Recovery Outside Advisable QC limits MI -Matrix Interference J -Estimated Value between MDL and POL 01110658 Page 6 12110R}111;54:19AM Quality Control Documentation 01110658 Page 7 12110/0111:54:25AM HOUSTON LAiJORATORY BBBO INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660·0901 ExxonMobil 5080275 Analysis: TPH Texas 1005 WorkOrde..: 01110658 Method: TNRCC 1005 Lab iJalch 10: 16268 Method Blank Samples in Analytical Batch: RunID: HP_8_0111198-916379 Unfts: mg/l lab Sample 10 Client Sample 10 Analysis Dale: 11/19/200120:47 Analyst: AM 01110658·016 6·0275 MW·3 Preparation Date: 111161200115:10 Prep By: J_F Method TNRCC 100S 01110658-026 MW-4 01110658·03B MW·l0 01110658·04B MW-ll : Analyle Result IRep Limit: >C12-C28 ND: 5.0 >C28-C35 ND, 5.0 C6-C12 NO 5.0 Total TPH C6-C35 ND' 5.0 $\.If'i': 1..chtof'O()Ctane 110.5 􀀷􀀰􀁾􀀱􀀳􀀰􀀠$1.Ifr. 0-TerphOOY.! ..._._L... 􀀱􀁏􀁓􀁾􀀴􀀠70-130 Laboratory Control Sample (les) RunlD: HF'􀁟􀁂􀁟􀀰􀀱􀀱􀀱􀀱􀀹􀁂􀁾􀀹􀀱􀀶􀀳􀁓􀀰􀀠Units: mgfL Analysis Date: 11/1912001 20;58 Analyst: AM Preparation Date: 11/1612001 15;10 Prep By: J_F Method TNRCC 1005 Anatyle Spike Added Result Percent Recovery Lower Limit Upper limit , >C12-C2B 50 49 9B 70 130: CB-C12 50 48 951 70 130: Total TPH (C6·C3S) 100 97 ..􀁾.... 70 130' Matrix Spike IMS11 Matrix Spike Duplicate fMSO) Sample Spiked: 01110658·01 RunlD: HP􀁟􀁂􀁟􀀰􀀱􀀱􀀱􀀱􀀹􀁂􀁾􀀱􀀶􀀳􀀸􀀲􀀠Units: mg/l Analysis Date: 111191200121:19 Analyst: AM Preparation Date: 11116/2001 15;10 Prep 6y: J_F Method TNRCC 100S 􀀬􀀭􀀭􀁾􀀠IAnal),!_ Sample MSD MSD Result MSD% IRPD RPD I low HighMS MS Result I MS % Limit : LimitResult Spike Recovery LimitSpike; ! Recovery : Added Added 1 ND 50 50 7050 99.7 50 10010.345 20 130'>ci2-C28 NO 50 48 95.5 50 48 95.310.192 20 70 130C6-C12 98.0' 0NO 98.0 100 98Total TPH (C6-C3S) 1Q{)_ 98 􀁾􀁟􀀿􀁏􀁾􀀠Qualifiers: ND/U 􀁾􀀠Not Detected at the Reporting Limit MI-Matrix Interference B -Analyte detected in the associated Method Brank D 􀁾􀀠Recovery Unf'eportable due to Dilution J 􀁾􀀠Estimated value between MOL and PQL ., -Recovery Outside Advisable ac Limits The percent recoveries for QC samples are correct as reported. Due to signifrcant figures and 01110658 Page 8 rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 1211010111:S4:32M1 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON. TX 77054 Quality Control Report (713) 600-0901 ExxonMobil 5080275 Analysis: Purgeable Aromatics WorkOrder: 01110658 Method: SW8021B Lab Batch 10: R48183 Method Blank Samples in Ana[ytical Bak:h: RunlD: VARE_011119A-917611 Units: ug/L Lab SarnDrs fO Client Sample ID Analysis Date: 1111912001 16:19 Analyst: DL 01110658-01A 6-0275 MW-3 01110658-02A MW-4 01110658-03A MW-10 01110658-04A MW-11 Laboratorv Control Sample (LeS) RunlD: VARE_011119A·911604 Units: ug/L Anafysis Date: 111191200114:58 Analyst DL Analyle Spike Added Result Percent Recovery Lower limit Upper Limit Benzene 50 53 107 70 130 Ethylbenzene 50 54 109 70 130 Methyl tart-butyl ether 50 53 106 70 130 Toluene 50 55 109 70 130 Xylenas.Total 150 164 1091 70 130 Matrix Spike (MSll Matrix Spike Duplicate (MSD) Sample Spiked: 01110657-05 RunlD: VARE_011119A-917622 Units: uglL Analysis Date: 111191200116:48 Analyst DL NDfU • Not Detected 􀁾􀁴􀀠tl1e Reporting LimIt Ml -Matrix Intenerence B • Analyte detected in the associated Method Blank D -Recovery Unreportable due to Ollullon J 􀁾􀀠Estimated value between MDL and POL • -Recovery Outside Advisable QC Limits iBenzene !Ethylbenzene ._...__. Analyte : Sample MS MS Result MS% MSO MSD Result Result Spike Recovery Spi"e Added Added 17 20 41 35 6.6 20 27 27 MSD% RPO Recovery 91.6 6.5' 102 0.324 RPO limit 21 19 nIMethYI teri:butyl etl1er 4.8 20 24 97 23 92.4 5.26 20 ,Toluene 17 20 38 1 3 104 0.139 20 jXylenes,Total I 22 60 Qualifiers: 85 1 􀀸􀁾􀀠101 3.24 18i Low High Limit Limit 32 164 52 142 39 150 38 15953, 144 The percent recoverIes for QC samples are correct as reported. Due to significant figures and 01110658 Page 9 rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 12J1D!0111:54:32AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (113) 660·0901 ExxonMobil 5080275 Analysis: Purgeable Aromatics WorkOrder: 01110658 Method: Swa021B Lab Batch 10: R48183 Qualifiers; NO/U -Not Detected at the Reporting Urn;! MI-Matrix Interference 8 􀁾􀀠Analyte detected in the associated Method Blank D· Recovery Unreportable due to Dilution J 􀁾􀀠Estimated value between MOL and POL .. -Recovery Outside Advisable QC Limits The percent recoveries for QC samples are correct as reported, Due to significant figures and 01110858 Page 10 rounding, the reported RPD may differ from the displayed RPO values but is correct as reported. 􀀱􀀲􀁊􀀱􀀰􀀱􀁪􀁽􀀱􀀱􀀱􀁾􀀵􀀴􀀺􀀳􀀲􀁁􀁍􀀠 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobii 5080275 Analysis: Purgeable Aromatics WorkOrder; 01110658 Method: SWS021B Lab Batch 10: R4a218 Method Blank Samples in Analytical Batch: RunlD: VARD_011120A-918272 Units: ug/L Lab Sample 1D Client Sample 10 Analysis Date: 11/2012001 11 :12 Analyst: D_R 011106SS-04A MW-11 Analyle Result Rep Limit! 􀁾􀀺􀁾􀁵􀁥􀁲􀁴􀀭􀁢􀁵􀀠Sun-: 1 4-Diftether uorobenzeno ND 95.3 1,0 72-130 Sun-: 4·BromoHuo!'Obenlene 88,3 70-130 􀁌􀁡􀁢􀁯􀁲􀀮􀁦􀀻􀀡􀁾􀁯􀁲􀁹􀀠Control Sample (LeS) RunlD: VARD_011120A-916271 Units: ug/L Analysis Date: 11/201200110:47 Analyst: D_R I An.lyle I SpikeAdded Result Percent Recovery lower IUpper Limit limit ,Methyl tert-butyl ether , 50 53 105 70, 130 Matrix Spike (MS) I Matrix Spike Duplicate {MSDl Sample Spiked: 01110360-10 RunID: VARD_011120A·918585 Units: uglL Analysis Date: 11/2012001 18:22 Analyst: D_R Analyle Sample MS MS Result i MS% MSD MSD Result MSD% Result Spike ! Recovery Spike Recovery Added I Added 'RPD IRPD limit Methyl tert-butyl ether NO, 20 241 120 20 24 12010,145 20 Low High Limit Limit 39 150 Qualifiers: NO/U • Not Detected at the Reporting Limit MI-Matrix Interference B 􀁾􀀠Analyte ootected In the associated Method Blank D -Recovery Unreportable due to Dilution J -Estimated value between MOL and pal • 􀁾􀀠Recovery Outside Advisable QC Limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01110658 Page 11 rounding, the repOrted RPD may differ from the displayed RPD values but is correct as reported. 1211010111:54:33 AM Sample Receipt Checklist And ChC;lin of Custody 01110658 Page 12 121100111:54:38 AM HOUSTON LABORATORY 8880 INTERCHANGE ORlVE HOUSTON, TX 77054 (713) 660-0901 Sample Receipt Checklist Workorder: 01110658 Received By: HB Date and Time Received: 11/16101 10:00:00 AM Carrier name: F.dEx TemperatlJre: 3 Chilled by: Water Ice 1. Shipping eontainer/cooJer in good condition? Ye Ii2l NoD Not Present 0 2. custody seals intact on shippping container/cooler? Ye 0 NoD Not Present 0 3. Custody seals intact on sample bottles? Ya 0 NoD Not Present 0 4. Chain of custody present? Ye Ii2l NoD 5. Chain of custody signed when relinquished and recelv Ye Ii2l NoD 6. Chain of custody agrees with sample labels? Ye Ii2l NoD 7. Samples in proper container/bottle? Yo Ii2l NoD 8. Sample containers intact? Ye Ii2l NoD 9. Sufficient sample volume for indicated test? Ye Ii2l NoD 10. All samples received within holding time? Yo Ii2l NoD 11. ContainerlTemp Blank temperature in compliance? Ye Ii2l NoD 12. Water· VOA vials have zero headspace Ye 0 NoD Not Applicable 0 13. Water· pH acceptable upon receipt? Ya 0 NoD Nol Applicable 0 SPL Representative:! Contact Date & Tlme:LI____________...J Client Name 􀁣􀁯􀁮􀁴􀁡􀁣􀁴􀁥􀁤􀀺􀁉􀁐􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀁾􀀠 Non Conformance I Issues:" 􀁆􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽� �􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀁾􀀠Client Inslruction.:IL-______________________________________..J 01110658 Page 13 12/100111:54:44 AM " ........ ! " .... /..ri) EXXON COMPANY, USA. (Sauthw... & W••hlngtan" CHAIN OF CUSTODY RECORD NO. UtI\ UIJ! J () Exxon Engineer. 􀀬􀁬􀀩􀁾􀀰􀀱􀀠Phon.:1!!R71'1-4>f4-9Q19 Consultant Co. Name Contact: 10 M 41'k Lt4(,h Addr..s: /4Z" 􀁩􀀮􀁫􀁊􀀢􀁬􀁜􀀺􀁾􀁐􀁨􀀮􀀮􀀬􀁆􀀢􀀢􀀺􀀠,'7:} -Z41·1Z"Z 0 k4l'l'f" dHaA 􀁾'''It:'br>"&-. RAS"It. 􀀨􀁐􀀧􀀺􀀧􀁏􀀬􀀻􀁩􀀷􀁲􀀭􀀭􀀭􀁾􀀻􀀧􀁾􀀻􀀻􀁾􀁉􀀼􀁉􀁕􀀻􀀭􀀻􀀻� �(TN Only): __-=:--:--____ AFE .. (Terminal Only): Consultan! Project #:.20 fSOQ 􀀱􀁾􀀠Looatlon: &:/+LJne,...J 111M",Itt+f (City) A44', 5tSq (Stata, Ili('EE 'I 0 C&M 0 5 Con.ull"nt Work Rele••• #: 􀁾􀁏􀀯􀀴􀁽7 q . Sampled By: 􀁢􀁾􀀱􀀱1hPIn;;, 􀁊􀁁􀁲􀁬􀁴􀀺􀁡􀁮􀁾􀀧􀀱􀁬􀁡􀀮􀀠SAMPLE 1.0. 􀁾􀁏􀁁􀁔􀁅􀀺􀁲􀁔􀁉􀁍􀁅􀁩􀁣􀁯􀁲􀀮􀁬􀁾􀁩􀁇􀁒􀁁􀀸􀁲􀀭􀁍􀁁􀁔􀁒􀁩􀁘􀀠10ll£ft1_ G-C:X17S n7/, 1_ -:; I(/1 S'􀁾􀁬􀁬􀁾􀁑􀀮􀀠1x:1;lsocrR Itic. ) ANALYS'S REQUEST: ICHECK APPROPRIATE BOX) pageLarJ. OTHER 00 􀁾q 􀁾􀀠I 􀁾􀀠0 􀁾􀀠10 I􀁾􀀠0, o It 􀁾􀀠I􀁾fu 􀁾􀀠/17"'J-AJ 􀁖􀁉􀀴􀁾􀁍􀁬􀀧􀁡􀀮􀁊􀀬􀀠1f.1tJ .:IUI 􀀢􀀧􀁾􀀯􀁤􀁾􀀠III! I I I I \ 􀁉􀁾􀀠I II I It I I I I I I I I I I I I I 1l1/U-1 J t't'lfk Ig/o " .,. ,,,. , • ITAT , , I'􀁓􀁐􀁅􀁃􀁾􀁬􀀠􀁏􀁾􀁾􀁏􀁎􀁕􀁍􀁉􀁔􀁾􀀠(SP!.ify) 11 RiMARKs: -' 12 HR./\-,24HR. 96 HR. •48 HR. 8 Business ·CoNKl US Prior Other to Sendll'lO SImple EXXON UST CONTRACT NO, C41483 SPECIAL REPORTING REOUIREMENTS (Specify) LAB USE ONLY laf II Storage localion PDF 0 D eoo QAlQC level Slanda'. CJ CLP CJ 0"'.. CJ /] "? I FAX 0 )fFAX C.O.c WIREPORT WORK ORDER 􀁾􀁬􀀩􀁬􀁬􀀧/\I 1d LAB WORK RelEASE /I: ?f1J (Y Time Rl!allved By: CUSTODY ReHnquish Dal. Time R",'ved By: RECORD Rollnqulshed; Date Time I O{-m(5:.> c 􀀳􀁾􀀠, " I o o 􀁾􀀠'" 􀁾􀀠􀁾􀀠r " 'i -< 􀁾􀀠a• « c c «• , \ Triplicate. 0ri91nal ' White lab's Copy • amn CI"ol Copy' Yellow o Email address:water.well@license.state.tx.us 6) Drilling Dale o Reconditioning a Deepening 4) Proposed Use (check) o Industrial 0 Irrigation a Irpublic Started //I /'/I () ! Dia.(in) From (ft) To (ft) 􀁾􀁾􀀭􀀫􀀭􀀭􀁾􀁾􀀴􀀭􀁾􀁾􀁾􀀠completed 1/I /'/I i) I Environmental Soil Boring Domestic Public Supply 0 De-watering 0 TestweU submitted? 0 Yes 0 Drilling Method (check) Driven Air ROlary 0 Mud Rotary 'ta' Bored Air Hammer 0 Cable Tool " 0 Jetted Other ------------8) Borehole o Dla. (in.) 9) Cementing Dati! 5) Attention Owner: Confidemialily Privilege Notice on reverse side of owner's copy. Texas Department of License and Regulation Water Well Dd/let/Pump Instal/et Ptogtsm This form must be completed and fued with the depanment and Qwner. within 60 days upon completion of the well. P.O. Box 12157 Austin, Texas 78711 15121463-7880 FAX (5121463-8616 Toll free (8001803-9202 within 48 hours o Jet o Submersible 0 Cylinder oBailer a Jetted 0 Estimated DYES 0 NO If yes. did you ,ubmit a REPORT OF UNDESIRABLE WATER Type Type of Water Depth of Strata ________ Was a chemkal analysis made 0 Yes 0 No Cementing from /./.? ft, to ..",-=,---,,-_:ft. 1/of saeks used 􀁾􀀠ft, t9 ft; lofsa<;ks used ___ Method 􀁕􀁳􀁥􀁤􀁜􀀮􀀮􀁟􀁾􀁾􀁾􀁶􀀺􀀮􀀬􀀭􀀬􀀢􀀬􀀮􀀮􀀬􀀮􀀬􀀬􀀭􀀭􀀢􀀬􀀬􀀡􀀧􀀬􀀬􀀬􀁶􀀧􀀻􀁾􀁬􀀢􀀧􀀭􀀭􀀢􀀢􀀧􀀾􀀭􀀧􀂷􀁾� �􀀢􀀧􀀭􀀧􀀭􀂷-,1.:.'_____ Cementing By r;-' 􀀬􀁾􀀠Distance to septic system field or other concentrated contamination __fL . Method of verification of above distance 10) Surface Completion oSpecified Surface Slab Installed oSpecified Surface Sleeve InstaUed Pitless Adapter Used Alternative Procedure Used 11) Water Level Static level ft. below Date __􀁾􀁟􀀭􀀢􀀺􀁉__ Artesian Flow gpm. Date I 12) Packers Did you knowingly penetrale a strata which contain undesirable constituents. TDLRFORMbOO!WWD White"TDLR Yellow -Owner Pink -Driller/Pump Installer Banks Water Well Report TM Information Solutions, Inc. October 25, 2001 CUENT EA Engineering. Inc. 1420 Valwood Parkway. Suite 170 Carrollton. TX 75006 SITE Exxon 6'()275 4191 Beltline Rd. Addison. TX 75244 102501'()83 P.O. Box 12851, Capitol Station, Austin, TX 78711 1701 Nueces, Austin, TX 78701 512.478.0059 FAX 512.478.1433 e-mail banks@banksinfo.com ©Copyright 1998 by Banks Information Solutions, Inc. Banks Information Solutions, Inc. '-"=i·cotl D ' //*SubIKt8tt. Water Well Report,. Map of Wells within One-Half Mile =Addison 2 • 8 Valle Rd Si 􀁏􀁾􀁾􀁏􀁾􀀮􀀲􀁾􀀵􀁾􀁾􀁏􀁾􀀮􀀵􀁾􀁾􀁏􀀮􀁾􀀷􀀵􀁾􀁩􀁩􀁩􀁩� �􀁩􀁩􀁩􀁾􀀱􀁾􀁾􀀱􀀮􀀲􀀵􀀠Miles • Ground Water W ••1a (Clusler) • Ground W ••W.D AIrport D Water body Banks Information Solutions, Inc.L' Part Ho.pbl cj State P.O. Box 12861, Capitol Station Austin, Texas 78711 1701 Nueces Austin, Texas 78701 I7.'v. ""h..,Prtrrwy rGlldlSI SKondiry and connectlnll rGlld 512-478-0059 FAX 512-478-1433 EMail: BANKS@BANKSINFO.COMN LocelrOlld /\.' Ac:cess nIoIId Octobe r 25, 2001 Banks Water Well Report TM Information Solutions, Inc. DETAILS . State 10 I Banks 10. Owner 'Of Well Type OrWell . Oeplh OrIHed COrripieHonDate LongHude Latitude " 33-02-4e 4811300090 Fred Harrington Domestic 320' 08/04/1970 -96.84031 32.9526 i State io . BQnkslD, 1 33-02-405 4811300970 IMAP 10 I2 Owner Of Well c.s. Hamilton TYpe Of Well .. ----Domestic ------------Depih Ddlled 800 ' CompleHon Date 0110111937 . Longitude -96.84111 ...... -LaHtude 32.94889 P.O. Box 12851, Capitol Station, Austin, TX 78711 1701 Nueces, Austin, TX 78701 612.478.0069 FAX 512.478.1433 e-mail bankS@banksinfo.com @Copyright 1998 by Banks Infonnation Solutions, Inc. Banks Water Well Report TM Information Solutions, Inc. SUMMARY Water Well Report "'Research Mapping Protocol The Bank. Information Solutlons,lnc. Water Well Report 􀁾􀀠Is prepared from ""ISIIng stale water well databases and addlUonal file data/records researeb conducted at T""a" regulatOf}' authorities. Submission ofdriller's log records upon completion of a drtlled water well became mandatory In 19li6. The state ofT",,"" has processed Ihese records Into several different filing systems within two state regulatory authorities. The water welililes, records and map loCations are maintained by the Texas Natural Reaou.... Cooaervation CommIsaionrrNRCC) and _ Texas Water DeVeIopnent Board(TWDB). Actual water well site locations ofIIIls report are geocoded and geopIoIIed directly from tile drilling records, drilling scheduJes, and driller's logs and ma"" su_ed by the water well doll..and maintained at_two primary water well regulatory authorities. Below Is a descliptloo oftile four filing systems utllized lorwell drilling records. Texalil Water Development Bo,,", (TWOB) Tex••Water Development Board maintains a file system 01_wafer well locations. TheSe well files are water well site locations lIIat hove been verified with • Held Inventoty Inspection by TWOS personnel. The weHs are lISS!gned a State ldenllll_ Number unique 10 that weiland plotted on county base map$, U.s.G.S. 7.6 minute topographical quadrangle map$, and In./lou"" geographk: Information system. Records will also Include analytical data attached with each drilling record. ThI.I. the cu....nt prolocolfor maintainingwater well records within the TWDB. Texalil Natural Resource Conservation Commission (TNRCC). The Tex"s Natural Resou_Con_Commission maintains a file system of plolled, partially numbered, and un· numbered water welllocaUons. Plotted water welilile. are water well .ltolocatlons Ihal have been determined from map information submitted on water well logs and subsequently pIolIed on TWOS county highway base mapa. This type of mapping and IIllng procedure ceased In June 1986. Partially numbered water well files are water well site locations pr_from 1986 lllrough 1990. These Wells .re provided. S_ldenlilication Number which establishes tile Well Iocallon somewhere within a 2.6 minute quadrant ofa 7.fJ minute quadrangle map, but tile aile _ hal never been Precisely mapped or verified by a !ilIa!e ofTexas staffmember. Un-numbered waler well ftles are water well site _s lllal have been pr_since June 1986. TIleR well records are filed solely on their county _ and are not provided a !ilhde Identlliallon Number nor are 1II0y mapped. This Is Ihe cu"ent prolocolfor malnlalnlng wat ..well records within tile TNRCC. Disclaimer Banlta InfomIaIIon SolutIo ..... Inc. hea pet10rmed a tIIorough and diligent search of all wells recorded with tile Texas Water DeveIopmenI Board and tile Teus Natural Resource C u••4r----------------------r-'",....􀀬􀀢􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀁾􀀧...􀁾􀁬􀁌􀁱􀀮􀀮􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀮􀀮􀀢􀀢􀀬􀀭􀀭􀀭􀀴i-----:--______________r--"'-""-"'_____f!.l!!!.. ..f:!! Tn fl. 􀁾􀀧􀁬􀀼􀀡􀀠r,,,;-;;""""""...,...􀀻􀀭􀀻􀀻􀀬􀁾􀁾􀁟􀁾􀀮􀀬􀁾􀀬􀀧􀁾􀀡􀀡􀀢􀀭oriw 11 􀀭􀀧􀀡􀀡􀀡􀁮􀀢􀀢􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀫􀁲􀀧􀀧􀀧􀁏􀀩􀀭􀀮􀀽􀁲􀁵􀀭􀀻􀀽􀀻􀁲􀁵􀁲􀁮􀁃􀀧􀁟􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭 􀀭􀁾􀀠􀀤􀀮􀁾􀀢􀀧􀁰􀀮􀁊􀀮􀁴􀀠w..1t 􀁾􀁉p.'_ ", '"Id"____,,.;. ..It''---'t......... dt.ar __.... ,Z"tIO 􀁴􀁟􀁾􀀬􀀨•. "_I.... 􀀱􀁯􀁉􀁾􀀠...􀁾􀁃•.n o..U 'f?!4?() UJlgt 􀀧􀁑􀁾􀁾􀁬􀁬􀁊􀁴􀀮􀀮􀀮__􀁉􀁾􀀮􀁤􀀮� �􀀭􀀭&I,.... __􀀮􀁟􀁾􀀢􀀠Aft'.I'" prfl'...􀁾􀁾􀁬􀀱... "".. _ .... i,,'''' "",.. .z:fl..ao .!,n..l", n""---,,,", 􀁾􀁉􀁉􀀠U ..... I\I:Ioorl..o, "l'u",su. 􀁾􀁥􀁴􀀬􀀠,t-;.. I,2 (.. 􀁉􀀭􀀺􀀺􀀺􀀺􀀭􀀺􀀺􀀺􀀺 􀀧􀁟􀁾􀁮􀁾􀀮􀁷􀁾􀁾􀁾􀀮􀁾􀀧􀁣􀀧􀁾􀀢􀁾􀁮􀁾􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀠bftMol t........dliQ. 11) 'll.l.n:Ir. q,W.ltr,II.... <:Mools"",, .,.,d)".lo _ .... , '" :&nol o 􀀬􀀼􀁾􀁯􀀻􀁴􀀻􀁕􀁉􀀢􀀧􀀠.... U n 􀁾􀀠1hItl 1Ia. :"1'...... U"'., 􀁾􀁬􀁏􀁦􀁏􀁜􀁬􀀧􀀼􀀢􀁴􀀠I4._________ ........_________________________ -+-+-I I3. 􀁾􀀮􀀮􀁴_____ 􀁾􀁁􀁒________b __4..f:tQ_.f't.•bow -.1, 􀀢􀀪􀁾􀁢􀁲___Z7)E.o ______ _ L. 􀁾___ ... __________􀁾􀀮􀀮􀀳􀀮􀁚􀁟􀁊􀀠llIIC, 􀁑􀁾􀁬􀀧􀁴􀂫􀁬􀁾􀁉􀁩􀁩􀀺􀁩􀀺􀁴􀀠__ ... ______ _ 5. l!!l!2' _.__ gqq__,,--.__i<.'1t2__", 􀁾􀀬􀀺􀁊􀀮􀀠b«d:. 6. 􀁾􀀮0:PP:w.... 5'; .. 􀁤􀁾􀁶􀀮􀁵.. 􀁾􀀮􀁡􀀮􀀮􀀮􀀮􀀮􀀺􀁴􀁾____________􀁾􀀠1 • .!'!!t. 􀁟􀁾_____________________________􀁾􀁴􀀭􀀭􀀭􀁟􀀭􀁟􀀠􀀻􀀮􀀮􀀬􀁾􀀠􀀮􀁬􀁉􀁾_____• 􀁂􀀮􀀭􀁬􀀮􀁾􀁟... __tn.. 􀁬􀁫􀁾􀁟... ____R. Clil_su.-.________ tl.􀁾􀀮􀁾􀀠_________􀁾􀀠lAo ______ ... ______ ... ___ ... _____ '" _ ... __ ..... ___ ... __ ... ____ _􀁾􀀮􀀠ria7j 7 &. 􀁾n.1_____􀁊􀁦􀁩􀀧􀁻􀁥􀁾􀁴____􀁾􀀶 MII4Iil.. _____________ BP-__!i__ s1z. ,. 􀁾􀀠􀁾􀀠􀁾􀁉,. n-____ ......._____ ..G*i ......... ....._____________ _ 􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭� �􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭 2 p",h. 􀀱􀀱􀀮􀀬􀁾􀁌􀀬􀀢􀀤􀁳􀀮􀀠.3 .3 􀀮􀀳􀁾3" h$/"" 􀁾􀀠 ISS" -u.3 8 􀁾􀀧􀀱􀁳􀀢􀀠 􀁾􀁾􀀠$1, 71 U.;A lIi. 6;5s" 23 "U>􀁾􀀢􀀠(,;,70 IS (;Io 10 10 '<"f0 710 􀁾􀁣􀀠71S 5> 7Zo S" 7'f!> as 7(;5: .2..0 748 .3 z,.:!1'00 􀁆􀁯􀀢􀁗􀀱􀁑􀁊􀀧􀁾􀁮􀀠So It. ,(;,.N.5'f'; SJy 􀁳􀁾􀂢􀁬􀁴􀀠fl:,J..... ski... a....,.,." sl.ql .. 81.... ll/..ql" 8 ...""" .$ h..;.1e. Sly SM./" 􀁾􀀬􀀮s .... J g,...C' 􀁳􀀮􀀢􀁾􀀱􀁥􀀠 􀁷􀁾􀁳􀁾􀀠 s.,,,r/., 􀀮􀁳􀁾􀁾􀀠l:<:iii-J ilIA,/':' ""'{,..s4tlJ .s.-,., ",,;...fe Sd)' <$1u,.1. 􀁥􀁫􀁳􀁾..4 4""""" sA..k 81"", sA"I., LiI"'n's;; C/>4-c.. I • _0• ,,.1.::1 '" • • • • nvoSff.lNCM fR...,. a.3(t.7eJ 􀁃􀁾􀀧􀁙􀀠-_. -...􀀭􀀬􀀭􀁾􀀭.. _-,," ... ·-. , EA Engineering, Science, and Techrwlogy APPENDIXD WASTE MANAGEMENT AND DISPOSmON (Soil (drill cuttings) were transported to the Waste Management Landfill in Lewisville, Texas. Purged groundwater was treated with a carbon treatment unit and discharged to the landscaped area on site.) Divestment Assessment INSTRUCTIONS ON REV.eRSE SIDE TEXAS NAlURAL'ResbuRCE CoNSERVATION COMMISSKlN Petroteum Storage Tank Division, MC 137 P.O. Box 13067 Austin, T axas 78711-3087 Pleas. type orprint (Form designed for use on al/tell2 ·pffch typewriler:) I 1. Generator's LPST 10 No. or ST 10 No. 2. Page 1 of PETROLEUM·SUBSTANCE WASTE MANIFEST ]0.-:·7.', 3. 􀁇􀁾􀁮􀁥􀁲􀁡􀁬􀁯􀁲􀀧􀁳Name; Contact Person, and Mailing Address A. Stale Menifest Document No. " 􀁾􀀬􀀱􀀠􀁾􀀱􀀠181832􀁬􀀺􀁘􀁾􀁻􀀨􀀬􀁎􀀠􀁾􀁦􀀡􀀠JBJ!.. t ';-,R l1 .Iit-\1'H ')}.; TJl!Jt-: 􀀨􀁾􀀩􀁲􀁡􀁕􀁬􀁟􀀠Rm K"""""'"• 1·; "" H.J ( ;.-, PO fJ(I,,, :.3'\\] H,"!.f:stl.'.r;, T\ 􀀧􀀬􀀢􀁾􀁾􀀺􀁩􀀰􀀠B. Generato(s Facility 10 No. 4. GeneratorsPhone ( ) Generator's Fax ( ). . .. 􀁾􀀠-,,Generator's Facility 􀁎􀁡􀁲􀁩􀀬􀁾􀀮􀀠􀁃􀀻� �􀀻􀀻􀁾􀁣􀁬􀀠\>';,rson, and Physical Address '. . j -;.-. 5. !:X\,Ot-;t\.f0BfL ((is 6-0n:vDall:! '.j(I\Hrtl C. Generator's Tank Owner 10 No. 􀀴􀁩􀁾􀀢􀀩􀀱􀀠􀁂􀁤􀁴􀁬􀁭􀁾􀀠/....􀁤􀁊􀁴􀀺􀀺􀀺􀀮􀁾􀀩􀁬􀀱􀀮� �'TX 6. G_ralors Facility Phone ( ) Generator's Fax ( ) }'.': 􀁾􀁜• II " ;. . 􀁾􀀠7. Transporter 1 Company Name and Address O. Transporters Phone , 􀁁􀁌􀀮􀀧􀁜􀁾􀁬􀁴􀁃􀁾􀀠TtUckmg {9:t:2) .1.t:\,)771 20J(, Ccnhuy 􀀨􀀧􀁴􀀮􀁾􀁟􀁈􀀱􀁣􀁲􀀠Hin.1 ConlactPerson, hvmg,"fX 1<;00: Jt.!trCla) 8. Transporter 2 Company Name and Address E. Transporter's Phone Contact Person: 9. Designated Facility Name and Site Address F. Facility's Phone 􀁜􀀢􀀻􀀧􀁾􀀻􀀺􀀵􀁬􀁦􀀮􀀺􀀠tvianau..:;mt;ut LaudfHl 􀁦􀁾􀀷􀀧􀀺􀀺􀀺􀀺􀁕􀀠5-1)<121 i600A Rllilr;"c St, Lewis\'i!le, T': 􀁾􀀵􀀱􀁊􀀶􀀢􀀠Contact 􀁐􀁾􀁲􀁳􀁯􀁮􀀺􀀠10. Facility 10 Number I02.:...:n f), 􀂷􀁜􀀮􀀺􀁖􀁨􀀱􀁴􀁾􀁨􀁂􀁮􀁤􀀠11. Waste Description (including Proper Class, and ID) 12. Containers 13. TolalQuantity 14. Unit 15. WasteCode a. "-::n 'I 􀀧􀀧􀀧􀀧􀁮􀁭􀁾􀁈􀀬􀀭􀀺􀁩􀀺􀁮􀁾􀀠\ 􀁮􀀻􀁲􀁾􀀠·,dr-if 􀁦􀀮􀁉􀀧􀀿􀀺􀀭􀀻􀀧􀁴􀁲􀁨􀀱􀀱􀁩􀁾􀀠/.::yei., b. G. Additional Description for Materials Listed AIlove 􀀺􀁾􀁮􀁎􀁆􀀠16. Special Handling InSlructionsandAdditlonallnformation N()hlF GENERATOR'S.CERTIFICATION: I ho",by decla'" the conlents 01 this consignment are fully and accurately descnbed above by.hlpping name and are classified, packed, marked, and labeled, and are in all respecl in proper condition for transport by highway according 10 applicable federal and state regulations. . , .. .. ,," . t·., ". , " --,. . ''T,t7'ir-.,n I 􀁾􀁾􀀮􀁦.,. • ..1 􀁾􀀮􀀺􀀧􀁽􀁳􀀮􀁾􀁲􀁮􀀠1 􀁐􀁲􀁩􀁮􀁴􀁡􀁤􀁦􀁔􀁹􀁰􀁥􀁤􀁎􀁡􀁭􀁾􀀠• , "'c t;, .. . .. ! 􀁓􀁩􀀹􀁾􀀭􀁲􀀠1!21eJb17. T-..A.-t P • ...,-,....... ,;",1' l'''4,.I... ,-;-!oTn,-u 􀁾􀀺􀀢􀁌􀀬􀀠!/Zr:;;,l I( . . 18. Transportor 􀁾•.􀁾􀁫􀁮􀁯􀁷􀁬􀁥􀁤􀁧􀁥􀀧􀀹􀁅􀁩􀁮􀁬􀁯􀁦Receipl of Materials 􀁾􀀺􀁥􀀯􀀱􀀠) Date i PrintedfT . if /' ///'" -􀀮􀁾􀀷􀀧􀀢􀀠􀀧􀀯􀁾􀁾􀀠/4..--J'. L.., do 19. Transporter2 Acknowledgeme'nt of Receipt of Materials I Sigoi.1ui., Dele PrintedlTyped Name V 20. Discrepancy Indication Space .' 21. Facility Owner/Operator. CertificatIon of receipt of 􀁰􀁥􀁴􀁲􀁯􀁬􀁥􀁬􀁬􀁭􀁾􀁳􀁵􀁢􀁳􀁴􀁡􀁮􀁣􀁥􀀠wastes covered by this manifest except as noted in Item 20. PrintedfTyped Name Signature Date 􀁔􀁎􀁒􀁃􀁾(05-()5-94) . . ..While -Originaf Yellow -STFacihty Pink -Transporter Green -Generator's first copy I rlG Gtr TEXAS NATURAL RESOURCE CONSERVATION COMMISSION PETROLEUM STORAGE TANK DIVISION CORRESPONDENCE IDENTIFICATION SHEET Date; Site Name: 􀁾􀀱􀀲􀁮􀁾􀁲􀁯􀁾􀁉􀁾􀁾􀁾􀁾________􀁌􀁐􀁓􀁔􀁉􀁄􀁎􀁾􀁏􀀮􀁾􀀺� �􀁾􀁾􀁾􀁾􀀽􀀽􀀽􀀽􀀽􀀽􀁾􀀠􀁅􀁸􀁾􀁸􀀢􀀬􀁯􀀢􀀬􀁮􀀭􀀢􀁒􀀯􀁓􀀢􀀢􀀺􀀢􀀬􀀶􀀭􀀢􀀬􀀰􀀲􀀬􀀬􀀬􀀭􀀷􀀬􀀭􀀬􀀵􀀬􀀭_____Facility ID N Site Address: 4191 Beltline Road Addison (Dallas, County), Texas This checklist must accompany all correspondence submitted to the RPR Section and should be affixed to the front ofyour submittal as a cover page. Please check the appropriate box for the type ofcorrespondence which you have submitted to the RPR Section. Check all boxes that apply if you are submitting more than one type ofcorrespondence. If you cannot find an appropriate category, please complete the "other" section. 0 Initial Abatement (1) 0 Tank Removal (2) 0 Excavation (3) 0 Waste Treatment (4) 0 Site Assessment (5) 0 Aquifer Testing (6) 0 VESISparge Testing (7) 0 Qtrly. GW Monitoring (S) 0 CAfe' Prep. (9) 0 GW Extracffreatment ((10) 0 Soil Vapor Extrac. (ll) 0 Operation & Main. (12) 0 Site Closure (13) 0 Plan A Risk Ass. (14) 0 Plan B Risk Ass. (15) 0 Semi-annual GW Mon. (16)* 0 Annual GW Mon. (1S) 0 Product Recovery (19) 0 Other proposal Assessment Product Recovery Report Form (TNRCC-0016) • Release Report Form (TNRCC-0621) [] Site Closure Request Form (TNRCC-002S) C Monitoring Event Summary and Status Report (TNRCC-0013) o Final Site Closure Report Form (TNRCC-0038 o Priority 4 LPST Case Closure Request Form (TNRCC-0461) o Other o O&MlPerformance Mon. 0 Plan B Risk Assessment 0 CAP InstaliationlModification o Property DivestiturelPhase I ESA 0 Corrective Action Plan (CAP) 0 AquiferlPilot Test Results o Off-site access assistance o Deadline Extension Request o Tank tightness test results o Request for State-Lead o Request for LPST Waste Code o Class V Reinjection Request o Notice to Owner/Operator for CAS Services o Petroleum-Substance Waste Manifest o Notice of Continuation of Groundwater Monitoring o Underground Storage Tank Registration Form o Notice of Continuation of Operation and Maintenance 0 Aboveground Storage Tank Registration Form o Other (anything that does not fit into one of the categories above) and report been'* monitoring, use Proposal Activity 16. I altest that all work has been conducted in accordance with accepted industry standards/practices and adhered to TNRCC guidance and rules. I certify that I am aware that misrepresentation of any of the above claims is a violation of 30 TAC 33.4453(b)(1)(E) and that this violation may result in the disciplinary actions set forth in 30TAC 334.4:53 and or 334.463 and 334.465. If aproposal is anached for preapproval, has the proposed work, in part or in whole, already been perfonned or in progress? 0 Yes 0 No If yes, what wv'''''._______________ (Date) I ( (972) 484-1420 (Telephone #) (972) 247-7220 (FAX#) Todd Frazee (Projex;, Manager) 01237 (CAPM !!«::r; 0 II :::E I I I i i \ I \J LEGENO '" -MONITOR WELL K -COMPOSITE SAMPLE 1.llCA110N IP!IIlJ&'T NO. EXXON 6-027550902.75 4191 BELT LINE ROADIf1GIJRE AIIIlISON, TEXASI ;5 M ;c 􀁾􀀠SITE MAP ILLUSTRATING COMPOSITE SOIL SAMPLES COLLECTED DURING TANK REMOVAL ACTII/ITES I TABLEl Analytical Results Showing Hydrocarbon Concentrations in Soil Samples Collected During UST Removal Activities Exxon 6-0275 4191 Bell Line Road Addison, Texas Sample ID Sample Location I Depth (ft) Date Benzene (ugIKg) 8020 Tolune (ugIKg) 8020 Ethytbenzene (ugIKg) 8020 Tala! Xylenes (ugIKg) 8020 Tolal BTEX (ug/Kg) 8020 TPH C6-C12 Range (mg/Kg) 1005 TPH >C12-C28 Range (rnglKg) 1005 TPH C2S-C-35 Range (mg/Kg) 1005 TPH C6-C35 Range (mgIKg) 1005 Total PAH (ugIKg) 8310 North Wall North Wal1I6 10126101 NO NO NO NO BOL NO NO NO NO NO East Walt East Wal1I6 10l26I01 NO 1.9 NO 4.0 5,9 NO NO NO NT NT South Wall South Wall 16 t0126/Oi NO NO NO 1.5 1.5 NO NO NO NT NT West Wall West WaH 16 10l26I01 NO NO 6 5.9 11.9 NO ND NO NT NT Tank Bottom N_ 8ottom North (Diesel) UST I 12 10126/01 NO NO 2.3 8 10.3 NO NO NO NO 24.8 BortomN Middle Bottom North Middle UST 112 10l26I01 9.9 16 9.6 􀀴􀁾􀀠80.5 NO ND NO NT NT BottomS Middle Bottorn South Middle UST 112 10126/01 5.9 11 IS 56 87.9 NO NO NO ND NT Bottom South Bottom South USTIl2 10126101 13 37 3.8 14.8 68.6 NO NO NO NT NT , LT-IN_ Product Line Trench 1112101 NO NO 10 I 11 NO NO NO NT NT LT-2N_ Product Line Trench 1112101 NO NO NO ND NO NO NO NO NT NT LT-3-Soutb ProdUCt Line Trench 1112101 1.2 NO 15 10.6 26.8 NO NO NO NT NT MiddleDl-East Dispenser IsJand 11/2/01 NO NO NO NO NO NO NO NO NT NT South DIW"" Dispenset Island 1112101 1.8 2.6 5.3 2-5 12.2 ND NO NO NT NT LT-I·Soutl Product Line Trench l1/1!/O1 130 1000 380 1880 3390 120 72 NO 192 NT LT*2·SouW T·3-Nortll Product Line Trench 1I11!/01 NO 500 190 8S0 1570 NO NO NO NT NT LProductUne Trench 11/8/01 210 2600 2100 8700 13610 390 380 NO 770 NT ND=Not Detecled NT= Not Tested BDL=Below Detection Limits TABLEl AnalyticaJ Results Showing Hydrocarbon Concentrations in Soil Samples Collected During UST Removal Activities Exxon 6-0275 4191 Belt Line Road Addison, Texas Sample SampieID Location I Depth (ft) LT4Nonl Product Line Trench LT-5 Product Line Trench LT·6 Product Line Trench LT·7 ProduCl Line Trench 􀁹􀁡􀁰􀁯􀁲􀁌􀁔􀁾􀀠Vapor Line North Trench NE·OI Dispenser Island NW-OI Dispenser Island MiddleDl-Dispenser West Island Dlcsel Dl Dispenser Island SE-DJ Dispenser Island NW·OI Dispenser Island Sp-I SoH Pile Sp-2 Soil Pile Sp-3 Soil Pile Sp-4 Soil Pile 51'"5 Soil Pile Sp-6 Soil Pile TPH Ethyl· To!3l To!3l C6·CI2 Date Benzene Tolune benzene Xylenes BTEX Range (ug/Kg) (ug/Kg) M/Kg) (uglKg) (ug/Kg) (mglKg) 8020 8020 8020 8020 8020 1005 1118101 NO NO 40 NO 40 NO lIf81!ll NO 220 250 16GO 2130 NO ll/8IQI 5.5 NO NO NO 5.5 NO II/8IQI NO NO NO NO NO NO 11/8/01 NO 15 2.7 10.3 \4.5 NO 11I8IQ1 NO NO NO NO NO NO lIf81!ll NO NO \6()0 6200 7800 330 llf8l!ll 230 2800 1500 6200 10730 230 11/81QJ NO 180 110 490 780 NO 1118101 160 1400 720 2850 5130 NO 1118101 NO NO 16()O 6200 7800 330 lIf81!ll NO GO 40 lSI 281 NO llI8IQI NO NO NO 6.1 6.1 56 1118101 NO NO NO NO NO NO 11l8IQJ NO NO NO 3.8 3.8 NO lIf81!ll NO 17 NO 47 64 NO 1lI8101 NO NO NO 114 114 NO TPH TPH >CIZ'(:28 C2S·C·35 Range Range (mg/Kg) (mg/Kg) 1005 1005 NO NO NO NO NO NO NO NO NO NO NO NO 160 NO 550 NO NO NO NO NO IGO NO NO NO 51 NO NO NO 130 NO 190 NO 79 NO Native Soil PAR results: Bottom North UST "" 0,0088 mglKg fluorene, 0.016 mg/Kg Naphthalene, Middle DI West;;:; 0.030 mg/Kg Aeenaphtbene, 0.960 mgIKg Fluorene. 1.200 mglKgNaphthalene.. TPH C6'(:35 Th!3l Range PAH (mgIKg) lug/Kg) 1005 8310 NO NO NO NT NO NT NO NT NO NT NO NT 490 NT 780 i 2,240 NO I NT , NO Nt 490 NT NO NT 107 NT NO NT 130 NT 190 NT 79 NT ND=NOI Detecled NT= Not Tested BDL=Below Delection Limits EA Engineering, Science, and Techllology APPENDICES/SUPPORTING DATA F:'lPro)\Exxon\sdfl6·02751Reports'VEA Tallk Excavation Report EA Engineer1i,g, Science, and Technology APPENDICES/SUPPORTING DATA APPENDIX A -TNRCC Correspondence APPENDIX B -Analytical Results APPENDIX C -Waste Profile and Disposal Documentation APPENDIX D -Photographic Documentation APPENDIX E -Release Detennination Report Form F:V'roj\Exxonlsdf\6-0275\ReportATEA Tank Excavation Report EA Engineering, Science, and Technology APPENDIX A TNRCC Correspondence F:\Pro}\Erxon\sdtVi-02751Reports\TEA Tank Excavation Report Robert}, Huston, Chairman R. B. "Ralph" Marquez, Commissioner John M. Baker, Commissioner Jeffrey A, Saitas, Executive Director TEXAS NATURAL RESOURCE CONSERVATION COMMISSION PrOleding Texas by Reducing and Preventing Pollution October II, 2001 MRDALEGOMM EXXON CO USA PO BX 4552 ROOM KT· 1270 HOUSTON TX 77210 Re: UST/AST removal at EXXON RiS #6-OZ75, 4191 BELTLINE RD, ,4J)DISON, TX: Activity 􀁳􀁾􀁨􀁥􀁤􀁵􀁪􀁥􀁤􀀠on 1110512001; TNRCC UST Facility No, 0026232; Notification received by TNRCC on 10/0912001. DEAR MR GOMM: This leiter acknowledges receipt by the Texas Natural Resource Conservation Commission (TNRCC) ofnotification for the referenced underground storage tank (UST) conslJUction activity, as required by 30 TAC §334,6. ' This letter does not constitute an official approval, permit or endorsement for the referenced activity or for any associated construction methods or equipment. A copy ofyour notification has been sent to the TNRCC regional office indicated below, The time and scope of this activity must be confirmed with the regional UST personnel 24 to 72 hours before the activity in order to arrange an inspection. Any rescheduling of the proposed construction must be cnordinated andlor appr.oved by authorized regional personnel Techmca! requirements which apply to variousVST 􀁣􀀨􀀩􀁮􀁳􀁮􀁬􀁬􀁣􀁾􀁩􀀨􀀩􀁾􀀠ac,iviti", are included in 30 TAC §334, Subchapter C. Also, alrUSl' installations, repairs; and removals must 'be 􀁣􀁾􀁮􀁤􀁵􀁣􀁴􀁥􀁤􀀠l:!y a registered UST conttactor wbo bas a licensed installer or on-site supervisor at the sit. during all critical .innctur••, as required by 30 TAC Chapter 334, Subchapter r. T.t,is leiter also serves as a temporary delivery certificate to allow initial deliveries into any new or replacement UST system. This temporary delivery certificate is valid/or no more than 90 days aj/er theftrst delivery a/regulatedsubstances into the new or replacement UST system, aj/er which a permanent TNRCC·issued delivery certificate must be posted or available at the [1ST/acility. Upon completion ofconstruction, the attached UST Registration and Self-Certification form must be completed and returned to the referenced address on the form. For further assistance, please contact the PST Registration Team, at (512)239-200 I. or the TNRCC regionai UST personnei indicated below, Sincerely, Donna Lancaster Registration Coordinator Regis!ration!,Review, and Reporting Division 􀁅􀁾􀁣􀁬􀁯􀁳􀁊􀁲􀁥􀀮􀀺􀀻􀀢􀁦􀁎􀁒􀁃􀁃􀀠UST Registration'& 􀁓􀁥􀁬􀁦􀀭􀁃􀁥􀁲􀁴􀁩􀁦􀁩􀁇􀁡􀁴􀁩􀁾􀁮􀀠Form· . i ' '. c 􀁾􀀮􀁾􀀬􀀠, • ¥o l0090Q3/1ate Regional Representative: Region 4, PST Team, (817)469-6750. P.O. Box 13087 • Austin, Texas 78711-3087 • 5121239-1000 • Internet address: www.tnrcc.state.tx.us printe4 0(1 􀁲􀁾􀁣􀁬􀁤􀁥􀁤􀀠paper ill!n:;! 􀁪􀁑􀁹􀂷􀁢􀁡􀁾􀁾􀁤􀀠in k FACSIMILE MESSAGE EA Engineering. Science. and Technology South Central Operations 1420 Valwood Parkway. Suite 170 Carrollton. Texas 75006 Telephone: 214-484-1420 FAX: 214-247-7220 PLEASE DEUVER TO: Name: Lonnie Gilley Company/Department: TNRCC Region 4 Phone: (817) 469-6750 FAX: (817) 588-5703 If you do not receive all pages clearly. call as soon as possible. SENTBY: Name: Mark Lach. For Todd Frazee Transmitting from: (972) 247-7220 Number of Pages 􀁾􀁮􀁣􀁬􀁵􀁤􀁩􀁮􀁧􀀠Transmittal Sheet): 1 Date: October 25, 2001 Time: 9:05 Project Code: 6-0275 MESSAGE: On behalf of ExxonMobil Corporation. EA is submitting notification that (1) 6,000 gallon fiberglass Underground Storage Tank and (3) 10,000 gallon fiberglass Underground Storage Tanks will be removed at Exxon 6-0275.4191 Belt Une Road. Addison, Texas. The UST removal is scheduled to take place at 12:00 PM lfI ctober 26. 2001. This is the site we talked about last weel< that is less than the 30 days from the submission of the day notice. If you have any questions, please feel free to call Todd Frazee or me at (972) 484-1420. Thanks. ORIGINAL Wlll: 0 FOLLOW VIA MAIL 0 FOLLOW VIA OVERNIGlIT EXPRESS 0 FOLLOW VIA MODEM YNOT FOLLOW SAlTiMOREliNEW YORKIISAN FRANCISCOIlUNCOLMlNEWARK!lCHICAGOIlA1lANTAilDAlLASIILOS ANGEt.ES1lcHAm.OTTEI'.l'NASHINGTON,DC UBOSTONDWEST PALM SEACHUSEATTLE EA Engineering, Science, and Technology APPENDIXB Analytical Results F:\Prollli;o:on\sdtVi-02751Reports\TEA Tank Excavation Report HOUSTON LABORATORY 8880 INTERCHANGE OAIVE HOUSTON, TEXAS 77054 (713) G&CJ.Os01 ExxonMobil RECEIVED Certificate of Analysis Number: NOV 0 5 2001 01101137 Report To: EA Engineering Mark Lach 1420 Valwood Parkway Suite 170 Carrollton TJ( 75006· ph: (972) 484·1420 lax; Project Name: 4191 Beltline Addison. TX Site: 6·0275,21044625 Site Address: PO Number: LWR1I21044S07 State: Texas State cart. No.: Date Reported: 1111101 This Report Contains A Total Of 18 Pages Excluding This Page And Chain Of Custody 1111101 Date I HOUSTON LABORATORY 8880 INTERCHANGE ORIVE HOUSTON. TX 77054 (713)000-0901 Case Narrative for: ExxonMobii Certificate of Analysis Number: 01101137 Report To: EA Engineering Mark Lach 1420 Valwood Parkway SuU.170 Carrollton TX 75006ph: (972) 484-1420 fax: Project Name: 4191 Beilline Addison, TX Sile: 6-0275,21044625 Site Address: PO Number: LWRII21044901 State: Texas State Cor!. No,: Date Reported: 1111101 Matnx spike (MS) and malrix spike duplicate (MSO) samples are chosen and tested al random from an analytical batch 01 'like' matrix to check tor possible matrix effect The MS and MSD will provide site specific matrix data only for those samples which are spiked by the laboratory. Since the MS and MSD are chosen at random from an analytical batch, the sample chosen for spike purposes mayor may not have been a sample submitted in this sampJe delivery group. The validity of Ihe anaifytical procedures for which data IS reported in this analytical report is determined by the Laboralory Control Sample (LCS) and and the Method Blank (MB). The Laboratory Control Sample (LCS) and the Method Blank (MB) are processed with the samples and the MSIMSD to ensure method criteria are achieved throughout the entire analytical process. Any other exceptions associated with this report will be lootnated In the analytical result pagels) or the quality control summary pagels). Please do not hesitate to contact us if you have any questions or comments pertaining to this data report. Please reference the above Certificate of Analysis Number. This report shall not be reproduced except in full. without the written approval of the laboratory. The reported results are only representative of the samples submitted for testing, SPL, Inc. is pleased to be of service to you. We antIcipate working with you in fuHifling all your current and future analytical needs. /SoniaWesi Senior Project Manager 01101131 Page 1 Oate 11/1/01 HOUSTON LABOFIATOFlY 8880 INTEFICHANGE DFlIVE HOUSTON, TX 77054 (713) 000-0901 ExxonMobii 􀁾􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭Certificate of Analysis Number: 01101137 RegortTo: EA Engineering Proiect Name: 4191 Beltllne Addison, TX Mark Lach 1420 Valwood Parkway Suite 170 Site: Sile Address: 6-ll275,21 044625 Carrollton TX PO Number: LWFl1l21044807 75006ph: (972) 484-1420 fax: (972) 247-7220 Slale: SID!!! !CI2-C28 ND 50 10131101 8:40 AM 886031 􀁔􀁾􀁐􀁾􀁈􀁾􀁔􀁾􀁅􀁘􀁾􀁁􀁾􀁓􀁾􀀱􀀰􀀰􀀵􀁾____________􀁾􀁾______􀁾__􀁾􀁍􀁾􀁃􀁾􀁬􀁾􀁾􀁔􀁎􀁾􀁒􀁾􀁃􀁾􀁃􀁾􀀱􀀰􀁾􀀰􀀵__􀁾􀁾􀁾􀁾􀁾􀁾__􀁾􀁾􀁾􀀠>C 28·C35 ND 50 10131101 8:40 AM 886031 􀁾􀁾􀁾􀁾􀀠􀁾􀀠50 1 10131101 8:40 AM 886031 􀁳􀁵􀁲􀁲􀀺􀁬􀀭􀁃􀁨􀁾􀁬􀁯􀁲􀁯􀁾􀁯􀁯􀁾􀁴􀁡􀁾􀁮􀁾􀀮􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀱􀁾􀀰􀁾􀀱􀀭􀀭􀁾􀀥􀁾􀁾􀀷􀀰􀁾􀀭􀁾􀁉􀀳􀀰􀁾􀀭􀀭� �􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀱􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀁾􀁾􀁾􀁾􀀷􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀁾10131101 8:40 AM 886031 10131101 8:40 AM 886031SUrr: 􀁯􀀮􀁔􀀮􀁲􀁰􀁾􀀬􀀺􀀺􀀺􀁥􀁮􀀺􀀮􀀺􀀡􀁹􀁩􀁣􀀺􀀮􀀭___________---.:9=2.=8_.:%=-.::7o -::..:.:130:::::.._______----,1,-____..:.:==..::.::::::....:..::::.-____...:::::::::::.: Prep Method Prep Date TNRCC 1006 101301200113:57 Sonia West Project Manager Qualifiers; NDIU -Not Detected at the Reporting Umi! >MCL -Result Over Maximum Contamination Limit(MCL) B -Analyie detected in the assooiated Method Blank D -Surrogate Reoovery Unreporteble due to Dilution • -Surrogate Recovery Ou1llide Advisable QC Umits MI -Matrix Interference J -Estimated Value between MDL and POL 01101137 Page 3 HI1I013;11:46PM HOUSTON LABORATORY 888() INTERCHANGE DRIVE 􀁧􀁾􀀷􀀠HOUSTON. TX 77054 (713) 88G-0901 Client Sample ID E. Wall Collected: 10126101 1 :40:00 SPl Sample ID: 01101137-02 Site: 6-0275,21044625 AnalyseslMethod Result Rep.Limit 011. Factor QUAL Date Analyzed Analyst Seq. II PURGEABlE AROMATICS MCl SW8021 􀁅􀁌􀁾􀁾􀁕􀁲􀁬􀁩􀁴􀁳􀀺􀀠ugiKg Benzene ND 1 10131/0117:32 TM 887866 Ethylbenzene ND 1 1 10/3110117:32 TM 887866 Toluene 1.9 1 1 1013110117:32 TM 887866 Xylene.,Totai 4 1 1 1013110117;32 TM 887866 Surr: 1,4-DiHuombenzene 111 % 59-127 1013110117:32 TM 887866 Surr: 4-Bromofluorobenzene 109 % 48-156 10131101 17:32 TM 887866 TPH TEXAS 1005 MCl TNRCC1005 Units: mg/Kg C6-C12 ND 50 10130101 17:31 AM 885997 >C12-C28 ND 50 10I30I01 17:31 AM 885997 >C28-C35 ND 50 10l50I01 17;31 AM 885997 Total TPH (C6-C35) NO 50 10130101 17;31 AM 885997 Su"" 1-Chlorooctana 94_1 % 70-130 10100101 17:31 AM 885997 SUIT: Q-Terpheny1 83.0 % 70-130 10130101 17;31 AM 885997 􀁾􀁾􀁾􀁨􀁤􀀻􀀻􀁌􀀺􀀺􀀻􀀻􀀻􀀺􀀠SeniaWest ----------------------􀁐􀁲􀁾􀁦􀁾􀁣􀁴􀀠􀀠Manager QualUiers: NDiU -Not Detected at the Reporting Limit >MCL -Re.ult Over Maximum Contamination Llmit(MCL) B -Analyle detected in the associated Method Blank D -Surrogate Recovery Unreportable due to Dilution '* -Surrogate Recovery Outside Advisable QC limits MI -Malrix Interlerence J -Estimated Value between MDL and POL 01101137 Page 4 1111/01 3:11:47 PM HOUSTON LABORATORY BBBD INTERCHANGE DRIVE HOUSTON, TX 77054 􀁾􀁾􀀷􀀠(713) 660-0901 Client Sample ID S. Wall Collected: 10126101 2:05:00 SPL Sample 10: 01101137-03 Site: 6-0275,21044625 Analyses/Method Result Rep.Limlt 011. Factor QUAL Date Analyzed Analyst Seq. II PURGEABLE AROMATICS MCL SW8021B Units: uglKg Benzene NO 10130101 19:27 TM 886262 Ethylbenzene NO 10130101 19:27 TM 886262 Toluene ND 1 10/30/0119:27 TM 886262 Xyl.e.n•••Total 1.5 1 10/30101 19:27 TM 886262 Surr: 1.4-DjfJuorobenzene 105 0/0 59-127 10130101 19:27 TM 886262 Surr: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀁬􀁵􀁯􀁲􀁯� �􀁥􀁮􀁺􀁥􀁮􀁥􀀠119 0/0 48-156 1 1013010119:27 TM 886262 TPHTEXAS 1005 C6-C12 ND 50 MCL TNRCC1005 Units: mwKg 10131/01 8:51 AM 886032 >C12-C28 ND 50 10131/01 8:51 AM 886032 >C28-C35 ..__....-Iotal TPH (CB-C35) Surr: 1-Chlorooctane NO ND 94.2 0/0 50 50 70-130 1 10131101 8:51 10131/01 8:51 10/31/01 8:51 AM AM AM 866032 886032 886032 Surr: o·Terpl1enyl 80.4 0/0 70-130 10131101 8:51 AM 886032 Prep Method Prep Date :TNRCC 1005 10I30I3001 13:57 Sonia West West QuaJifiers: NDIU -Not Detected at the Reporting limit "MCL -Result Over Maximum Contamination Limlt(MCL) B -Analyle detected in the associated Method Blank D -Surrogate Recovery Unmportable due to Dilution • -Surrogate Recovery Outside Advisable QC limits MI -Matrix Interference J -Estimated Value between MDL and POL 01101137 Page 5 11/1/01 3:11:47 PM HOUSTON LABORATORY 88ao INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 ClienlSamplelD W. Wall Collected: 10/261011:35:00 SPL Sample ID: 01101137-04 􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭� �􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭Site: 6-0275,21044625 Analyses/Method Result Rep.Limit Oil. Factor aUAL Date Analyzed Analyst Seq. # PURGEABLE AROMATICS MCl swa021B Unils: uglK!I Benzene ND 1 10130101 19:57 TM 886263 􀁅􀁾􀁢􀁥􀁮􀀬􀁥􀁮􀁥􀀠6 1 10l30I01 19:57 TM 886263 Toluene ND 1013010119:57 TM 886263 􀁾􀁾􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀽􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀮􀀭􀀭􀀭 􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾Xylenes,Tata! 5.9 1 1013010119:57 TM 886263 Surr.l,4-Dlffuorobenzene 103 % 59-127 10/3010119:57 TM 886263 SUIT: 4-Bromoftuorobenzene 20B MI % 48-156 10l30I01 19:57 TM 886263 TNRCC 1005MClTPHTEXA_S_1_0_05____________􀁾􀁾􀀭􀀭􀀭􀀭􀁾􀀽􀁟􀀭􀀭􀁾􀁾􀀭􀀭􀁾􀁾􀁾􀁾􀀮􀀠...___Units: mglKg C6·C12 ND 50 10/31/01 9:02 AM 88B033 >C12-G28 ND 50 10131101 9:02 AM 886033 >C2B-C35 ND 50 1 10131101 9:02 AM 886033 Total TPH (C6.c35) ND 50 1 1 10131101 9;02 AM 886033 Surr: 􀀱􀁾􀁃􀁨􀀡􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀁥􀀠95.0 % 70·130 10131101 9;02 AM 886033 Surr. 0-Terphenyl 79.9 '1'. 70·130 10/31101 9:02 AM BBB033 Prep Method Prep Date Prep Initials TNRCC 1005 10l30l200113:57 J F 􀁾􀁾&LdMCL -Resull Over Maximum Contamination LImit(MCL) B -Analyte detected In the associated Method Blank D 􀁾􀀠Surrogate Recovery Unreportable due to DlIution • -Surrogate Recovery OUtside Advisable OC Limits MI • Matrix Interference J -Estimated Value between MDL and POL 01101137 Page 6 11/1/013:11:48PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 􀁾􀁾􀀷􀀠(713) 660-0901 Client Sample ID Tank Boltom North Collected: 10126101 1:45:00 SPL Sample ID: 01101137-05 Site: 6-0275,21044625 AnalyseslMethod Result Rep.Urni! Dil. Faclor QUAL Date Analyzed Analyst Seq. # -------_....._-----􀀭􀀭􀀭􀀭􀀭􀀭􀁾....------POLYNUCLEAR AROMATIC HYDROCARBONS MCL SW831 0 Units: ug!Kg Acenaphthene NO 3,3 10130101 19:11 YN 886022 Acenaphlhylene NO 3,3 10130101 19:11 YN 888022 Anthracene NO 3_3 1013010119:11 YN 886022 Benz(a)anlhracene NO 3,3 1013010119:11 YN 886022 Benzo(a)pyrene NO 3.3 10130101 19:11 YN 886022 Benzo(b)fluoranthena NO 3.3 1 10130101 19:11 YN 886022 Benzo(g,h,i)pe'Ylena NO 3.3 1 10I30I01 19:11 YN 888022 Benzo(k)ftuoranthene NO 3,3 1 101301()1 19:11 YN 888022 ChJys8ne NO 3.3 1013010119:11 YN 886022 Oibenzo(a,h)anthracene NO 3.3 1 10130101 19:11 YN 888022 Fluoranthene NO 3.3 1 10130101 19:11 YN 886022 Rumens 8.8 3.3 1 1013010119:11 YN 886022 Indano(l,2,3-cd)pyrene NO 3.3 1 1013010119:11 YN 886022 Naphthalene 16 3.3 1 10130/0119:11 YN 888022 Phenanthrene NO 3,3 10130101 19:11 YN 886022 Pyrene NO 3,3 1013010119:11 YN 886022 Surr: 1*Fluoronaphthalene 52,0 % 41-97 10130101 19:11 YN 888022 SUrf: Phenenthran ..dl0 75,7 % 38·108 10130101 19:11 YN 888022 Benzene 1 Ethylbenzene 2,3 1 10130101 20:27 TM 886264 Toluene NO 1 1 10130101 20:27 TM 886264 􀁘􀁙􀁬􀁥􀁮􀁥􀁳􀀬􀁾􀁯􀁴􀁡􀁬􀀠8· 1 1 10130101 20:27 TM 886264 Surr: 1,4-Difluorobenzene 111 % 59-127 10/30101 20:27 TM 886264 Surf: 4-Bromoftuorobenzene 117 % 48-158 10130101 20:27 TM 886264 TPH TEXAS 1005 MCL TNRCC 1005 Units: mg!Kg C6-C12 NO 50 10130101 18:03 AM 888000 >CI2-C28 NO 50 10130101 18:03 AM 886000 >C28-C36 NO 50 1 10130101 18:03 AM 886000 Tolal 􀁔􀀻􀀧􀁰􀀰􀁈􀁾􀀨􀀻􀀻􀀻􀁃􀀶􀀻􀁏􀀭􀀮􀀭􀀻􀁏􀀺􀁃􀀳􀀻􀀻􀀰􀀵􀀩􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁎􀀧􀀻􀀺􀀻􀁏􀀭􀀭􀀭􀀭􀀭􀀻􀀺􀀻􀀵􀀰􀁾􀀭􀀭􀀭􀀭􀀭􀁾􀀱􀀭􀀭􀀭􀀭􀁾􀁾􀀺􀀺􀀺􀀧􀀺􀀭􀀺􀀺􀁾􀀧􀀻􀀭􀀭􀀧􀀺􀀺􀀷􀁩􀀭􀀭􀀭􀀭􀀺� �􀀽􀀽1013010118:03 AM 886000 Surr: 1-ChlorOOctane 88,4 % 70-130 10I30I01 18:03 AM 888000 Surr: o-Terphenyl 73.S % 70-130 10130101 18:03 AM 888000 Sonja West Project Manager Gualifiers: NOIU • Not Detected at the Reporting limit >MCL -Result Over MaxImum Contamination limit(MCL) B -Analyle detected in the associated Method Blank o -Surrogate Recove'Y Unraportable due to Dilution '" -Surrogate Recovery Outside AdVisable QC Limits MI -Matrix Interference J Estimated Vatue between MOL and POL Ot 101137 Page 7 11/1/Q1 3:11:43 PM 886264 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660'()901 Client Sample ID Tank Bottom North Middle Collected: 10126101 2:20:00 SPl Sample ID: 01101137·06 Site: 6·0275,21044625 AnalyseslMethod Result Rep.Limit Oil. Factor QUAL Date Analyzed Analyst Seq. # Units: uglKg ... 10180101 20:58 TM 886266 Ethylbenzene 9.6 10130101 20:58 TM 886266 Toluene 16 10130101 20:58 TM 886265 Xylene',Total 45 10180/01 20:58 TM 886265 Surr: 1.4-0ifluorobenzene 120 % 59-127 1013001 20:58 TM 886265 PURGEABlE AROMATICS Benzene 9.9 Surr: 4·Bromofluorobenzene 118 % 48-156 10130/01 20:58 TM 886266 TPH TEXAS 1005 C6-C12 >C12·C28 NO NO 50 50 MCl TNRCC 1005 1 1 Units'J!IlIIKg 10130/01 18:14 AM 10130101 18;14 AM 886001 886001 >C28-C35 NO 50 1 1018010118:14 AM 886001 Total TPH (C6-G35) Surr. 1..chlorooctane NO 91.5 % 50 70-130 10180/0118:14 10130101 18:14 AM AM S86oo1 886001 Surr,.o-Terphenyi 72.3 % 70·130 10/3010118:14 AM 886001 PreR Method iPreQ Date PreQ Initials TNRCC 1005 1013012001 13:57 􀁾􀁾U2.t!:d:;C::::;_______________ Sonia West Project Manager Qualifiers: NOIU • Not Datected at the Reporting Umit >MCL -Result Over Maximum 􀁃􀁯􀁮􀁴􀁡􀁭􀁩􀁮􀁡􀁾􀁯􀁮􀀠Umit(MCL) 8 -Aralyte detected in the assooiated Method Blank o -Surrogate Recovery Unreportable due to Dilution '" -Surrogate Recovery Outside Advisable QC Limits MI • Matrix Interference J -Estimated Value between MOL and POL 01101137 Page 8 11/11013.:11:49 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 66G-0901 Client Sample ID Tank Bottom South Middle Collected: 10/261012:10:00 SPL Sample 10: 01101137·07 Site: 6-0215,21044625 Analyses/Method Result Rep.Llmit Oil. Factor QUAL Date Analyzed Analyst Seq. II PURGEABLE AROMATICS MCL swa021B Units: uglKg Benzene 5.9 10130101 21:28 TM aa8286 Ethylbenzene Toluene Xyienes,ToIal Sun: 1,4·0ifluorobenzene Surr: 4-Bromofluorobenzene 15 11 56 114 116 % % 1 59·127 48·156 1 1 10130101 21 :28 10/30101 21:28 10130101 21 :28 10/30101 21 :28 10130101 21 :28 TM TM TM TM TM 886286 aa6266 886266 8aa266 aa6286 TPH TEXAS 1005 C6-C12 NO 50 MCL TNRCC 1005 Units: mgiKg 10130101 18:24 AM 886002 >C12·C28 NO 50 10130101 18:24 AM 886002 ND 50 1013010118:24 AM 886002 Total TPH (C6·C35) NO 50 10130101 18:24 AM 886002 SUIT: 􀀱􀁾􀁃􀁨􀁬􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀁥􀀠88.6 % 70·130 10130101 18:24 AM 8BB002 SUrT: 0-TeMCL· Result Over Maximum Contamination Limit(MCL) B • Analyle detected in the associated Method Blank D • SUrrogate Recovery Unreportable due 10 Dilution •• Surrogate Recov..y Outside Advisable OC Limits MI 􀁾􀀠Matrix Interference J • Estimated Value between MDL and POL 01101137 Page 9 11/11013:11:00 PM HOUSTON LABOAATOAY 8800 INTEACHANGE DRIVE HOUSTON, TJ( 77054 􀁾􀁾􀀷􀀠(713) 66G-0901 Client Sample 10 Tank Bottom South Collected: 10126/01 2:00:00 SPl Sample 10: 01101137·08 Site: 6-0275,21044625 AnalyseslMethod Aesult Rep.Limit Dil. Faclor QUAL Dale Analyzed Analyst Seq.# PURGEABlE AROMATICS ... Benzene 13 Mel SW8021B Units: uglKI! 10/30/01 9:59 TM 886267 Ethylbenzene Toluene 3.8 37 1 1 10/30/01 9:59 10/30/01 9:59 TM TM 886267 886267 Xylenes,Total ....􀁾....-----Surr: 􀀱􀀮􀀴􀁾􀁄􀁩􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠Surr: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀀱􀁵􀁡􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠14.8 154 MI 121 % % 1 59-127 48-156 10/30/01 9:59 10/30101 9:59 10/30/01 9:59 TM TM TM 886267 886267 886267 TPH TEXAS 1005 Mel TNRCC1005 Units:mglKgmm C6·C12 ND 50 10131101 9:12 AM 886034 ,C12-C28--_... >C28-C35 ND ND 60 50 1 1 101311019:12 10/31101 9:12 AM AM 886034 886034 Total TPH (C6-C35) ND 50 1 10131101 9:12 AM 886034 SUrf: l-Chlorooctane 91.7 % 70-130 10/31101 9:12 AM 886034 Surr: 0-T erphenyl 71.5 % 70-130 10/31101 9:12 AM 886034 􀀬􀀮􀀬􀀭􀂣􀁾􀀠ahdz.=;;; 􀁾􀀠--------------------------------------------Project Manager OUalifiers: NDIU -Not Dateoled at the Reporting Limit >MCL -Result Over Maximum Contamination Limit(MCL) B -Analyle detected In the associated Method Blank D -Surrogate Recovery Unreportahle due to DiluVon • -Surrogate Recovery Outside Advisable QC Limits MI -Matrix Interference J -Estimaled Value between MDL and POL 01101137 Pagal0 11111013:11;50 PM Quality Control Documentation 01101137 Page 11 11/11013:11:51 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660·0901 ExxonMobll 4191 Belll!ne Addison, TX Analysis: TPH Texas 1005 WorkOrder: 01101137 Method: TNRCC1005 Lab Batch 10: 15887 Method Blank Samples in Analytical Balch: RunlD: HP_8_011030A-885994 Units: mgIKg LS'lb SamQle 10 !;lIen! Samele ID Analysis Date: 1013012001 16:39 Analyst: AM 01101137·01A N.Wall Preparation Date: 1013012001 13:57 Prep By: J_F Method TNRCC 1005 01101137 -02A E.Wall 01101137·03A S. Wall Analyle Result Rep Limltl >C12·C2B ND 50: >C2B..c35 NO 50 C6-C12 ND 50 Total TPH tG.O:CS5 ND 50 SUrr: 1-QtJlofOOClane 93.51 70-130 Surr: o·Terphenyi 82.3 ... 70·130, 01101137-04A W.Wall 01101137-05B Tank Bouom North 01101137-06A Tank BoUam North Middle 01101137-07A Tank Bonom South Middle 01101137-08A Tank Bonom South Laboratorv !;antrol &I.mple (LeS) RunlD: HP_8_0i1 030Ml86030 Units: mglKg Analysis Date: 10131/2001 8:08 Analysl: AM Preparation Date: i 013012001 13:57 Prep By: J_F Method TNRCC 1005 Analyte Spike Added Result Percent Reoovery Lower Limit Upper Limit >Ci2·C28 .._----_.... C6-C12 500 540 109 70 130 500. 520 105 70 130 Total TPH (C6·C35) 1000 1060 106 70 130 􀁍􀁡􀁴􀁲􀁩􀁬􀀡􀁩􀁊􀁾􀁾􀁾􀁾􀁴􀀨􀁍􀁓􀀩􀀠JMatrix Spike Duplicate (MSD) Sample Spiked: 01101137-01 RunlO: HP_B_011030Ml85995 Units: mglKg Analysis Date: 101301200117:10 Analyst: AM Preparation Date: 1013012001 13:57 Prep By: J_F Method TNRCC 1005 MS Result MSD I MSD Result RPD:RPDMS MS% MSD%Analyte Sample Low High Spike ii Result Spike RecoVllry Recovery Limit·; Limit Limtti Added i Added I SOO 400 80.B 8.701 20 130>CI2-C26 ND: 5001 430. 86.4 70 500 420C6-C12 NOi 500 440! 88.0 83.4 70 1305.371 20 NO! 10001 670. 87.0 1000 820 82.0.Total TPH (C6·C35) 5.92i 20 70 130 Qualifiers: ND/U· Not Detecled at the Reporting Limit MI 􀁾􀀠Matrix Jnterference B 􀁾􀀠Analyte detected in the associated Method Blank D • Recovery Unreportable due to Dilullon J -Estimated value between MDL and POL •• Reoovery Outside Advisable QC limits The percent recoveries for QC samples are correct as reported. Due to signlficant figures and 01101137 Page 12 rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 11/11013:11:S6PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660·0901 ExxonMobil 4191 BelUine Addison, TX Analysis: PurgeabJe Aromatics Wo,kO,der: 01101137 Method: SW8021B Lab Batch ID: R46S28 Method Blank Samples In Analytical Satch: RunlD: HP_O_Ol1030A·8844S4 Units: uglKg Lab Sample 10 Client Sample ID Analysis Date: 1013012001 10:49 Analyst: TM 01101137·03A S. Wall Anwyt_ Resull Aep Limit, +_-'N""'O._ 1.0, ND:-----ui: NO 1.0 ""-__________ X nes Talal NO 1.0 SUIT. 1 Olffl/orobenzene .....96.4: 59-127'􀁾􀁓􀁾􀁵􀀧􀀢􀁲􀁲􀀺􀁾􀀮􀀴􀀷􀀢� �􀀽􀁲􀀢􀀧􀁯􀁭􀁾􀁯􀁦􀁩􀀢􀀧􀁵􀀢􀀧􀁯􀁲􀀢􀁯􀀺􀀢􀀢􀀬􀀬􀀢􀀧􀁮􀁺􀀽􀀮􀀧􀀭􀀺􀁮􀁃􀀺􀀭􀀮􀀭􀀭􀀭􀀭􀀫􀁾􀀠101.1 􀀴􀀸􀁾􀀱􀀵􀁾􀀳􀀬􀀠laboratory Control Sample (LeS) AunlD: HP_OJll1030A-8B44B3 Units: ugIKg Analysis Date: 1013012001 10:11 Analyst: TM 01101137·04A W.Wall 01101137·05A Tank Bottom North 01101137-06A Tank Bottom North Middle 01101137·07A Tank Bottom Soutll Middle 01101137-08A Tank Bottom South I Analyts i Spike IAesull I Percent Added ! Recovery LOWer limit .. .. UpperLimit 120Benzene I 50 44 89 60 Etllylbenzene 50, 43 87 68 127 :Toluene I 501 44 80 64 1221 :Xylenes,Total I 150, 130 87: 68 1291 􀀭􀀭􀁾Matrix Spike (MSi JMatrix Spike Duplicate tMSD) Sample Spiked: 01101137·01 AunlD: HP_O_011030A·886081 Units: ugIKg Analysis Date: 1013112001 5:34 Analyst: TM MSD MSD Aesult MSD% APD Low HighAn.lyte I Sample MS ' MS ResuJt I MS % RPD Spike Aecovery Limit Limit LimitAesull SPike! i Recovery Added, Added 74.0 1720 12.21 34Benzene I ND 201 15 83.6 35. 139! 137:Ethylbenzene ND: 201 13 65.4 20 15 76.1 15,1 ! 35 311 20 31: 137,Toluene ND 201 13 64.9 16 78.5 18.9 28I 60 46 76.7 19 144IXylenes,Total NDI 411 68.3 11.5 38I 601 Oualifiers: NDiU • Not Detected at the Aeporting Limit MI -Momx Interlerence B • Analyte dejected in tlle associated Mathod Blank D -Recovery Unreportabfe due to Dilution J -EsUmaled value between MDL and POL * -Recovery Outside Advisable QC limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01101137 Page 13 rounding, the reported RPD may differ from tlle displayed APD values but is correct as reported. 11ItlO1 3:11;56 PM HOUSTON U\l30RATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 􀂣􀁲􀁾􀀷􀀠ExxonMobii 4191 Beltline Addison. TX Analysis: Purgeable Aromatics WorkOrder: 01101137 Method: SW8021B Lab Batch 10: R46649 Method Blank Samples in Analytical Batch: AunlD: HP_O_Oll031A-886916 Units: ug/Kg lab Sample ID Client Sample 10 Analysis Date: 10/31/2001 6:34 Analyst TM 01101137-01A N.Wall 01101137-02A E.Wall LJ?urr: 􀀴􀀭􀁂􀁲􀁯􀁭􀁯􀁦􀁬􀁯􀁯􀁲􀁯􀁢􀁥􀁮􀁾􀁥􀁮􀁥􀀠...􀁾􀁾..􀁾_ ..98.51 48-156 ! Analyle Result AepUmH 􀁾􀀭...---.. :Senzene NO 1.0 l£!hlAbonzene NO 1.0 'Toluene ND 1.0 IX\lienesTotal NO' 1.0 I Sun: 1 4-Dilfuorobenzene 95.4, 59-127 laboratory Control Sal'f.lple {LeS} AunlD: HP_O_011031A-l!8S909 Units: ugIKg Analysis Date: 1013112001 5:04 Analyst: TM Analyte Spike Aesult Percent Lower Upper RecoveryAdded Limit Urnlt Benzene 50i 51' 102 12060 Ethylbenzene 49 99 12750 68 Toluene I 50 50 100 64 122. ...􀁾􀀭􀁾􀁾... .S,Total 147150 129,98' 68 ...􀁾􀁾􀀭􀀭􀁾􀁾.. Matrix Solke (MIDI Matrix Spike Dupl]eate IMSO) Sample Spiked: 01101137-01 AunlD: HP_O_011031A-886912 Units: uglKg Analysis Data: 1013112001 5:34 Analyst: TM CAnalyte Sample MS MS Result MS% .1 MSD MSDAesult Aesult Spike Aecovery Spike Added I Added 'Benzene ND 20 15 74.0 20 17 1 Ethylbenzene ND. 20 13 65.4 20 15: Toluene ND, 20 13! 64.9 20 16 iXylenes,Total NDI 60 -..􀀭􀁾􀁾􀁾􀁾... 411 68.3 60 46 MSD% RPD Recovery 83.6 12.2 76.1 15,1' 78.5 16.91 76_7: 11.5 RPD Low High I Umit Limit Limit, 34 35 139! 35: 31 137, 281 31 􀁾􀁾􀀠􀁾􀀹􀀠1441 􀀭􀀽􀀭􀀭􀀭􀀺􀀭􀀺􀀭􀀺􀀻􀀭􀀭􀀭􀀻􀀭􀀻􀀻􀀺􀀺􀀺􀀻􀀭􀀻􀀭􀀻􀀽􀀬􀁾􀀺􀀻􀀭􀀺􀀺􀀭􀀺􀁾􀀠...􀁾-_... aualifiers: ND/U -Not Detected at the Reporting Umit MI -Mattix Interference B -Analyte detected In the associated Method Blank D -Recovery Unreportable due to Dilution J -Estimated value between MDL and POL • -AecOllt>'Y Outside Advisabte OC Limits The percent recoveries for QC samples are oorreot as reported. Due to significant figures and 01101137 Page 14 rounding, the reported APD may differ from the displayed RPD values but is correct as reported. 11111013:11:57 PM HOUSTON LABORATORY 8660 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobii 4191 Beillin. Addison, TX Analysis: Po.ynuc!ear Aromatic Hydrocarbons WorkOrner: 01101137 Metllod: SW8310 Lab Batch 10: 15817 Method Blank Samples In Analytical Batch: RunlD: 2_011030A-ll86020 Units: uglKg Lab Sample 10 Client Sample 10 Analysis Date: 1013012001 17:55 Analyst: YN 01101137-oSB Tank Bottom North Preparation Date: 10l30I200110:00 Prep By: LL Method SW3550B Analyte Result Rep Limit 1 ,Acenaghthena NO 3.3 NO 3.3􀁾􀁾􀁾􀁮􀁡􀁰􀁨􀁴􀁨􀁹􀁦􀁥􀁮􀁥􀀠, NOAnthracene 3.3: Benz{a)anthracana ND 3.3'li:3]iBenzo(a)pyrene NO BenzoH.'l lIuoranthane ND' 3.3' 'Benzoio,h,l}oe£vlena NO 3.31 iBSnzofk}f!uotanthene NO 3.3 3.31Ch en. NO NO􀁴􀁧􀁌􀁾􀁮􀁺􀁯􀁲􀁡􀀠h}ant hracene 3.3 ,Fluoranthene NO 3.3 􀁎􀁄􀁾􀀠3.3Fluorene 3.3'Indenol1 2 3·cdlovrene NO NO 3.3􀁾􀁑􀁴􀁩􀁴􀁨􀁡􀁬􀁥􀁮􀁥􀀠,Phenanthrene NO 3.3 NO 3.3: sur;:; 1-Fluoronaphthalene 􀀴􀀱􀁾􀀹􀀷􀁾􀀠60.0 Sun: Phenanlhrene..o10 64.3 38-108 Laboratory Control Sample ILCS) RunlD: lL011030A-llB6021 Units: uglKg Analysis Date: 1013012001 18:33 Analyst: YN Preparation Date: 101301200110:00 Prep By: J_L Method SW35S0B I Analyle I Spike Result Percent Lower Added Recovery Limit Acenaphthene I 16.7, 12, 70 29: 􀁉􀁁􀁣􀀮􀁮􀁡􀁰􀁨􀁾􀁥􀁮􀁥􀀠16.7 121 70 25 iAnthracene 16.7 111 68 25 Benz(ajanthracene 16.7 13 76 26 IBenzo(ajpyrene 16.71 14 86: 28 iBenZO(b)lluoranthene I 16,7: 131 76 29 IBenzo(g,h,i)perylene 16.7 131 77 22 Benzo(kjfluoranlhene 16_7 12 741 30 IChrysene 16.7 13i 76, 31 ,Dlbenzo(a,h)anlhracene 16_7 12 74, 27, Fluoranlhene 16.7 12 70: 231 Fluorene 1 16.7, 11 68 27' Indeno(1.2,3-cd)pyrene 16,71 12 73 2BI Upper 1 Umit 1051 119 101" 􀀢􀀧􀁾􀀠114 118 130 120 138 120110 􀁾􀀠123 Qualifiers: NDIU • Not Detected at the Reporting Limi! MI -Matr1x Interference B -Analyte detected in the associated Method Blank D -Recovery Unreportable due 10 Dilution J -Estimated value between MOL and paL • -Recovery Outside Advisable ac Limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01101137 Page 15 rounding, the reported RPD may differ from the displayed RPD valu.s but is correct as reported. 11111{)13:11:58PM -----HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 􀂣􀁲􀁾􀀷􀀠ExxonMobii 4191 Beilline Addison, TX Analysis: Polynuclear Aromatic Hydrocarbons WorkOrder: 01101137 Method: SW8310 Lab Batch 10: 15817 Laboratory Cootrol Sample (beS) RunlD: Untts: ugIKg Analysis Date: 10130/200118::)3 Analyst: YN Preparalion Dat.: 1013012001 10:00 Prap By: JJ-MethOd SW3560B Analyle Spike Added Result Percent Recovery Lower limit Upper Limit Naphthalen. 16.7 11 66 25 106 􀁾􀀭􀀭.... Phenanthrene 16.7 12 71 25 111 Pyrena 16.7 12 73 27 115 􀁟􀁾􀀽􀁌􀀮􀀮...._ .Matrix 􀁓􀁰􀁩􀁫􀁾􀀮􀀠(MS' JMatrix Spike Duplicate (MSDl Sample Spiked: 01101130-04 RunlD: Z,011030A.aB6035 Units: uglKg Analysis Date: 10/301200121:05 Analyst: YN Preparation Date: 101301200110:00 Prep By: J_1. Method SW3550B MS MS Result MS%Analyle Sample High IRPD RPD'lowMSO I MSD Result I MSO %! Recovery Spike RecoveryResult Spike Limit Limtt Limit Added Addedi , .. 6.7 40.2 16.7 , 9, 54.116.7Acenaphthene 1 ND 29.3 50 9 99 --:----' ···1 2o.g46.1 16.7 9.5 56.916.7 7.7 50 4,Acenaphthylene ND 105.-._... 43.9 50' 1416.7, 7.3 16.7 S.S 52.7 18.2:Anthracene NO 83 , 51.3 16.7 12 70.3 31.2 50 24! 115IBenz(a)anthracene NO' 16.7 9 16.7 10 52.7 16.7 14 74.1 33.7, 50 21' 92.Benzo(a)pyrene I NO 49.8 14' 13516.7' 9.2 16.7 14' 77.2 43.2, 50iBenzo(b)fluoranthena NO ..._------_.... 11 16.7 14, 70.9NO 16.7 51.6 􀀳􀁩􀁾􀀵􀀱􀀠50 141'Senzo(g,h,i)perylena 1 16.7 12, 70.5ND 16.7 8.6 48.6 36.6 50 19Benzo(k)tluoranthena 125' 171,8,7ND 16.7 50.3 16.7 12 68.6Chrysene 330.8' 50 49.6 16.7NDi 16.7 9.1 12 65.3 27.3 50 31 106Dlbenzo(a,h)anthracene 1 51.49.4 16.7 12 64,4, 22.4Fluoranthene i NO! 16.7 50 126,8,, NO, 16.7 6.9 37.6 16.7 9.2 51.8 31.8 50 1 131,'Fluorene 16.7 10' 55.2 16.7 13 72.11 26.5, 50: 21NO 119,lndeno(I,2,3-cd)pyrene ..I . 91 1ND 5.91 29.7 16.716.7 8.2 43.1 36.8 50 8INaphthalene 7.81 43.0ND 16.7 9.9 55.8 25.8 22:Phenan!hrene 16.7 50 99 ND 16.716.7. 9.6 52.9 12 68.S 26.2 50 3. 128IPyrene Qualifiers: NOIU • Not Detected at the Reporting Limit MI • • Matrix Interlerence B • Analyle detected in the associated Method Blank D 􀁾􀀠Recovery Unreporlable due to Dilution J • Estimated value between MOL and pal •• Recovery Outside Advisable ac limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01101 t37 Page 16 rounding, the reported RPO may differ from the displayed RPO values but is correct as reported. 1111101 3:11:55 PM Sample Receipt Checklist And Chain of Custody 01101137 Page 17 11/1/013:11:59 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, 1X 77054 (713) 880-0901 Sample Receipt Checklist Wonrorder. 01101137 Received By: OS Date and Time Received: 10/30101 9:30:00 AM Carrier name: FedEx Temperature: 2 Chilled by: Water Ice 1. Shipping container/cooler in good condition? 2. Custody seals intact on shrppping container/cooler? 3. Custody seaJs intact on sample bottles? 4. Chain of custody present? 5. Chain of custody signed when relinquished and received? 6. Chain of custody agrees with sampre labels? 7. Samples in proper containerlbottle? 8. Sample containers intact? 9. Sufficient sample volume for indicated test? 10. All samples received within holding time? 11. ContainerlTemp Blank temperature in compliance? 12. Water 􀁾􀀠VOA vials have zero headspace? 13. Water .. pH acceptable upon receipt? SPL Representative:1 CUent Name contacted:Li=.===========::::l Non Conformance Client Inslructionls: Ve. [i1I NoD Not Pre.ent Yes NoD Not Present [i1I Ves 0 No Not Present [i1I Ve. [i1I NoD Yes [i1I NoD Ves [i1I No Ves [i1I NoD Yes [i1I NoD Yes [i1I No Ves [i1I NoD Yes [i1I Ves 0 NoD Not Applicable [i1I Ye. NoD Not Applicable Ii!l Conlaet Date & 􀀧􀀧􀀧􀀧􀀧􀀧􀁾􀀧􀁌􀁟..___________J 01101137 Page 18 11/1101 3:12;00 PM .., Ul/UI.(:JI Triplicatlf. 􀁉􀁃􀀺􀁈􀁾􀁁􀁾􀁉􀁎􀁾􀁏􀁾􀁆􀁾􀁃􀀺􀁕􀀺􀁓􀁔􀁾􀁏􀁾􀁄􀀺􀁙􀁾􀁒􀁾􀁅􀀺􀁃􀀺􀁏􀁒􀀺􀀺􀁄􀁾􀁎􀁏􀀺􀀺􀀮􀁾􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀁾__􀁾􀁐􀀺􀁾􀀺􀁹􀀽􀀽􀁾􀁾􀀽􀀱􀀽􀀱(Southweot a Waohlngton) t-􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀀭􀁾􀀭􀀭􀀮􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀀭􀀭􀀭􀀭􀁾􀁾􀀭􀀭􀀮􀁾􀁾􀀠EXXON COMPANY, USA. e""on Engineer: Phone: 713 6 =ct; 9 c. /$? Consultant Co. Name 􀂣􀁦􀀩􀁅􀀭􀁾􀀠Contact: 􀁾􀁡rj::..1acL ANALYStS REQUEST: (CHECK APPROPRIATE BOX) 􀁁􀁰􀀺􀀺􀀻􀀮􀀯􀀺􀁾􀁤􀀠Fax: q-p. 􀁾􀀧􀀷􀁌􀀷􀀲􀀠􀁾􀁡􀀠􀁾􀀠􀁾􀀠0 I /!!::-too RAS It. 􀁾-o.;:l. 7.5 FacilltylStafl> ID /I (TN Only): 0 " i!i AFE /I (Terminal Only): Consuttont 􀁾􀁉􀁴􀀮􀁾-Oa 􀁾􀀭􀁾􀀠􀁾􀀠􀁾􀀠I􀁾􀀠LooatiQ'ktiJC/l 􀁂􀁥􀁬􀁦􀁌􀀢􀁶􀀨􀁯􀀨􀁧􀁾􀁾􀀠􀁾􀁡􀁁􀀯􀀠􀀨􀁓􀁴􀁡􀁴􀁾􀁚􀁔􀁙􀀠ffi i 􀁾􀀠􀁾􀀠􀁾􀀠con.ulantWarl< Re sa II: 􀁾􀀠􀁾􀀠􀁾􀀡􀀠􀁾􀀠􀁾􀀠0 􀁾􀀮􀀮􀀺􀁳􀀺􀀮􀀺􀁭􀁾􀁰􀁉􀁥􀁤􀀺􀀺􀀺􀀺􀀺􀁂􀁹􀁾􀀺􀁾􀁾􀁦􀀡􀁩􀁆􀀮􀁅􀀮􀀽􀀽􀀽􀁾􀁾􀁾􀁩􀁦􀁆􀁲􀁩􀁾􀁾􀁩􀀮􀁩􀁩􀁩􀁾􀁾􀁾􀀡􀁩􀁪􀁾􀁾􀀻􀀻􀀻􀀻􀁆􀁾􀁾􀀠8 􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾u..:« us... C) 􀁯􀁾􀀾􀀼􀀰􀀡􀀡􀁩􀀠".SAMPLE 1.0. ci 1J 􀁾􀀠'" .. S .. <5 ZUnlC. ... O ... > 0 0 0 ,. m􀁾􀀠􀁾􀀠Ii m " a ".. 􀁾􀀠Iiii 0 ;0 0 0 􀁾􀀠􀁾􀀠:giii Ii! 􀁾􀀠;;; 􀁾<5 0-or '">. " w 􀁾􀀠,.:;; .. 􀁾w '"., .. .. AI 􀁾􀁏􀀠1\ I/oh, 􀁉􀁴􀀿􀀻􀁾􀀮􀁢X vi I/tF: III i>< 'AIm r.J.-l l.d1/,.. I'-If*' <;-aud Wy( 􀁾􀀠"" -􀁾􀁊􀀠􀁾􀀠Iti'ob 􀁾􀀠('V 1\ SPECIAL DETECTION LIMITS (Specify) REMARKS:TAT 24 HR. V. 48 HR. 72 HR ....... : T: 98HR_ f>􀁔􀁾􀀻􀁘􀀠􀁾􀁏􀁾􀀠I}S III 0 􀁾Tt! 􀁾IlrT6f aBusiness 'Contact us Prlor to Sanding Sample other EXXON UST CONTRACT NO. SPECIAL REPORTING REQUIREMENTS (Specify) LAB USE ONLY Lot /I Sroraga Location C41483 PDF 0 DEDD 􀁾􀀠de) Slandatd 0 CLP 0 􀀺􀀺􀀮􀁾􀁾Levi. A < iJFAJY'P D FAX C·O-C WIREPORT IINORK ORDER#: () /161/37 LAB INORK RELEASE It. 􀁒􀁥􀁾􀁮􀁱􀁵􀁾􀁈􀁾􀀧􀀷􀁊� �􀀷􀁔􀀷􀁔􀀠Or Time 􀁾􀁉􀀠Received By:I L IIII I Jl' MIt?M . In /-z.(J ",,1/5?􀁾􀀧􀀢􀀩􀁬􀁩􀀠JOriginal ,White Lab's Copy' Green Client Copy' Yellow CUSTODY I􀁒􀁥􀁬􀁬􀀡􀀱􀁱􀁊􀁩􀁩􀁾􀀺􀀠I c;:> II /VI b 0 ' I 117D.trl! 'I Tim. Received By: RECORD . . Date -. 􀀽􀁮􀁭􀁥􀀺􀁣􀀺􀀭􀀭􀀭􀀭􀁫􀀽􀁾􀀽􀀺􀀺􀀺􀀭􀀺􀁴􀁲􀀭􀁾􀁬􀀢􀁜􀁾􀁟􀀻􀀻􀀺􀀻􀁦􀀻􀁺􀀺􀀻􀀻􀁴􀁩􀁬􀁮􀀺􀁟􀀺􀀺􀀻􀁟􀀺􀀺􀀺􀁝Relinquished: .. 1 .'., .'/ .' HOUSTON lABORATORY aaao INTERCHANGE DRIVE HOUSTON, TEXAS 77054 (113) SfiCH)901 RFr.EIVED ExxonMobil 􀁾􀁉􀁏􀁖􀀠1 9 2001 Certificate of Analysis Number: 01110243 EA 􀀢􀀧􀀱􀁾􀁜􀀮􀀮􀀱􀁉􀀱􀁾􀁴􀁅􀁒􀁉􀁎� �􀀠Report To: EA Engineering Mark Loch 1420 Volwood Parkway Suite 170 Carrollton TX 75006ph: (972) 484-1420 fax: -------' Project Name; 5090275 Site: 6-0275,21044479 Site Address: PO Number: LWRII21044977 State: Tex.. State Cert. No.: Date Reoorted: 11114101 This Report Contains A Total Of 13 Pages Excluding This Page And Chain Of Custody Date 11114101 HOUSTON LABORATORY 8880 INTERCHANGE ORIVE HOUSTON, TX 77054 (713) 660·0901 Case Narrative for: ExxonMobii Certificate of Analysis Number: 01110243 Report To: Project Name: 5090275 EA Engineering Site: 6-{)275,21044479 Mark Lach Site Address: 1420 Valwood Parkway Suite 170 PO Number: LWRII21044977 Carrolfton 1)( 􀁾􀀠Texas 75006State Cart. No.: ph: (972) 484-1420 fax: Date ReDorted: 11114101 Matrix spike (MS) and mallix spike duplicate (MSO) samples are chosen and tested at random from an analytical batch of "like" matrix to chOCk for possible matrix effec!. The MS and MSO will provide sHe specific matrix data only for 1I1ose samples which are spiked by the laboratory. Since the MS and MSO are chosen at random from an analytical batch, the sample chosen for spike purposes mayor may not have been a sample submitted in this sample delivery group. The valldlly of the analytiCal procedures for which data is reported in this analytical report is determined by the Laboratory Control Semple (LCS) and the Meli10d Blank (MB). The Laboralory Control Semple (LCS) and the Method Blank (MB) are processed with the samples and the MSIMSO to ensure method crileria are achieved throughout the entire analytical process. Any olher exceptions associaled with Ihls repon will be footnoted In the analytical result pagels) or the quality control summary pagels). Please do not hesitate to contact us If you have any questions or comments pertainIng to this data report Please reference the above Certificate of Analysfs Number. This report shall not be reproduced except in full, without the written approval of the laboratory, The reported results are only representative of the samples submitted for testing. SPl. Inc. is pleased to be of service to you. We anticipate working with you in fullflling all your current and future analytical needs. 01110243 Page 1 􀀺􀁌􀁾􀀠Date Senior project Manager 11114101 HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX n054 (713) 660-0901 ExxonMobil Certificate of Analysis Number: 01110243 ReQortTo: EA Engineering Project 􀁾􀁭􀁥􀀺􀀠5090275 MarkLach 1420 Valwood Parkway Suite 170 Site: Slle Address; 6-0275,21044479 Carrollton TX PO Number: LWR#21044977 75006ph: (972) 484-1420 fax; (972) 247-7220 State: Stale Cart. NQ.: Texas Fax To: DS!te Re2orted: 11114101 Date Received ! Client Sample 10 I Lab Sample 10 Matrix Date Collected COCID HOLD , 111710110;00:ooAM.LT-l-North 01110243-01 Soil 1112101 _.. 0 !LH-North 01110243-02 1112101 1117101 10:00:00 AMSoil 0 'Middle DI-East 01110243-03 11/2/01 111710110:oo:ooAMSoil [J 01110243-04 Soil 11/2101 I 1117/01 10:00:00 AMISoUth 01 West 0 01110243-05 I Soil 1112101 1117101 10:00:00 AM ILT-a-South ...IL, 􀁾􀁾􀁾􀁟􀁾__􀁾__􀁾___________________________________􀀱􀁟􀀯􀀱􀁾􀀰􀁾􀀱􀀠Sonia Wast Dale Senior Project Manager Joel Grice Laboratory Director Ted Yen Quality Assurance Officer 01110243 Page 2 111141018:21:44 AM HOUSTON LABORATORY es80 INTERCHANGE DRIVE HOUSTON, TX 77054􀁾􀁾􀀷􀀠(713) es0-0901 Client Sample 10:LT-1-North Collected: 1112101 SPl Sample 10: 01110243-01 Site: 6-0275,21044479 AnalysesIMethod Result Rep.Limit Dil. Faetor QUAL Date Analyzed Analyst Seq. II PURGEABlE AROMATICS MCl SW8021B Units: ug,lKg Benzene NO 1 1 11109101 4:05 TM 904954 Ethylbanzene 10 1 1 11109101 4:05 TM 904954 Totuena ND 11/09101 4:05 TM 904954 Xylenes,Total 1 11/09/01 4:05 TM 904954 Surr: 􀀱􀀮􀀴􀁾􀁄􀁩􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠109 % sg-l27 11/09101 4:05 TM 904954 Surr: 4-Bromofluorobenz:ana 94.0 % 48-156 11/09101 4:05 TM 904954 TPH TEXAS 1005 MCl TNRCC1005 Units: mglKlI C6-C12 ND 50 11/12101 19:15 AM 906016 >C12-C28 NO 60 1111210119:15 AM 906016 >C28·C35 NO 60 1111210119:15 AM 906016 Total TPH (C6-C35) NO 50 11/1210119:15 AM 906016 Surr: 1..chlorooctane 102 % 70-130 1111210119:15 AM 906016 SUIT: 0-T erphenyl 104 % 70-130 11/1210119:15 AM 906016 Sonia West Project Manager aualifiers: NDIU -Not Detected at !he Reporting Umit >MCL -Result Over Maximum Contamination Llmit(MCL) B • Anelyte detected in !he associated Method Blank D -Surrogate Recovery Unreportable due to Dilution •. Surrogate Recovery Outside Advisable OC Limite MI -Matrix Interference J -Estimated Value between MOL and POL 01110243 Page 3 11/141018:21;47 JW. HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054􀁾􀁾􀀷􀀠(713) 660-0901 Client Sample 10: LT-2-North Collected: 1112101 SPL Sample 10: 01110243-02 Site: 6-0275,21044479 AnalysesIMethod Result Rep.Limit Oil. Factor QUAL Date Analyzed Analyst Seq.• PURGEABLE AROMATICS MCL SW8021B Units: ugIKg Benzene NO 11109101 4:33 TM 804955 Elhylbenzene ND 11109/01 4:33 TM 904955 Toluene ND 1 1 11/09/01 4:33 TM 904955 Xyienes,Tolal ND 1 1 11/09/01 4:33 TM 904955 SUIT: 1,4-Difluorobenzene 97.6 % 59-127 1 11/09101 4:33 TM 904955 Surt: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀁊􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠9 1.3 % 48-156 11109/01 4:33 TM 904955 TPH TEXAS 1005 MCL TNRCC1005 Units: mglKg C6-C12 ND 50 1 11/12101 19:25 AM 908017 >CI2-C28 ND 50 11/1210119:25 AM 906017 >C2&-C35 ND 50 1 11/12101 19:25 AM 906017 Total TPH (C6-C35) ND 50 1 11112101 19:25 AM 905017 Surr: l-Chioroootane 103 % 70-180 11112101 19:25 AM 906017 SUIT: o-Terphenyl 103 % 70·130 11/1210119:25 AM 906017 SonfaWest Project Manager Qualifiers: NDiU -Not Delected at Ihe Reporting Urnil >>MCL -Result Over Maximum Contamination Umit(MCLl B -Anaiyte detected in the associaled Method Blank D • SUlTogate Recovery Unreportable due to Dilution •• Surrogate Recovery Outside Advisable QC Urnils MI • Malrix Interlerence J -Eslimaled Value between MDL and POL 01110243 Pege4 11/14f018:21:48 AM HOUSTON LABORATORY SB80 INTEROHANGE DRIVE HOUSTON, TX 77054 (713) 66()'0901 Client Sample 10: Middle Df-East Collected: 1·112/01 SPl Sample 10: 01110243-03 Site: 6-0275,21044479 AnalyseslMethod Result Rep.Limit Dil. Factor QUAL Date Analyzed Analyst Seq. II PURGEABlE AROf\llATICS MCl SWB021B 􀁕􀁮􀁩􀁴􀁳􀀺􀁵􀁾􀁋􀀹􀀠Benzene ND 1110910111:32 TM 904956 Ethylbenzene Toluene ND ND 11/09/01 11:32 11109/01 11:32 TM TM 904956 904956 Xylenes,T otal ND 1110910111:32 TM 904956 Surr: 1.4-Difluorobenzene 94.6 % 59-127 1110910111:32 1M 904956 SUrT: 4-Bromofiuorobenzene 94.3 % 48-156 1110910111:32 TM 904956 TPH 􀁔􀁅􀁘􀁾1005 MCl TNRCC1005 Units: mglKg 06-012 ND 50 1111210119:36 AM 906018 >CI2·028 ND 50 11/1210119:36 AM 906018 >C28-C35---.--. Total TPH (06-035) ND ND 50 50 11/1210119:36 11/1210119:36 AM AM 908018 906018 Su,,: 1-Chlorooctane 103 % 70-130 1111210119:36 AM 906018 Su,,: o-Terphenyl 106 % 70-130 11/1210119:36 AM 906018 Sonl.West Project. Mana"'gc;.er'-___________________________________.___ QuaUfier.: NDIU -No! Detecled at the Reporting limit >MOL -Result Over Maximum Contaminaoon L1mit(MCL) B -Analyle delected in tI1e associated Method Blank D -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery Oulslde Advisable OC limijs MI 􀁾􀀠Mattix Interierence J -Estimated Value between MDL and POL 01110243 Page 5 11114101 6:21:48 JW --HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 􀁾􀁾􀀷􀀠(713) 660·0901 Client Sample 10: South DI West Collected: 11/2101 SPL Sample 10: 01110243..()4 Site: 6-0275,21044479 AnalysesIMethod Result Rep.limit Oil. Factor QUAL Date Analyzed Analyst Seq. II PURGEABlE AROMATICS MCL SWB021B Units: ug/Kg Benzene 1.8 1 11109/0112:00 TM 904957 Ethylbenzene 5.3 1 11/09/01 12:00 TM 904957 Toluene 2.6 11/09/01 12:00 TM 904957 Xylenes,Total 2.5 1 1 11109101 12:00 TM 904957 SufT: 1,4-Dffluorobenzene 117 % 59·127 1 11/09/01 12:00 TM 904957 Surr: 4-Bromofluorobenze ne 90.1 % 48·156 11/09/0112:00 TM 904957 TPH TEXAS 1005 CS-G12 >C12·C29 ND NO 50 50 MCL TNRCC1005 1 Units: m!l!Kll 11/09/01 2:35 AM 11/09/01 2:35 AM 904520 904520 >C2a-G35 NO 50 1 11109/01 2:35 AM 904520 rotal TPH (C6-035) ND 50 1 11/09/01 2:35 AM 904520 Surr: 1 􀁾􀁃􀁨􀁬􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀁥􀀠Surr: o·Terpherryl 112 112 % % 70·130 70·130 1 1 11/09/01 2:35 11/09/01 2:35 AM AM 904520 904520 Sonia West Project Manager Qualifiers: ND/U • Not Detected at the Reporting Limit >MCL· Result Over Maximum Conillminalion Limit(MCL) B • Analyle delec1ad in the associated Method Blank D • Surrogate Recovery Unreportable due to Dilution •• Surrogate Recovel}' Outside Advlsabie ac Limits MI 􀁾􀀠Matrix Interference J . Estimated Value between MOl and paL 01110248 Page 6 11/14/01 8:2:1:49 />M HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660·0901 Client Sample 10: l T -3·South Collected: 1112/01 SPL Sample 10: 01110243·05 Site: 6-0275,21044479 Analyses/Method Result Rep.Llmlt Oil. Factor QUAL Date Analyzed Analyat Seq. # PURGEABLE AROMATICS MCL SW6021B Units: uQfKg Benzene 1.2 11/09101 12:26 TM 904956 Ethylbenzene 15 11/09/01 12:26 TM 904958 Toluene ND 11/09101 12:26 TM 904956 Xytenes.Total 10.6 11/09/01 12:28 TM 904956 .._ .._SUIT: 1,4·Dlfluorobenzene 107 % 59-127 1 11/09101 12:26 TM 904958 Surr: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁡􀁮􀁥 􀀠94.4 % 48·156 1 11/0910112:26 TM 904958 TPH TEXAS 1005 MCL TNRCC 1005 Units: mQfKg C6-CI2 ND 50 11109101 3:07 AM 904524 >CI2·C28 ND 50 1 11109101 3:07 AM 904524 >C28..c35 ND 50 1 11109101 3:07 AM 904524 T atol TPH (C6·C35) ND 50 1 11109/01 3:07 AM' 904524 SUIT: I·Chlorooclane 106 % 70·130 1 11109101 3:07 AM 904524 SUIT: 0-T erphenyt 111 % 70·130 1 11109/01 3:07 AM 904524 Sonia West Project Manager Qualifiers: NDiU • Not Detected at the Reporting limit >MCL . Result Over Maximum Contamination Umlt(MCL) B • Analyte detecled in the associated Method Blank D 􀁾􀀠Surrogate Recovery Unreportable due to Dilution •• Surrogate Recovery Oulslde Advisable QC limits MI 􀁾􀀠Matrix Inlelierence J • Estimated Value between MDL and POL 01110243 Page 7 11/14/01 8:21:49 AM Quality Control Documentation 01110243 Page 8 111141018:21;50 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobii 5090275 Analysis: TPH Texas 1005 WorkOrder: 01110243 Method: TNRCC1005 Lab Bate. 10: 16032 Melllod Blank Samples In Analyllcal Balch: RunlD: HP_8_0'11128-905995 Units: mg/Kg Lab !iamele 10 Client Saml2ie ID Analysis Date: 111121200115:10 Analyst: AM 01110243-01A LT-l-North Preparation 􀁄􀁡􀁴􀁥􀁾􀀠1110712001 12:38 Prep By: J_F Method TNRCC 1005 01110243-02A LT-2-North 01110243-03A Middle DI-East Analyl. I Result Rep Limit >C12-C2B NO 50 >C2B-C35 NO 50 :C&C12 ND 50 iTotaITPH CS-C35i NO 50 I Surr:; 1.(;hlorooctana SUIT: (}oTerohem:! 99_9 lQ1.3 70-130 70-130 Laboratory Control !iample fLeS) RunlO: HP ....8_0111128-905996 Units: mg/Kg Analysis Date: 11/121200115:21 Analyst AM Preparation Date: 11107f2001 12:38 Prep By: J_F Method TNRCC 1005 Analyte UpparSpike Resutt􀁾I Lower ILimitAdded ! Limit >C12-C28 550 109170 130500 C6-C12 130500 480 961 70 ,Total TPH (C6-C35) 103 70 1301000, 1030 .. Matrix Spike IMS) 1 Matrix !ipike DupliCllte fMSDl Sample Spiked: RunlD: Analysis Date: Preparation'Date: Sample Result Analyle l>c12-c28 NO !C6-C12 ND Total TPH (C6-C35) ND 0111 01 05-01 HP􀁟􀁂􀁟􀀰􀀱􀀱􀀱􀀱􀀲􀁂􀁾􀀹􀀰􀀵􀀹􀀹􀀸􀀠Untts: mg/Kg 111121200115:42 Analyst AM 111071200112:38 P!C12-028 ND 50' 􀀧􀀻􀀮􀁃􀀲􀀸􀁾􀁃􀀳􀀵􀀠NO 50 ca-c12 NO' 50' Total TPH (C6-C351 ND 50 􀁾􀁓􀁵􀁲􀁲􀀮􀀺􀀠1--ChloroOOtane 108.4 70-130 Surr: o--Terohanvl 110.8 70-130 Laboratorv Control Sample {LCS} RunlD: HP_B_Ol1109D-904550 Units: mgIKg Analysis Date: 1110912001 9:46 Analyst: AM Preparation Date: 1110712001 18:35 Prep By: J] Method TNRCC 1005 I Analyle I Spike Result : percent. 1 Lower Added ; Recovery Limit !>C12-C28 ! 500 5001 l00! 70 IC6-CI2 I 500 480 961 70, Upper ! limit 130! 130' IT otal TPH (C6-C35) 10001 9801 98, 70, 130! 1 Matrix Spike IMS) 1Matrix Spike Duplleate IMSOI Sample Spiked: 01110243-04 RunlD: HP_B_011109D-904521 Units: mgIKg Analysis Date: 1110912001 2:46 Analyst: AM Preparation Date: 111071200118:35 Prep By: J_F Method TNRCC 1005 MS Result MSD% ' RPD HighAnalyte Sample , MS MSD, I MSD Result 􀁒􀁐􀁾􀁉􀀠LowI MS%Result : Spike Spike Recovery limit, Recovery limit! Umit I . Added Added: 500, 6401 128 130,>C12-C28 NO 500, 680' 132'* ! 3_07 20 70 500 5501 110 500: 560 1111 1_271 20 70i 130C6-C12 1 ND 'Tolal TPH (C6-C35) ND 1000 1190, 119 10001 1220, 122 2.49 20 70: 130I ... Qualifiers: NDIU -Not Detected at the Reporting Umfi Mf -Matrix Interference B • Analyte detecled in the associaled Method Blank 0-Recovery Unreportable due to Dilullon J • Estimated value between MOL and PQL * -Recovery Outside Advisable ac limits The percent recoveries for QC samples are correct as reported. Due to slgnificant figures and 01110243 Page 10 rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 11114101 8:21:54 AM HOUSTON LABORATORY 8890 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobll 5090275 Analysis: Purgeable Aromatics WorkOrder: 01110243 Method: SW8021B Lab Balch 10: R47488 Method Blank Samples in Analytical Batch: RunlD: HP_J_Ol1109A-904953 Units: ugIKg Lab Sample 10 Client Sample 10 Analysis Date: 11109/2001 3:37 Analysl: TM 01110243'01A LT-l-Narth 01110243-02A LT-2-Narth 01110243-03A Middle DI-East Analyte I 􀁒􀁥􀀮􀁵􀁾􀀠Rep Llmtl Benzene NO 1.0 Elhvlboozene NO 1.0 Toluene NO' 1.g 'x>!.....TOlal ND 1.0 SUIT; 1 􀀴􀁾􀁄􀁬􀁦􀁬􀁵􀁯􀁲􀁯􀁢� �􀁮􀁺􀁥􀁮􀁥􀀠00.1 70-130 SUIT: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁬􀀱􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠95.8 70-130.. 01110243-04A SoUlh 01 Wast 01110243-05A LT -3,Soulh 􀀭􀁾....􀀭􀀭􀀭􀀭􀁾􀀽􀀽􀀽􀀽􀀭􀀻􀀻􀀭􀀺􀀺􀀭􀁣􀀭􀀺􀀺􀀭􀀻􀀺􀀭􀀻􀀻 􀀭􀀻􀀠;:-;-------------laboratory 􀁃􀁾􀁲􀀮􀁴􀁴􀁲􀁑􀀡􀀠Sample (LCS) RunlD: HP􀁟􀁌􀀰􀀱􀀱􀀱􀀰􀀹􀁁􀁾􀀹􀀰􀀴􀀹􀀵􀀰􀀠Unlls: ugIKg Analysis Date: 1110912001 0:46 Analysl: TM Analyte Spi Result Pen:enl Lower Upper I RecoveryAdd limit Umit ,i ,Benzene 50 58 117 117 70 124 jEti1ylbenzene 50' 57, 114 78 129' IToluene 70 126:50: 881 116 ,Xylenes,TotaI 1501 1651 110 71 130, Matrix Spike fMS1/Matrix SeUse Duplicate (MSDl Sample Spiked: 01110174-17 RunlD: HP_J_Ol1109A-904951 Units: ugIKg Analysis Date: 1110912001 1:43 Analyst: TM MSD MSD Result Analyte Sample MS Result MS% MSD% RPD RPD Low HighMSIi Result SpikeSpike , Recovery Reoovery Limit Umit LimitI :Added Added ND 121 500jBenzene 5001 610 640' 129 5.07 34__________M.____ 351 139500:--600 120,Ethylbenzene I ND 500 620 3,78124 35 31 137 500i 620' 124 500 640iToIuene NO 128 3.59 28 31' 137 15001 1770 118 1500 1790IXylenes,Totai NO 119 1.12 38 191 144 Qualifiers: NDiU • Not Detected at 1I1e Reporting Limit MI-Matrix Interference B -Analyte detected In 1I1e associated Method Blank o. Recovery Unreporlable due to Dilution J -Estimated value between MOL and POL • -Recovery Outalde Advisable QC Limits The percent recoveries for QC sampfes are correct as reported. Due to significant figures and 01110243 Page II rounding. the reported RPD may differ from Ihe displayed RPD values but Is correct as "'ported. 11/14101 S:21:S5AM Sample Receipt Checklist And Chain of Custody 01110243 Page 12 11/141018:21:56AM HOUSTON LABORATORV 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Sample Receipt Checklist Workorder: 01 I I 0243 Received By: OS Date and Time Received: 11nt01 10:00:00 AM Garrier name: FedEx Temperature: 4 Chilled by: Water Ice 1. Shipping container/cooler in good condition? 2. Custody seals intact on shlppping container/cooler? 3. Custody seals intact on sample bottles? 4. Chain of custody present? 5. Chain of custody signed when relinquished and received? 6. Chain 01 custody agrees with sample labels? 7. Samples in proper containeribottfe? 8. Sample containers intact? 9. Sufficient sample volume for indicated test? 10. All samples received within holding time? 11. ContainerITemp 8Jank temperature in compliance? 12. Waler -VOAvials have :zero headspace? 13. Water -pH acceptable upon receipt? Ves V•• Ve. Ves Ves Ves Ves Ves Ves Ves Ves Ves Yes 􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠0 0 NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD NoD No! Present 0 No! Present 􀁾􀀠Not Present 􀁾􀀠Not Applicable 􀁾􀀠No! Applicable /ill SPL Representative:1 􀁭􀁾􀀠Contact Pate & Client Name contacted:li===========::::l Cllentlnstrucll,ms:r========================================================='" 01110243 Page 13 iln4l018:21:57 !W. " EXXON COMPANY, USA. O · CHAIN OF CUSTOOY RECORD NO. f--..-, --1\ \ 􀁏􀀧􀁬􀁙􀁾􀁰􀁡􀁧􀁥􀁾􀁾, ANALYSIS REQUESl: 􀁾􀀠OTHER(CHECK APPROPRIATE BOX) -􀁾􀁉􀀭􀀭􀁾􀀬􀀭􀀭􀀭􀁲􀀭􀁲􀀠_. . --,----,---,-0 0 0 '" :J /:ao w g OJ" '" 0 0 0 􀁾􀀠1! 0 0 z 0 􀁾􀀠w !2 '" :f 􀁾􀀠0 n. -' 􀁾􀀠-' 􀁾􀀠a 􀁾􀀠􀁾􀀠0 0.. '" z 0 ;; 0 0 0 􀁾􀀠-' N /:'" ., m 􀁾a; 􀁾􀀠0 0 􀁾􀀠1< 􀁾g 􀁾􀀠co .. '" >!CI2·C28 ISO 50 11/14/01 16:36 AM 909149 >C28·C35 NO 50 11/14101 16:36 AM 909149 Total TPH (CS-C36) 490 50 1 11/14/01 16:36 AM 909149 Surr: 1-Chlorooctane 147MI % 7()'130 1 11/1410116:36 AM 909149 Surr; a·Terphenyi 100 % 7()'130 1 11/14/01 16:36 AM 909149 Preo Method Prep Date ,Prep Initials TNRCC100S 11/091200116:41 Sonia West Project Manager Qualifiers: ND/u • Not Detected at the Reporting Limit >MCL -Result OVer Maximum Contamination Limit(MCL) B • Analyte detected in the associated Method Blank 0-Surrogate Recovel)l Unreportabla dualo Dilution •• Surrogate Recovel)l Outside Advisable QC Limits MI • Matrix Interference J -e.ijmated Value between MDL and PQL 01110375 Page 3 11J26fOl 9:24:27 /J.M HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample 10: LT-1 South Collected: 111810111:10;00 SPLSamplelD: 01110375-02 Site: 6-0275,21044625 AnalyseslMethod Result Rep.Limit Dil. Faclor QUAL Dale Analyzed Analyst Seq. # PURGEABLE AROMATICS MCL SW8021B Units: ug/Kg Benzene 130 380Ethylbenzene_________-.:::=-___ 50 50 50 50 11110101 22:58 1111010122:58 TM TM 904750 904750 Toluene 1000 50 50 1111 0101 22:58 TM 904750 Xylene',Tolal 1880 50 50 1111 0101 22:58 TM 904750 Surr: 1,4-Difluorobenzene 134MI % 59-127 50 1111010122:58 TM 904750 Surr: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠122 0/0 48-156 50 11110101 22:58 TM 904750 TPH TEXAS 1005 MCL TNRCC1005 Units: mgIKg C6-C12 120 50 1 11114101 17:08 AM 909152 >C12-C28 72 50 1 1111410117:08 AM 908152 >C28-C35 Tolal TPH (C6-C35) SUIT: 􀀱􀁾􀁃􀁨􀁬􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀁥􀀠SUrT: 0-T"rphenyl NO 192 119 102 0/0 0/0 50 50 70-130 70-130 1 1 1 11114/0117:08 11114101 17:08 11/1410117:08 11/14101 17:08 AM AM AM AM 909152 908152 909152 909152 Prep Prep Method TNRCC 100S ,Prep Date ;111091200116:41 prep lnltlals I J F Sonia West Projec1 Manager Qualifiers: NDIU -Not Detected at the Reporting Umtt >MCL -Result Over Maximum Contamination Limit(MCL) B -Analyle detected in tile associated Method Blank o -Surrogate Recovery Unrepcrtable due to Dilution • -Surrogate Recovery Outside Advi.able OC Umits MI -Matrix Interference J -Estimated Value between MOL and POL 01110375 Page 4 11fi6l01 9:24:29 PJ/; __ __ ____________________________ HOUSTON LABORATORY BB80 INTERCHANGE DRIVE HOUSTON, TX 77054 􀁾􀁾􀀷􀀠 , (713) 660-0901 Client Sample 10: NE-DI Collected: 1118/01 10:30:00 SPl Sample 10: 01110375-03 Site: 6-0275,21044625 Analyses/Method Result Rep.Llmlt 011. Factor QUAL Date Analyzed Analyst Seq. # PURGEABlE AROMATICS Mel SW8021B Units: u!lKg Benzene ND 5 5 111131018:34 TM 906890 Ethylbenzene ND 5 5 111131018:34 TM 906890 Toluene ND 5 5 111131018:34 TM 905990 Xylenes,Total ND 5 5 11113101 B:34 TM 908990 Surr.: 1.4-0ifluorobenzene 187 MI % 59-127 5 • 11/13101 8:34 TM 908990 Surr. 4-Bromoftuorobenzene 108 % 48-156 5 111131018:34 TM 906990 TPH TEXAS 1005 MCL TNRCC 1005 Units: mg/Kg C6-C12 ND 50 1111410117:19 AM 909153 >Cl::l-C28 ND 50 11114101 17:19 AM 909153 >C28-C35 ND 50 1 1111410117:19 AM 909153 Total TPH (C6-C35) ND 50 1 11114101 17:19 AM 909153 Surr: 1-Chlorooctane 103 % 70-130 1 11114101 17:19 AM 909153 Surr: 0-Terphanyi 97.6 % 70-130 1 11114101 17:19 AM 909153 iPreo MethOd Plep Dale 􀁣􀀮􀀧􀁔􀁎􀀽􀁒􀁃􀀽􀀭􀁃􀀺􀀺􀀺􀀮􀁣􀀮􀁬􀀰􀀰􀀵􀀽􀁟􀀭􀀭􀀬􀀭􀀬􀀱􀁾􀀱􀀱􀁾􀀰􀀹􀀯􀀲􀀰􀀰􀀱􀀠16:41 􀁾􀁾􀁾􀀮􀁾􀁟􀁾/_d 􀁾􀀠 __ Sonia West Proiect Manager Qualifiers: ND/U -Not De1eC1ed at lhe Reporting Limit >MCL -Result Over Maximum Contamination Limit(MCL) B -Analyte detected in the associated Method Blank D -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery OutSide Advisable QC Limits MI -Matrix Interference J -Estimated Value between MDL and POL 01110375 Page 5 11128101 9;24:31 ft.M HOUSTON LABORATORY SSOO INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 66().0901 Client Sample 10: Vapor L T·North Collected: lllatOl 11 :30:00 SPl Sample 10: 01110375·04 Site: 6-0275,21044625 AnalysHIMethod R••ull Rep.Llmit 011. Factor QUAL Date Analyzed Analyst Seq. # PURGEABlE AROMATICS MCl SWB021B Units: uglKg Benzene ND 111131019:05 TM 908991 Elhylbenzene 2.7 11113101 9:05 TM 908991 Toluene 1.5 1 11/13101 9:05 TM 908991 Xyfenes,Total 10.3 1 1 11113101 9:05 TM 906991 Surr: 􀀱􀀮􀀴􀁾􀁄􀁩􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠114 % 59·127 1 11/13/01 9:05 TM 908991 Surr: 4·Bromofluorobenzene 135 % 48·156 1 11113/01 9:05 TM 906991 TPHTEXAS 1005 MCl TNRCC1005 Units: mg!Kg C6-C12 ND 50 1 11/1410117:30 AM 909154 >C12-C28 NO 50 11114/0117:30 AM 909154 >C28-C35 ND 50 11/14101 17:30 AM 900154 Total TPH (C6-C35) NO 50 1 11114101 17:30 AM 909154 Suw. 1 􀁾􀁃􀁨􀁬􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀁥􀀠108 % 70-130 1 1111410117:30 AM 909154 Surr: 0-T erphenyl 104 % 70-130 1 11/14101 17;30 AM 909154 ! Prep Method Prep Date :Prep Initials I TNRCC 1005 11/0912001 16;41 J F ..--Sonia West Project Manager Qualifiers: NDIU • Not Detected at the Reporting Limit >MCL • Result Over Maximum Contamination Llmil(MCL) 6 • Analyle detected in the associated Method Blank 0-Surrogate ReeDvelY UnreportabJe due to Dilution • -Surrogate RecovelY Outside Advisable QC Limits MI -Mallix Interierence J • Eafimaled Value be_en MOL and POL 01110375 Page 6 11/2&'01 9:2:4:33 AM HOUSTON LABORATORY 0000 INTERCHANGE DRIVE HOUSTON. TX 77054 (713) 660-09Ql Client Sample 10: LT-2-South Collected: 11/8101 12:30:00 SPI. Sample 10: 01110375-05 Site: 6-0275,21044625 Analysesll'llethod Re.ult Rep.Limlt Oil. Factor QUAL Date Analyzed Analyst Seq. II PURGEABLE AROMATICS MCI. SW8021B Units: u!tKg Benzene ND 50 50 11/10101 22:28 TM 904748 Ethylbenzene 190 50 50 11/10101 22:28 TM 904748 Toluene 500 50 50 1111010122:28 TM 904748 Xylenes.Total 880 50 50 11110101 22:28 TM 904748 Surr. 1.4-0Ifluorobenzene 122 % 59-127 50 11/10101 22:28 TM 904748 Surf: 4·Bromoffuorobenzene 112 % 48-156 50 11/10/01 22:28 TM 904748 TPH TEXAS 1005 C6-C12 ND 50 MCL TNRCC1005 1 Units: mglKg 11/1410117:41 AM 909155 >C12-C28 ND 50 11/1410117:41 AM 909155 >C28-C35 Total TPH (C6--C35) SUrr: 1-Chlorooctane ND ND 110 % 50 50 70-130 ..---... 1 1 11/1410117:41 1111410117:41 1111410117:41 AM AM AM 909155 909155 909155 6urr: 0-T e!phenyl 105 % 70-130 11114/0117:41 AM 909155 ,prep Melhod iTNRCC 1005 Prep Dete 111091200116:41 Pre Initials J F 􀁾􀁾a..L£-?--z::::::; Sonia West ----------------------Project Manager Queilliers: ND/U -Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Limit(MCL) B -An.lyIe detected in the associated Method Blank o -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery Outside Advisable QC Limits MI . Melli. Interlerence J -Estimated Value between MDL and PQL 01110375 Page 7 11/26101 9:24:35 AM HOUSTON LABORATORY SSBO INTERCHANGE ORIVE HOUSTON, TX 77054 􀁾􀁓􀁦􀁇􀀡􀁌􀀷􀀠(713) 680-0901 Client Sample 10: Middle DI West Collected: 1118101 12:40:00 SPl Sample 10: 01110375-06 Site: 6-0275,21044625 AnafyuslMethod Result Rep.Llmit Oil. Factor QUAL Date Analyzed Analyst Seq. II POLYNUCLEAR AROMATIC HYDROCARBONS MCl SW831 0 Units: ug.'Kg Acenaphthene SO 66 20 11/19101 8:48 YN 914603 Acenaphthylene NO 66 20 11/19101 8:46 YN 914803 Anthracene NO 660 200 11119101 9:29 YN 914604 Benz(a)anthraceno NO 660 200 11/191019:29 YN 914604 Benzo(a)pyrane NO 66 20 11/19/018:48 YN 914603 Benzo(b)fluoranthene NO 66 20 11/19101 8:48 YN 914603 Benzo(g,h,i)perylene NO 66 20 11/19101 B:48 YN 914803 Banzo(k)ftuoranthena NO 66 20 11/19101 8:48 YN 914603 Chrysene NO 66 20 11/19101 8:48 YN 914603 Oibenzo{a,h)anthracene NO 66 20 11/19101 8:48 YN 914803 FJuoranthene NO 660 200 11119/01 9:29 YN 914604 Fluorene 960 66 20 11119101 8:48 YN 914803 Indeno{ 1 ,2,3-<:d)pyrene NO 66 20 11119/018:48 YN 914603 Naphthalene 1200 660 200 11/19101 9:28 YN 914604 Phenanthrene NO 660 200 11119101 9:29 YN 914604 Pyrene NO 8BO 200 11119101 9:29 YN 914604 Surr. 1-FluoronaphUlalene 0 % 41·97 20 11119101 8:48 YN 91480S Surr: l-Ruoronaphthalana D % 41-97 200 11/19101 9:28 YN 914604 Surr: Phenanthrene-dl0 0 % 38-108 20 111191018:48 YN 914603 Surr. Phenanthrene-dl0 0 % SS-I08 200 11119101 9:29 YN 914604 Benzene 100 100 909230 Ethylbenzana 1500 100 100 11114/01 15:40 909230 Toluene 2SOO 100 100 11/1410115:40 TM 909230 Xylenas,Tolal 6200 100 100 11114101 15:40 TM 909230 Surr: 1,4-Difluorooonzene 122 % 59-127 100 11114101 15:40 TM 909230 Surr: 4-Bromofluorobenzene 134 % 48-156 100 11/1410115:40 TM 908230 TPH TEXAS 1005 MCl TNRCC1005 Units: mg/K9 (:6.C12 230 50 1 11114101 17:52 AM 909156 >CI2-038 550 50 1111410117:52 AM 909156 >C28·C35 ND 50 11114101 17:52 AM 909156 Total TPH (C6-035) 780 50 11/1410117:52 AM 908156 Surr: l-Chlorooctane 131 MI % 􀀭􀀽􀀷􀀺􀀺􀀺􀀺􀀰􀀮􀀭􀀺􀀱􀀺􀀺􀀳􀀰􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀺􀀭􀀭􀀭􀀺􀀭􀀭􀀭􀀭􀀭􀀭􀀺􀀽􀀭􀀧􀀷􀀮􀀧􀀭􀀺􀀭􀁃􀀭􀀽􀀭􀀽􀀺􀁃􀀭􀀭􀀺􀀭􀀺􀀭􀀧􀀺􀀭􀀭􀀭􀀭􀀺􀀢􀀺􀀭􀀽 􀀧􀀺􀀧􀀺􀀺􀀻􀀻􀀻11/1410117:52 AM 908156 􀁳􀁾􀁵􀀽􀁾􀁾􀀮􀁏􀀽􀀮􀁾􀁔􀁥􀀽􀁱􀁭􀁾􀁥􀁮􀀽􀀽􀁾􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀁉􀁾􀀧􀀷􀁾􀁾􀂷􀁾􀁾􀁾􀀷􀁾􀁾􀁾􀀱􀁾􀀳􀁾􀀰􀀭􀀭􀀭􀀭􀀭􀀭􀀭1 11/1410117:52 AM 908156 !prep Method ;TNRCC 1005 Sonia West Project Manage' Qualifiers: NOIU • Not Oetected at the Reporting Limit >MCL • Result Over Maximum Contamination 􀁌􀁬􀁭􀁩􀁾􀁍􀁃􀁌􀀩􀀠B • Analyle delactecl in the associated Method Blank 0-Surrogate Recovery Unreportabla due to Dilution •• Surrogale Recovery Outside Advisable QC Limits MI • Matrlx Interference J • EsUmaled Value between MDL and PQL 01110375 Page 8 11126101 9:2CI2-C28 >C28-C35 Total TPH (C6-C35) Surr: 1-Chlorooctane Surr. 0-Terphenyl ND 40 ND ND 109 122 ND ND ND ND 110 105 % % % % 25 25 25 25 59-127 48-156 50 50 50 50 70-130 70-130 MCl MCl SW8021B 25 25 25 25 25 25 TNRCC 1005 Units: uglKg 11/13/01 15:23 TM 11/1310115:23 TM 11/1310115:23 TM 11/13/0115:23 TM 11/1310115:23 TM 11/1310115:23 TM Units: mglKg 11114/01 18:03 AM 11/14/0118:03 AM 11/14/01 18:03 AM 1111410118:03 AM 11/14/0118:03 AM 11/14/0118:03 AM 907969 907969 907969 907969 907969 907969 909157 909157 909157 909157 909157 909157 Prep Method TNRCC 1005 Prep Date 11/0912001 16:41 Prep Initials J F Sonia West Project Manager Qualifiers: ND/U -Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Limit(MCL) 8 -Analyte detected in the associated Method Blank o -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery Outside Advisable ac Limits MI -Matrix Interference J -Estimated Value between MDL and POL 01110375 Page 9 , 1126101 9:24:39 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample 10: Diesel 01 Collected: 1118101 1:30:00 SPL Sample 10: 01110375-08 SlIe: 6-0275,21044625 Analyses/Method Result Rep.Llmit Oil. Factor QUAL Date Analyzed Analyst Seq. # PURGEABLE AROMATICS Benzene ND 50 Mel swa021B 50 Units: uglKg 11/10101 20:56 TM 904744 Ethylbenzene 110 50 50 11110101 20:56 TM 904744 Toluene Xyienes,Tolai 190 490 50 50 50 50 11/1010120:58 11110101 20:56 TM TM 904744 904744 Surr: 1 􀁁􀁾􀁄􀁬􀁦􀁬􀁕􀁏􀁦􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠120 % 59-127 50 11110101 20:56 TM 904744 Surr: 4-Bromofluorobenzene 111 % 48-156 50 11/1010120:56 TM 904744 TPH TEXAS 1005 C6-C12 ND 50 MeL TNRCO 1005 Units: mglKg 11/1410118:14 AM 909158 >CI2-C28 ND 50 11/14101 18:14 AM 909158 >C2&-035 NO 50 11/1410118:14 AM 909158 Tota! TPH (C6-C35) ND 50 1 11/1410118:14 AM 909158 Surr: 1-Chlorooclane 112 % 70-130 1 11/14/0118:14 AM 909158 Surr: o-Terphenyl 105 % 70-130 1 1111410118:14 AM 909158 IPrep Me1hod iprep Date IPrep InitialsI trNRCC 1005 IJ F I Sonia West Project Manager Qualifiers: NDIU -Not Detected at the Reporting limit >MCl -Result Over Maximum Corrtsmlnation Limlt{MCl) B -Analyla detected in the associated Method 􀁂􀁬􀁡􀁮􀁾􀀠D -Surrogate Recovery Unreportable due to DiluUon • -Surrogate Reeove!)' Outside Advisable QC limits MI -Matrix Interference J -Estimated Value between MOL and pal 01110375 Page 10 11J2M.l1 9:24:41 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample ID: SE 01 Collected: 11/8/01 1;40;00 SPL Sample ID: 01110375-09 Site: 6-0275,21044625 AnalysesIMethod Result Rep.Llmlt Oil. Factor QUAL oate Analyzed Analyst Seq. II MCl SW8021B Benzene 160 so SO 11110101 21:27 TM 904747 􀁐􀁕􀁒􀁇􀁅􀁁􀁂􀁌􀁅􀁁􀁒􀁏􀁍􀁁􀁔􀁾􀁉􀁃􀁓􀁾______􀁾􀁾____􀁾􀁾__􀁾􀁾____􀁾􀁾􀁾􀀠Unit s: u9!Kg Ethylbenzene 720 so SO 11110101 21:27 TM 904747 Toluene 1400 so SO 11110101 21:27 TM 904747 Xyienes.Total 2850 50 50 11/10/01 21:27 TM 904747 Surr: 1.4-Difluorobenzene 143MI % 59-127 50 11110101 21:27 TM 904747 50 1111010121:27Sun: 4-Bromofluoroben'-z'-ene----'-'-=--::-:---':::-:-::::---------::::.---120 % 48-166 TM 904747 TPH TEXAS 1005 Mel THRee 1005 Units: m9!Kg G&C12 ND SO 1111410118:24 AM 909159 >C12-C28 NO so 1 11/1410118:24 AM 909159 >C28-C35 NO 50 1 1111410118:24 AM 909159 Total TPH (C6-C35) ND 50 1111410118:24 AM 909159 SUIT: 1-Chlorooctane 113 % 70-130 1111410118:24 AM 909159 SUIT: o-Terphenyl 107 % 70-130 130 1111410118:24 AM 909159 Prep Method 'Prep Date Prep Initials, "T,-,N:..:R.::.CC.:;...:10.:::0:.:5'----.J11/0912001 16:41 J_F Sonia West Project Manager Qualifiers: NDIU -Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Limlt(MCL) B -Analyte detected In the associated Method Blank o . Surrogate Recovery Unmportable due to Dilution • -Surrogate Recovery Outside Advisable QC Limits MI 􀁾􀀠Matrix Interierence J -Estimated Value between MOL and POL 01110375 Page 11 11126101 9:24:43 AM HOUSTON LABORATORY 6860 INTERCHANGE DRIVE HOUSTON, TX 77054􀁾􀁾􀀷􀀠(713) 660·0901 Client Sample 10: LT-3 North Collected: 11/8101 1:45:00 SPL Sample 10: 01110375·10 Site: 6-0275.21044625 Analyses/MelMod Result Rep.Llmit Oil. Facto, QUAL Date Analyzed Analyst Seq. # PURGEABlE AROMATICS MCl SW8021B Units: ugfKg Benzene 210 100 100 1111410113:05 TM 905649 Ethylbenzene 2100 100 100 11/1410113:05 TM 906649 Toluene 2600 100 100 1111410113:05 TM 908649 Xylene',Tolal 8700 100 100 11/14101 13:05 TM 908649 Surr: 1,4·Dilluorobenzene 135MI % 59·127 100 1111410113:05 TM 908649 Surr; 4-Bromofluorobenzene 146 % 48·156 100 11/1410113:05 TM 908649 TPH TEXAS 1005 C6-C12 ,C12-C28 ,C28·C35 Total TPH (CQ.C35) Surr: I·Chlorooctane SUIT: ""T erphonyl 390 380 NO 770 153MI 111 % % 50 50 50 50 7(J.130 7(J.130 MCl TNRCC 1005 1 1 Units: mglKg 11/1410118;35 AM 11/1410118:35 AM 11114/01 16:35 AM 11/1410116:35 AM 11/14/0118:35 AM 11/1410118:35 AM 909160 909160 909160 909160 908160 909160 Prep Method TNRCC 1005 :Prep Dale ;111091200116:41 41 :Prep 􀁉􀁮􀁲􀁮􀁡􀁬􀁳􀁾􀀠SOni. West P,oject Manager Quafifiers: NOIU • Not Detected at the Reporting Limit ,MCL • Result Ove' Maximum Contamination Limlt(MCL) B • Analyle detected in the associated Method Blank o . Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery Outside Advisable OC limits MI • Mabix Intelierenee J. Estimated Value between MOL and POL 01110375 Page 12 11120019:24:45 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample 10: SP-l Collected: 11/8/01 2:05:00 SPl Sample 10: 01110375-11 Site: 6-0275,21044625 Analyse.lMethod Result Rep.Limit DII_ Factor QUAL Date Analyzed Analyst Seq,# PURGEABlE AROMATICS MCl SW8021B Units: uglKg Benzene ND 10 10 11/10101 4:39 TM 904454 Ethylbenzene 40 10 10 11/10101 4:39 TM 904454 Toluene 60 10 10 11/10101 4:39 TM 904454 Xylenes,Total 181 10 10 11/10101 4:39 TM 904454 Surr: 1,4·Difluorobenzene 125 % 59-127 10 11/101014:39 TM 904454 Surr: 4-Bromofluorobenzene 124 % 48-156 10 111101014:39 TM 904454 TPH TEXAS 1005 MCl TNRCC 1005 Units: mglKg C6-CI2 ND 50 11/14/01 18:46 AM 909161 >CI2-C28 ND 50 11/14/01 18:46 AM 909161 >C28-C35 ND 50 11/14/01 18:46 AM 909161 Total TPH (C6-C35) ND 50 11/14/01 18:46 AM 909161 Surr: 1-Chlorooctane 110 % 70-130 11/14/01 18:46 AM 909161 Surr: o-Terphenyl 106 % 70-130 11/14/01 18:46 AM 909161 Prep Method Prep Date Prep Initials TNRCC 1005 11/09/2001 16:41 J F Sonia West Project Manager Cualifiers: ND/U -Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Limit(MCL) B -Analyte detected in the associated Method Blank o -Surrogate Recovery Unreportable due to Dilution * -Surrogate Recovery Outside Advisable QC Limits MI -Matrix Interference J -Estimated Value between MDL and POL 01110375 Page 13 11/26101 9:24:47 IW. HOUSTON LABORATORY 8SS0 INTERCHANGE DRIVE HOUSTON, TX 77064􀁕􀀺􀁾􀀷􀀠(713) 660-0901 Client Sample 10: SP-2 Collected: 11/8/012:10:00 SPl Sample 10: 01110375-12 Site: 6-0275,21044625 AnalysesIMelhod Result Rep.LImit Oil. Factor QUAL Date Analyzed Analyst Saq,# PURGEABlE AROMATICS MCl SW8021B Units: ugIKg Benzene ND 1 11/1410115:10 TM 909229 Ethylbenzene ND 1 1111410115:10 TM 909229 Toluene ND 1111410115:10 TM 909229 Xylenes,Tole1 Surr: 1,4-Difluorobanzene 6.1 121 % 1 59-127 11/14/0115:10 11/1410115:10 TM TM 909229 909229 SUff: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁲􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁡􀁮􀁥� �121 % 48-156 1 1111410115:10 TM 909229 TPH TEXAS 1005 MCl TNRCC 1005 Units: mg/Ks C6-G12 56 50 1 11/1410118:57 AM 909162 >C12·C28 51 50 1 11/1410118:57 AM 909162 >C28-C35 ND 50 1 11114/01 18:57 AM 909162 Tolel TPH (C6-C35) 107 50 11114/0118:57 AM 909162 Surr: l·Chloroootane 114 % 7()"130 11/1410118:57 AM 909162 Surr:o-T erphenyl 108 % 7()"130 1 1111410118:57 AM 909162 Sonia West Project Manager Qualifiers: NDIU -Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Limil(MCL) B -Analyte detected in the associated MethOd Blank D • Surrogate Recovery Unreportabla due to Dilution • -Surrogate Recovery Outside Advisable QC Limits Mi • Matrix Interference J • Estimaled Value between MDL and POL 01110375 Page 14 11126101 9:24:4& AM HOUSTON lABORATORY 8880 INTERCHANGE ORIVE HOUSTON. TX 77054 (713) 660·0901 Client Sample ID: SP-3 Collected: 11/8/012:15:00 SPl Sample ID: 01110375-13 Site: 6'()275,21044625 AnalyseslMethod Result Rep.Limit Oil. Factor QUAL Date Analyzed Analyst Seq. # PURGEABlE AROMATICS MCl SW8021B Units: uglKg Benzene NO 5 5 11113101 9:35 TM 906992 Eihylbenzene NO 5 5 11/13101 9:35 TM 906992 Toluene NO 5 5 11/13101 9:35 TM 906992 Xyienea,Total NO 5 5 11/131019:35 TM 906992 Surr: 1,4·0ifluorobenzene 106 % 59·127 5 11/13101 9:35 TM 906992 109 0/0 411-156 5 11/13/019:35 TM 906992 TPH TEXAS 1005 MCl TNRCC 1005 Units: mglKg C6-C12 NO 50 11/14101 19:08 AM 909163 >CI2·C28 NO 50 11/1410119:08 AM 909163 NO 50 11/14101 19:08 AM 909163 Total TPH (C6-C3S) NO 50 1 11/1410119:08 AM 909163 Surr: '·Chlorooclane 107 % 70·130 1 11/1410119:08 AM 909163 􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀁾􀁾􀁾􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀮􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀁾􀁾􀁾􀁾􀁾􀀭􀀭􀁾􀁾􀀽Surr: o-Terphenyl 101 0/0 70-130 1 11/1410119:08 AM 909163 prep Method :Prep Date Prep Initials ,TNRCC 1005 11/0912001 16:41 J F Sonia West 􀁐􀁲􀁯􀁬􀁥􀁣􀁴􀁲􀀮􀁬􀁾􀁦􀁉􀀢􀁾􀀢􀀧􀀠_____________________________ _________ Qualifiers: NDIU • Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Umit(MCL) B -Analyle delected in the associated Method Blank D -Surrogate Recovery Unreportable due to Dilution • -SUrrogate Recovery Outside Advisable QC Limits MI -Matrix Interference J • Estimelad Value between MOL and PQL 01110375 Page 15 1112e1Q1 S:'24:50 AM HOUSTON LABORATORY S880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample 10: SP-4 Collected: 11/8101 2:25:00 SPl Sample 10: 01110375-14 Site: 6-0275,21044625 AnalysesIMethod Result Rep.L1mlt 011, Factor QUAL Date Analyzed Analyst Seq_II PURGEABlE AROMATICS MCl SW8021B Units: uglKg Benzene ND 1 11/0910119:19 TM 904462 Ethylbenzene ND 11109/0119:19 TM 904462 Toluene ND 11109101 19:19 TM 904462 Xylenes,Totel 3.8 1 1110910119:19 TM 904462 Surr. 1 􀀬􀀴􀁾􀁄􀁪􀁦􀁴􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠145MI % 59-127 1 • 1110910119:19 TM 904462 SUrf; 4-Bromofluorobenzene 109 % 48-156 1 11/09/0119:19 TM 904462 TPH TEXAS 1005 MCl TNRCC1005 Units: mglKg C6-C12 NO 50 1 11114101 19:19 AM 909164 >C12-C28 130 50 1 1111410119:19 AM 909164 >C28-C35 Total TPH (C6-C35) Surr: 1-Chlotooctane Surr: 0-Te'Phenyi NO 130 109 110 % % 50 50 70-130 7()-130 1 1 11/14101 19:19 11114/0119:19 11114/0119:19 11114101 19:19 AM AM AM AM 909164 909164 909164 909164 Preg Method !TNACC 1005 eril2 Dat!i 111091200116:41 I􀁐􀁲􀁾􀁑􀀠􀁉􀁏􀁩􀁬􀁬􀁾􀀡􀁩􀀠:J F Sonia West Proje<:t Manager Qualifiers: ND/u -Not Detected at the Reporting Limit >MCL -Aesult Over Maximum Contamination Umit(MCL) B -Analyle detected in the assOC12-C26 190 50 1 11/14/0119:30 AM 909167 NO 50 1 1111410119:30 AM 909167 190 50 108 % 70·130 Total TPH (C6-C35) . SUIT: 􀁉􀀮􀁃􀁨􀁬􀁯􀁲􀁯􀁯􀁣􀁴􀁡􀁮􀀭􀁥􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀢􀀺􀁣􀀭􀁾 􀀬􀀭􀀽􀁾􀀻􀀭􀀭􀀭--_... SUIT: 0-Terphenyl 108 % 70·130 1 11114101 19;30 1111410119:30 11114101 19;30 AM AM AM 909167 909167 909167 Prep MtlIttod ,TNRCC 1005 Prep Date 1110912001 16:41 ,Prep Initials: 'J_F 􀁾􀁾ak,,=<=;;:; Sonia West --------------------------􀁐􀁲􀁯􀁾Manager Qualifiers: NDIU· Not Detected at the Reporting Limit >MCL -Rasult Over Maximum Contamination UmIt(MCL) B -Analyle delected in the associated Me1hod Blank D -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery Outside Advisable OC limits MI -Malrix Interference J -E.tlmated Value between MOL and POL 01110375 Page 17 11126A}1 9:24:54 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample 10: SP-6 Collected: 11/8101 2:35:00 SPl Sample 10: 01110375-16 Site: 6-0275,21044625 Analyses/Method Result Rep.Limit Dil. Factor QUAL Date Analyzed AnalYst Seq. I PURGEABlE AROMATICS MCl SW8021B Units: ug/Kg Benzene ND 25 25 11/1310116:55 TM 907970 Ethylbenzene ND 25 25 1111310116:55 TM 907970 Toluene ND 25 25 11/1310116:55 TM 907970 )(ylenes, Total 114 25 25 1111310116:55 TM 907970 Surr: 1.4-0ifluorobenzene 102 % 59-127 25 11/1310116:55 TM 907970 SUIT: 4-Bromofluorobenzena 109 % 48-156 25 11/1310116:55 TM 907970 TPH TEXAS 1005 MCl TNRCC 1005 Units: mgiKg C6-CI2 ND 50 11/14101 19:41 AM 909169 >CI2-C28 79 50 11114101 19:41 AM 909169 >C28-C35 ND 50 11/1410119:41 AM 909169 Total TPH (C6-C35) 79 50 11/1410119:41 AM 909169 SUIT: l-Chlorooctane 109 % 70-130 11114101 19:41 AM 909189 Surr. o-Terphenyl 106 % 70-130 1111410119:41 AM 909169 􀀺􀁰􀁲􀁥􀁾􀀠Method PrgQ !&!g 􀁐􀁲􀀡􀁩􀁕􀁾􀀠􀁉􀁮􀁩􀁕􀁾􀁉􀂧􀀬􀀠TNRCC 1005 1110912001 16:41 JJ Sonia West Project Manager Qualifiers: NDIU -Not Detected at the Reporting Umil >MCL -Result Over Maximum Coniaminatlon Umlt(MCL) B -Analyle detected in the associated Method Blank D -Surrogate Recovery Unreportable due to Dilution • -Surrogate Recovery OulSide Advisable OC Umlls MI -Matnx Interference J -Estimated Value between MDL and POL 01110375 Page 18 i li26f01 9:24:56 AM HOUSTON LABORATORY 8880 INTERCHANGE ORIVE HOUSTON. TX 77054􀁾􀁾􀀷􀀠(713) 680-0801 Client Sample ID:lT-5 Collected: 11/8101 2:50:00 SPl Sample ID: 01110375-17 Site: 6-0275,21044625 AnalyseslMethod Result Rep.Llmlt DII. Factor QUAL Date Analyzed Analysl Seq. II PURGEABlE AROMATICS MCl SW8021B Units: u!!!K!l Benzene NO 10 10 11/09/01 20:50 TM 904465 Ethylbenzene 250 10 10 11/09/01 20:50 TM 904465 Toluene 220 10 10 11109/01 20:50 TM 904465 Xylene., T olal SUrf: 1. 􀀴􀁾􀀰􀁩􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠1660 196MI % 10 59-127 10 10 . 11109/01 20:50 11109/01 20:50 TM TM 904465 904465 SUIT: 􀀴􀁾􀁂􀁲􀁯􀁭􀁯􀁦􀀱􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠135 % 012-028 NO 50 11/14101 20:13 AM 909175 >028-C35 Total TPH (06-035) NO ND 50 50 1 11114/01 20:13 11/14101 20:13 AM AM 909175 909175 Sun: l-Chlorooctane 109 % 70-130 1 11/1410120:13 AM 909175 SUrf: 0-Te1Jlhenyl 106 % 70-130 11/14/0120:13 AM 909175 'Prep Method Prep Date TNROO 1005 11/09/2001 16:41 Sonl.West Project Manager Qualifiers: NDIU -Not Delected at the Reporting L1mil >MCl· Rasult Ovar Maximum Contamination L1mlt(MOl) 8 -Analyle detected In the associaled Mathod Blank o -Surrogate Recovery Unreportable due to Dilution • -Surrogate Reccvary Outside Advisable QC L1mlls MI· Matrix Interference J -EstlmaUld Value between MOL and POL 01110375 Page 19 11126101 9::24:57 PM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Client Sample 10: L T-6 Collected: 11/8/01 2:55:00 SPl Sample 10: 01110375-18 Site: 6-0275,21044625 AnalysesIMethod Resull Rep.Urn!t Oil. Faclor QUAL Date Analyzed Analyst Seq. # PURGEABlE AROMATICS Benzene 5.5 5 MCl SW8021B 5 Units: ug/Kg 11/09101 20:20 TM 904464 Elhylbanzene NO 5 5 11/09101 20:20 TM 904464 Toluene NO 5 5 11/09/01 20:20 TM 904464 Xylenes,T alai NO 5 5 11/09101 20:20 TM 904464 SUn': 1􀀬􀀴􀁾􀁄􀁩􀁦􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠128MI % 59·127 5 11/09101 20:20 1M 904464 Surr. 4-8romofluorobenzene 116 % 48-156 5 11109101 20:20 TM 904464 TPHTEXAS 1005 CB-CI2 NO 50 MCl TNRCC 1005 Units: mgIKg 11/14101 20:24 AM 909176 >C12-C28 NO 50 1 11/1410120:24 AM 909176 >C28·C35 NO 50 11/14/0120:24 AM 909176 Tolal TPH (CB-C35) NO 50 11/14101 20:24 AM 909176 Surr. 1-Chlorooclane 105 % 70-130 11/14101 20:24 AM 909176 Surr: o-Terphenyl 99.2 % 70-130 11114101 20:24 AM 909176 􀁾􀁐􀁲􀁥􀁰􀀠Mii!lJod Preo Date 'Prep Initiafs: iTNRCC 1005 il1/09l200116:41 J F Sonia West Project Manager Qualillers: NO/u -Not Detected at the Reporting Limit >MCL -Result Over Maximum Contamination Umit(MCL) B -Analyte detected In the associated Method Blank o -Surrogate Recovel)' Unreporlable due to Dilution • -Surrogate Reoovel)' Outside Advisable ac Limits MI -Matnx Interference J -EsIImated Value between MOL and PQl 01110375 Page 20 11126101 9:24:59 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 600·0901 Client Sample 10: LT-7 Collected: 11/8/01 3:00:00 SPL Sample 10: 01110375-19 Site: 6·0275,21044625 Analyses/Method Result Rep.Limit Oil. Faetor QUAL Date Analy.C12-G28 >C28-CS5 Surr: o--Terphenyl NO NO NO NO 110 108 % % 50 50 SO SO 70-130 70-1 SO MCL TNRCC 1005 1 1 UnHs:mgIKg 11114101 20:35 AM 11/14101 20:35 AM 11/14101 20:35 AM 11/14101 20;35 AM 11/14101 20:35 AM 11114/01 20:35 AM 909177 909177 909177 909177 909177 909177 ,Prep Method ;TNRCC 1005 Prep Date 111091200118;41 Prep Initials: J F Sonia West Prolect.Manager Qualifiers: NDIU • Not Detected at the Reporting Umit >MCL -Result Over Ma>lmum Contamination Llmlt{MCLJ B • Analyte detected in the associated Method Blank o -Surrogate Recovery Unreportable due to Dilution •• Surrogate Recovery Outside Advisable OC Limits MI· Matrix Interference J • Estimated Value between MOL and POL 01110375 Page 21 11ti$101 9'.25:01 AM Quality Control Documentation 01110375 Page 22 11/2M)1 9:115:02 AM HOUSTON LABORATORY aeao INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobl1 5090275 􀂣􀁲􀁾􀀷􀀠Analysis: TPH Texaol0OS WorkOrder: 01110375 Method: TNRCC 1005 Lab Batch 10: 16103 RunlD: Analysis Date: Preparaffon Date: Method Blank HP_8_0111140-909147 Units: mg/Kg 111141200116:14 Analyst: AM 11/09/200116:41 Prep By: J5 Method TNRCC 1005 Sample. in Analytical Batch: Lab Sample 10 Client Sample ID 01110375-01 A NWDI 01110375-02A LT-l South 01110375-03A NE-OI 01110375-04A Vapor LT-NorIh 01110375-03A LT-2-Soulh 01110375-06A Middle 01 West 01110375-07A LT-4 North 01110375-06B Diesel 01 01110375-09A SE 01 01110375-10A LT-3 North 01110375-11A SP-l 01110375-12A SP-2 01110375-13A SP-3 0111 0375-14A SP-4 01110375-15A SP-5 01110375-16A SP-6 01110375-17 A LT-5 01110375-18A LT-6 01110375-19A LT-7 Laboratorv Control Sample ILCS) RunlD: HP_8_0111140-909148 Units: mg/Kg Analysis Dale: 111141200116:25 Analyst: AM Preparation Dale: 1110912001 16:41 Prep By: J5 Method TNRCC 1005 Analyte Percent Lower Upper :Spike I Result Added ' Recovery Limit Limit ;Gi":i:62e 450 91 70 130500 C6-C12 500 95460 70 130: 1 Total TPH (C6-C35) 1000 93 70 130:930, ------.._-----_....._---􀀭􀀭􀀧􀀧􀀧􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀺􀀭􀀺􀀭􀀺􀀭􀀺􀀭􀀭􀀭􀀺􀀺􀀭􀀺􀀺􀀬􀀭􀀭􀀭􀀺􀀺􀀺􀀺􀀽􀀭􀀺􀀭􀀺􀀺􀀭􀀺􀀭􀀬􀀭􀀭􀀭􀀺􀀺􀀭􀁾􀀺􀀺􀀭􀀭􀀭􀀺􀀺􀀻 􀀭􀀺􀀭􀀭􀀽􀀽􀀽􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀂭Matrix Spike (MS) I Malrix Spike Ouplioate (MSO) Sample Spiked: 01110375-01 RunlD: HP_8_0111140.009150 Units: mg/Kg Analysis Date: 11/14/200116:46 Analyst: AM Preparation Date: 1110912001 16:41 Prep By: J5 Method TNRCC 100S aualifiers: NDIU -Not Detected al the Reporting Umlt MI -Matnx Interference B -Analyte detected in the aSSOCiated Method Blank 0-Recovery Unreportable due to Dilution J -Estimated value between MOL and PQL • -Recovery OUtside Advisable QC 􀁕􀁭􀁾􀁳􀀠The percent recoveries tor QC samples are correct as reported. Due to significant figures and 01110375 Page 23 rounding, tile reponed RPO may differ from the displayed RPO values but is correct as reported_ 11121W1 9;25:52 AM HOUSTON LASORATORY BBBO INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 ExxonMobil 5090275 Analysis: TPH Tex.s 1005 WorkOrder: 01110375 Method: TNRCCloo5 l.ab Batch ID: 16103 I ,>C12-C28 Analyle IC6.C12 􀁾TPH (Ce-C35) Sample Result 160 3301 MS Spike Added 500 500 I 490: 1000; MS Result I MS % ! MSD IRecovery , Spike ! Added 610! 88.61 500 570; 49.6' , 500 .. 1180i 69.0 'I 1000: MSD Result I MSD % i RPD 1 Recovery I 􀁒􀁐􀁾Ilow, IHighUmlt , limft ' Limit' I 6501 96.8: 8.65 20 701 􀀱􀀳􀁾􀀠1000; 135' 􀁾􀀲􀀮􀀵􀀧􀀠20 70' 130, 1650 1 􀀱􀀱􀀶􀁾􀀰􀀺􀀸􀀧􀀠1 20 701 130: """"Qualifiers: NDIU -Not Detected at the Reporting Umit MI-Matrix Interference B • Analyte detected in the associated Method Blank D Recovery Unreportable due to Dilution J -Estimated value between MDL and POL • -Recovery Outside Advisable OC Llmlls The percent recoveries for ac samples are correct as reported. Due to significant figures and 01110375 Page 24 rounding, the reported RPD may differ from the displayed RPD values but Is correct as reported. 111"26101 9:25:52 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX n054 (713) 660-0901 Quality Control Report ExxonMobil 5090275 Analysis: Purgeable Aromatics WorkOrder: 01110375 Method: SW8C21B Lab Batch 10: R47363 Method Blank Samples in Analytical Batch: RunlD: HP_O_011109A·902OB5 Units: uglKg Lab Samel!: 10 Client Samele 10 Analysis Date: 11/09/200111:53 Analyst: TM 01110375-11A SP-l 01110375-14A SP·4 01110375·17A LT·5 01110375·18A LT'5 Oi 110375·i 9A LT·7Analyle Result Rep Limit 8_ NO 1.0 Ethvlbenzeno Toiuene NO NO 1.0. 1.0 :Xyjenas Total Surr: 1 4-0lfIuorobenzene ND 97.7 1.0 7Q·13O Sul'r. 443romofluorobenzene 92.5 70·130 Laboratory Control Sample (LCS) RunlD: HP_0_OI1109MI02078 Units: uglKg Analysis Date: 111091200111:23 Analyst: TM Analyle Spike Added Result Percent Recovery Lower Limit Upper Limit Benzene 50 50 99 70 124 : Ethylbenzene 50 46 97 78 128 IToluene 50 49 99! 70. 123 iXylenes,Total 150 142 95 711 130. Matrix Spike (MS) I Matrix Spike Duplicate tMSO) Sample Spiked: 01110375·19 RunlD: HP_0_01 I I09A·913162 Units: uglKg Analysis Data: 1111712001 0:31 Analyst: TM Analyta 1 Sample MSiSpikeResult iAdded: MS Resun MS% Recovery MSD Spike Added MSD Result MSD% Recovery . RPD RPD Limit Low Limit High Limtt Benzene NO! 2( 8.7 43.6 20 11 56.41 25.6 34 35 139 Ethylbenzene ND 2( 8.2 38.2 20 10 49.3: 25.3 35 31 137 ,Toluene ND 20 8.3 41.4 20 11 54.2 26.7 28 31 137 IXylenes,ToIal ND 60 22 36.7 60 29 48.3 27.5 38 19 144 Qualifiers: ND/U • Not Detected at the Reporting Limit MI • Matrix Interterenee B • Analyle detected In the associatad Method Blank o -Recovery Unreportable due to Dilution J . Estimated value between MOL and POL •• Recovery Oulslde Advlsabla QC Limils The percent recoveries for QC samples are correct as reported. Due to significant figures and 01110375 Page 25 rounding, the reported RPD may differ from the displayed RPD values but is cornect as reported, 11J2S1019:25:59M1! HOUSTON lABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-0901 􀂣􀁲􀁾􀀷􀀠ExxonMobii 5090275 Analysis: Purgeable Aromatics WorkOrder: 01110375 Method: SWS021a Lab aatch ID: R47469 Method alank Samples In Analytical Satch: RunlD: HP_O_Oll110A-904736 Units: uglKg Lab Sample ID Cljent Sample JO Analysis Date: 1111012001 9:42 Analyst TM 01110375-02A LT-1 South 01110375-05A LT-2-South 01110375-0BA Diesel 01 0111037S-09A SEDI Analyle Aesult Rep limit Benzene 􀁅􀁴􀁨􀁾􀁢􀁥􀁮􀁺􀁡􀁮􀁥􀀠ND NO 1.0 1.0 Toluene ND 1.0 iXvlenes Tota! I NO 1,01 .?urr. 1 4-Difluorobanzene I, 99"41SUIT: 4·Bromofluorobenzane r 913,0 70,130ri Laboratory Control Sample (LCS) RunlD: HP_O_011110A-904734 Units: ugIKg AnalYSis Date: 11110120019:12 Analyst: TM j Analyle I Spike , Added Result Percent Aecovery Lower Limit Upper Limit iBenzene 1 50 44 89 70 124 IEthylbenzene 50 44i BB 7B 128 IToluene 1 SOi 44 B8 70 1261 IXylenes,Tolal I 150i 131: 87 71 130, ...􀁾􀀠Matrix Spike IMS) I Matrix Spike Duplicate (MSDI Sample Spiked: 01110324-16 AunlD: HP_O_011110A-913136 Units: uglKg Analysis Date: 11117/20015:05 Analyst TM SampieAnalyte MS MS Aesult I MS% MSD% RPD !APD, 1 Low i HighMBD.I MBO Result '! Result SpikeSpike Recovery iLimit, Umit : LimitIRecoveryAdded Added !, ! : Ii 15i 72,020 201 15, 73.4IBenzene I NO 1.911 34 351 139 151 75,9 16iEthyJbenzene NO 20 2.58, 35 31j 131'201 ... 77.9 ;Toluene NO 20. 151 74.3 201 16: 76.0 2,34' 28 31 1 1371 ,Xytenes,T01al NO! 60 451 75.0 601 461 76_7' .. 2.201 38 􀀱􀀹􀁌􀁾􀀠QuaUfiers: NDIU· Not Detected at the Reporting Limit MI 􀁾􀀠Matrix Interference B -Analyte detected in the associated Method Blank o -Recovery Unreportable due to Dilution J -Estimated value between MOL and POL •• Recovery Outside Advisable OC Limits The percent recoveries for QC samples are correct as reported. Due to significant figures and 01110375 Page 26 rounding, the reported RPD may diNer from the displayed APO values but is correct as reported, 11/26101 9:26:(l6AM HOUSTON LABORATORY BBBO INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) OO().Q901 ExxonMobii 5090275 Analysis: PurgeabJe Aromatics WorkOrder: 01110375 Method: SW8021B Lab Batch 10: R47597 Method Blenk Samples In Analytieal Bateh: RunIO: HP_O_011113A-9009S2 Units: uglKg Lab Sam!!le 10 Client Sam!!le 10 Analysis Date: 11/13120016:33 Analyst: TM 01110375-03A NE-OI 01110375-04A Vapor LT-North 01110375-07 A LT-4 North Analyle I Result Rep Llmijl Benzene 1 ND 1.0 Eth benzene ND Toluene ND 1 􀁾􀁟􀁮􀁥􀁳􀁔􀁯􀁴􀁡􀁬􀀠NDI 1 StitT. 1 4·DifluorobeOl:sne 96.7: 7().1 Surr: 4-Bromofluorobenzena 92.31 7tH 01110375-13A SP-3 01110375-15A SP-5 01110375-15A SP-6 Laboratory Control Sample (LeS) RunlD; HP_O_011113A-1lOS978 Unil.: ug/Kg Analysis Date: 11/13120016:02 Analyst: TM Analyte Result Percent Reoovery Lower Umi! Upper Umit Benzene 45 89' 70 124 E!hylben.ene Toluene 50 44 45 89 89 78 70 128 126 IXylenes,Total 150, 131 87 71 130 Matrix Spike CMS) I Matrix Spike Duplicate (MSO) Sample Spiked: 01110375-03 RunID: HP_O-'l11113A-!l13159 Units: uglKg Analysis Date: 11/1/l12OO1 21 :29 Analyst: TM Analyte Sample MS MS 􀁒􀁥􀁳􀁵􀁾􀀠I MS % MSD MSD 􀁒􀁥􀁳􀁵􀁾1 MSD% RPD RPD ILow High Recovery Umit : Umit LimitResult Spike Recovery: Spike 'I' Added , I Added 􀁢􀁣􀀽􀀭􀁣􀀭􀀭􀀭􀀭􀀭􀀭􀀫􀀭􀀭􀀭􀀭􀀻􀀺􀀻􀀻􀀺􀀻􀁴􀀭� �􀀭􀀻􀀻􀀺􀀻􀀻􀁉􀀭􀀭􀀭􀀺􀀻􀀭􀀻􀁴􀀭􀀭􀀽􀁩􀀭􀀭􀀭􀀻􀀻􀀻􀀻􀁬􀀭􀀭􀂷􀂷􀂷􀂷􀀭􀂷􀂷􀂷􀀭􀀭􀀻􀀺􀀻􀀻􀁉􀀭􀀭􀀭􀀭􀀻􀀻􀁾􀀻􀁟􀀻􀁯􀀻Benzene NO 20 141 67.6 20 14 67.9 0.539 34, 35 139 Ethylbenzen. NO 20 11 57.2 20 12 58.6 2.50 35 31 137 TOluene 2B 31 137 Xylene',Total NO 20: 121 57.5 2OJ-___􀀢􀀧􀀱􀀳􀁽􀀭􀀭􀁟􀁾􀀵􀀹􀀮􀀴􀀠3.26 NO 601 341 56.7 60 35 58.3 2.901 38 19 144 Qualifiers: NDIU -Not Detected at Ihe Reporting Limit M! -Matrix Interference B -Analyte detected in the associated Method Blank o • Recovery Unreportable due to Dilution J -EsHmated value between MOL and POL •• Recovery Outside Advisable OC Limits The percent recoveries tor QC samples are correct as reported. Due to significant figures and 01110375 Page 27 rounding, the reported RPD may differ from the displayed RPO values but is correct as reported. 111261019:26:13AM HOUSTON LABOAATORY 8880 INTERCHANGE DAIVE HOUSTON, TX 77054 Quality Control Report (71S) 880-0901 􀁾􀁾􀀷􀀠 ExxonMobil 5090275 An.lysis: Purgeable Aromatics WorkOrder: 01110375 Method: SWB021B Lab Balch 10: R47688 Method Blank Samples in Analytical Batch: AunlD: HP_O_011114A-llOB64S Units: ug/Kg Lab Sample 10 Client Sample 10 Analysis Date: 11/1412001 7:50 Analyst: TM 0111OS7S-01A NWDI AnalyteI IBenzaneIEthvlbenzene Toluene 􀀧􀁾􀁟􀁡􀁮􀁥􀁳􀀠􀁔􀁏􀁾􀀡.. SUIT: 1 􀀴􀁾􀁏􀁬􀁴􀁬􀁵􀁯􀁲􀁯􀁢􀁥􀁮􀁺􀁥􀁮􀁥􀀠SuO': 4·Bromo1Joorobenzene 0111037s.12A SP·2Result RepUmi NO 1.0 NO 1.0 ND 1.0' 0111OS7S-0M Middle 01 West 0111OS7S·10A IT·3 North , NO 1.0 98.5: lQ-1SQi 96.01 70·1301 Laboratory Control Sample (LCS) RunlD: HP_O_011114A-908644 Units: ug/Kg Analysis Date: 11/1412001 7:19 Analyst: TM Analyte Spike Added Aesult Percent Recovery lower Limit Upper Limit Benzene 50: 44 88 70 124, Ethylbenzene : 50 Toluene I 50 441 44 88 89 78 70: 128 "'12e Xyienes,Total I 1& 130 87 71 130 Matrix Spike eMS11 Matrix Spike Duplicate (MSD) Sample Spiked: 01110081-02 RunlD: HP_O_011114A-913156 Units: ug/Kg Analysis Date: 11/17120013:34 Analyst TM Analyte Sample I MS MSO MSD AesultMSAesuit MS% RPOMSD% IAPD low High Aesult : Spike Recov!lf)l Recovery ! Umit Umit UmitSpike i •Added Added: : IBenzene 15 72.9 20 15 77.2 5.72NDI 20 13934: 35 Elhylbenzene NDI 2Q: 15 72.8 201 15 77.4 6.12 137351 31 Tofuene : ND: 201 15' 75.4 201 16 79.8 5.65 28 31 1371 Xylene., T ota! NDI 601 44 73.3 60: 46 76.7 4.44 38 19 144: Qualifiers: ND/U • Not Detected at the RepOrting Limit MI -Matrix Interference 6 • Analyte dewcted in the associalad Method Blank D • Recovery Unreportable due to Dilution J -Estimaled value belween MDl and pal •• Recovery Outside Advisable OC UmilS The percent recoveries for QC samples are correct as reported. Due to signifICant figures and 0111OS7S Page 28 rounding, the reported APD may differ from the displayed RPD values but Is correct as reported. 11126/019:26!19AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 Quality Control Report (713) 660-{)901 £r-"":!'Z/ExxonMobil 5090275 Analysis: Polynuclear Aromatic Hydrocarbons WorkOrder: Ot110375 Method: SW831 0 Lab Balch 10: 15266 Method Blank Samples In Analylical Batch: RunlO: 2..0111186-914904 Units: ugJ1(g Lab Sample 10 Client Sample 10 Analysi. Date: 11/1812001 16:13 Analyst: YN 01110375-06A Middle 01 We.t Preparation Date: 1111612001 14:13 Prep By: Method Analyte Result IRep Limit ,Acenaohthene NO, 3.3: iAcenaohthvlene NO 3.3 'Anthracene ND 3.3' NO 3.3􀁾􀁾􀁢􀀩􀁦􀁬􀁵􀁯􀁭􀁮􀁬􀁮􀁥􀁮􀁥􀀠NO 3.3􀁉􀁊􀀿􀁾􀀢􀁮􀁺􀁯􀁬􀁯􀀮􀁨􀁊􀁽􀁯􀁥􀁍􀁥􀁮􀁥􀀠NO 3.3'􀁉􀁂􀁥􀁮􀁾􀁫􀁬􀀨􀁊􀁵􀁯􀁦􀁀􀀬􀁮􀁴􀁨􀁥􀁮􀁡􀀠iCh ..,. NO. 3.3, 􀀬􀁄􀁬􀁾􀀮􀀮􀀮􀁊􀀲􀁻􀁩􀁩􀁬􀀠h)aothracena NO 3.3 :Ruoranthene NO 3.S. Fluorene NO 3.31 NO 3.3􀁾􀁮􀁯1 2 3-cdlovrene NO 3.3􀁾􀁡􀁰􀁨􀁴􀁨􀁡􀁴􀁬􀀧􀁬􀁦􀁬􀁥􀀠ND 3.3􀁾􀁾􀀮􀁮􀁴􀁨􀁲􀁥􀁮􀁥􀀠NO 3.3Pvmoe 􀁾􀁵􀀺􀀱􀁾􀁆􀁬􀁵􀁯􀁲􀁯􀁮􀁡􀁰􀁨􀁴􀁨􀁡􀁬􀁥􀁮􀁡􀀠69.8 41·97 Burr: ?henanlhrene-d1O 74,71 38-100 Benz(a)anlhmcene . NO 3.3 ,Sanzo a)pyrena ND 3.3 Laboratory Control Sample (LCS) RunlO: 2..0111188·914905 Units: ugJ1(g Analysis Date: 111181200116:51 Analyst: YN Preparation Date: 11/1612001 14:13 Prep By: Method Analyte Spike Result Percent Lower Upper Added Recovery Umit limIt Acenaphthene : 16.7 13 75 29. 105i Acenaphthylene 16.7: 13 79 ....25: 119: Anthracene 16.71 12 73 25: 101 Benz(ajanthracene 16.71 14 84 26i 114' Benzo(ajpyrene 16.7! 16: 97 28: 114 Benzo(b)fluoranthene 16.7 141 86 29 118 8enzo(g,h,ijperylene 16.71 14: 85 22: 130 iBenzo(k)f1uoranthene 16.7! 14 84 30 120 Chrysene 16.7' 14 81 31 138 Dibenzo(a,h)anthracene 16.7: 14 81 27 120 Fluoranthene 16.7 13 75 28 110. Fluorene 16.7 12 73 27 105 Indeno(I,2,3-cdjpyrene 16.7 14 81 28 123: aualifiers: NO/U -Not Detected at the Reporting Limit MI -Matrix Interterence B -Analyte detected in the associated Method Blank o-Recovery Unreportable due 10 DiluUon J -Estimaled value between MOL and pal • -􀁾􀁥􀀼􀀺􀁯􀁶􀀮􀁲􀁹􀀠Outside Advisable QC Limits The percent recoveries for ac samples are correct as reported. Due to signiftcant figures and 01110375 Page 29 rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 11i26i01 9:26;25 AM HOUSTON LABORATORY 8880 INTERCHANGE DRIVE HOUSTON. TX 77054 Quality Control Report (713) 66().0901 ExxonMobil 5090275 Analysis: Polynuclear Aromatic Hydrocarbons Wo,kOrde" 01110375 Method: SW8310 Lab Balch ID: 16266 Laboratory Contrpl Sample ILCS) RunlD: 2_0111100·914905 Units: ugIKg Analysis Date: 111181200116:51 Analysi: YN Prepamtion Dais: 111161200114:13 Prep By: Melhod ! Analyle Spike IResult Added Percent Recovery Lower LimH Upper Limit INaphthaiene , 16.7: 12 69, 25 106: :Phenanthrene 16.7 13; 25761 11'1 tyrene I 16.71 13 78 27 11 51 Matrix Spike IMS) I Matrix Spike Duplicate (MSD) Sample Spiked: 01110375-06 RunlD: 2...01111 BB-Il14005 Units: ugIKg Anafysis Date: 111191200110:07 Analyst YN Prepamtion Dala: 111161200114:13 Prep By: J..L Metl10d SW3550B Analyle I Sample IMS ; MSRasuit MS% MSD MSD Result I MSD % RPDIRPD Result Spike Recovery Spike ! Recovery ! Umit !Added Added , , , Acenaphthene ND, 16.7 80 28.4 16.7 91 98.4i 110' 50 Acenaphthylene , ND 16.7, 29 176 .. 16.7 19 114· 43.0 50 Anthracene , , NDI 16.7 42 251' 16.71 43 260 ' 3.66 50 :Sanz(a)anthracene NO! 18.7 120. -433 ' 16.7. 200, 73.4 282' , 50 Benzo(a)pv,ene NO 16.71 18 107 ' 16.7 19 115" : 7.93 50, rBenzo(b)iiuoran1hene ND; 16.7i 1T 99.0 16.7 17 103 3.59 50 ND 15 ·1010' 16.7 16 Low, High Limit I Limit 91 991 4! 105; 14 831 24 115 21 92: 14 1351 1, 141'Benzo(g.h.l)pe,ylene 16.71 ·1000 ' i 0.526 1 50 iBenzo(k)tluoranlhena ND 16.7: 16 94.5 16.7 16 93.7: 0.8 􀀧􀀱􀀹􀁾􀀱􀁾􀁾􀀠Chrysene ND Dlbenzo(a.h)anthmcene 16.7! 83 225' 16.7 65 239' 6.26 50 3 171' NO 16.7 Fluoranthane ND 16.7 Fluorene 880, 16.7 ,lndeno(l.2.3-cd)pvrene , ND 16.7, !Naphthalene :Phenanthrene IPyrene 1200 16.71 ND 16.7 NO 16.71 ... 15' 16.t-844' 16 -843' rO.l43 3501 2180 ,. 16.7 170 1030· ,. 910, 147' 16.7' 1100' 1050' l' 14 83.7 16.7, 14 8S.3 3.07" 1200 ·66.3 ' 16.7 15001 1420 ' 220' 350 ·172 ' 16.71 450 375' 541" 160 62.7 16.71 140 ·15.2' ,328' 50 31 106i 50 8 126 50 1 ...;= 131 50 21 119 50 8 91 50 22 99i 501 3 128 Qualifiers: ND/U • Not Detected al Ihe Reporting Umit MI -Mellix Interlerence B • Analyle delected In the asSOCiated Method Blank D • Recovery Unreportable due to Dllullon J -Eedmalad value between MDL and POL .. -Recovery Outside Advisable QC Umits The percent recoveries for ac samples are correct as reported. Due to significant figures and 01110375 Page 30 rounding. 1I1e reporlad RPD may differ trom Ihe displayed RPD values bul is correct as reported. 1112t1101 9:26:25 AM Sample Receipt Checklist And Chain of Custody 01110375 Page 31 11/26101 9:26:26 AM HOUSTON LABORATORV 8880 INTERCHANGE DRIVE HOUSTON, TX 77054 (713) 660-0901 Sample Reoeipt Checklist Workorder: 01110375 Received By: OS Date and Time Received: 1119101 10:00:00 AM Carrier name: FedEx Temperature: 3 Chilled by: Water Ice .....-.._1. Shipping container/cooler In good condition? Ves 􀁾􀀠NoD Not Present D 2. Custody seals intact on shippping container/cooler? Ve. D No Not Present 􀁾􀀠3. Custody seals intact on sample bottles? Yes D NoD Not Present 􀁾􀀠4. Chain of cuslody present? Ves 􀁾􀀠NoD 5. Chain of custody signed when relinquished and received? Yas 􀁾􀀠NoD 6. Chain 01 cuslody agrees with sample labels? Ves D 􀁎􀁯􀁾􀀠I.Semple 10 NE 01 was written on COC twice, Sample 10 NW DI was received but not on coe 7. Samples in proper contalneribottle? Yes 􀁾􀀠NoD 8. Sample containers intact? Yes 􀁾􀀠NoD 9. SufficIent sample volume for indicated test? Yes 􀁾􀀠NoD 10. All samples received within holding time? Yes 􀁾􀀠No 11. Containerlremp Blank temperature In compliance? Yes 􀁾􀀠NoD 12. Water -VOA vials have zero headspace? Yes D NoD Not Applicable 􀁾􀀠13. Water· pH acceptable upon receipt? Yes No Not Applicabte 􀁾􀀠SPL Repr •••ntative:IWyatl, Neaundra Contact Date lit Time: 111 114/01 4:24:00 PM Client Name contected:F.IMs:=:rk=L=a=c:=h==========i Non Conformance : 1,Logged in NE 01 only one time, Also, logged in NW 01 wilh collection date and lime from container per NW Issues:i;:i:=';;:=;0;:;=:;=;==:==;==;=='=:====7:::::=::=:;;==:=:;;==;=='=:==;==;===:7==;==::;::::=;=: :;::::=:;;==:::;Client Instructions: Notified Mark of sample received, however, not listed on the chain of custody & informed him of sample which was listed twice on Ihe chain, Per Msrk analyze the sample 'NW 01' for BTEXITPH along with the other samples, 01110375 Page 32 11/261019:26:27 AM EXXON COMPANY, USA. ICHAIN OF CUSIDDY RECORD 000 \ \ 10"J15' ; 􀁾􀀠 I 5J AIWYSI$IIiQUBT: I _ &.xon engIRtlHJr;PL:eGo-flit I'hooe! 􀀷􀀡􀁾,.􀁾􀀠􀀬􀁾􀀠-"', _1A1E1ICIX) ! OmullantCo.N_: 􀁾􀁛􀀻􀀢􀀺􀀴􀁌􀁃􀁟􀀺􀀠/41ar,AL 􀁉􀁾􀁛􀁝􀀠i 􀁾􀀠1 1° :1'1 ? 0 ,J Q i \ 􀁾 PlIo",,; 􀀱􀀻􀀧􀀺􀁦􀁩􀁾􀀺􀀺􀀠_1HSt.e £4-C>S1-tr.,, 1'-a 0 D, i u , 􀁾􀀠I .., lJ( 2: 􀁾􀀡􀀠Iii Il! g 0IJ IJ 10t 2 1ft 􀁾􀁾􀀠RAS II: -FacilitvfStale 10 , (TN Only): 􀁾􀀠'" :;: i 0 􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠i AFE *(fenninal Onlyl: Con t Il"rOfeclf: 3'<.. 􀁾􀀠i :!i 0 􀁾􀀠i 1;' 􀁾􀀠i" .iIt LOCIlIian: t(/tL "'.-$..;C(ClIy}: 1;7J:,(f).J 􀁾􀀠'" i 􀁾􀀠􀁾􀀺􀀠􀁾􀀠􀁾􀀠'-0 􀁾(Stale): 0 0 ft 􀁅􀀠cd o SOT 􀁾􀁾􀀠􀁾􀀮􀁨􀀮􀀻􀁪􀀡􀀠􀀱􀀡􀁾􀀱􀁾􀁾􀁧􀀠 Consultant 􀁷􀁾􀀠A ease!; '" ci 7.,.10 􀁬􀁪􀁹􀁾􀀻􀁬􀀠S-'8 Ii i I' 􀁾􀀠2 􀁾􀀠iii ;:; t; !J 12 ;i 􀁾􀀠􀁾􀀠 s::: Sampled By: "::f-=:. L a 15 j w 8 II 9 f :e :! "1 g ; 􀁾􀀠:t.􀁾􀀠-. 􀁾􀀠􀀨􀀡􀀩􀀭􀁾􀀢􀁾􀁇􀁩􀀢􀀧􀁾􀁛􀁦􀀠t: ftIIIAtRlK 0 􀁾􀀠f 12:0 tw· 􀀭􀁾􀁾􀀠􀀮􀁾􀀠-􀀭􀀭􀁾􀀭•• -• 􀁾􀀠• ";"" 􀁾􀀮􀀠, 􀁉􀁾􀀠1#6:'" PI 􀁏􀀡􀁾􀀠X Ilce.':l' ..d l.r-./C.".,..-l. 􀁕􀁾􀀱􀁦􀁪􀀠. ". • Alt:=-1\ r -""U!. '...,.-1--""" r-􀁾􀀠LzI : \)_t'!O-LI _11. 1 􀁉􀁉􀀺􀁾􀀠, 11,-:' 􀁾􀁾􀁩􀀠􀀾􀁾􀀠, /+1.. 7. -s;.....u.. 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TX 770$.4 Ph' {713t 660·0&&1 F.., (7131 65tHl!l!5 Ph: , __-e77. -----EXXON COMPANY, USA. 􀁉􀀭􀀭􀀭􀁾􀀠.. l). ./"., /' 􀁾􀁾"J 􀁩􀀡􀀺􀀮􀀮􀀮􀀯􀁾Exxon Engineer: 􀁾􀀭􀀮􀀠􀁾􀁁􀀠Phone: Consultant Co. Name: 􀁾S'􀀺􀁾􀀠Contact: :n L" "",,,...;/'1 2" 0 vi Phone: 􀁦􀀧􀁦􀁩􀁾􀀣􀁲􀀻􀀱􀁪􀁽􀀮􀁾􀀠J1,{.>L.e EI}6 5/'{OtfA.Fax: " ::; '" rx= RAS #: -0 :)."l::S Facility IState 10 # (TN Only): ..YJ'J. ::a£AFE /I (Terminal Only): 􀁾􀀠􀁣􀁾􀁮􀁴Project II: J!2 Location: tf/tL f3 ("$ e!City): 􀁾􀀺􀁦􀁣􀀺􀀾􀀮􀀮􀁬􀀠(State): 􀁾􀁅􀀠0 C & 􀁾􀁾􀁾􀀠0 SOT Consultant WO} ,: ci -zjO!lie;,;2 S//􀁾􀁌􀀭Sampled By: tV""' -aU.;;, ili , --􀀭􀁾􀀭r-MATR'X 􀀭􀁾_ SAMPLE I.D. TIME COMP. GRAB H.n SOIL AIR OCHER 􀁄􀁁􀁾􀀠IAI£ PT f{td 􀁯􀁬􀁾􀁾􀀩􀀨􀀠X ICELr-/􀁾."..:t-/. .. Li:iD AI£"-1\ T 􀁨􀁴􀁬􀁾􀀠---, \)M.II... 􀁌􀁴􀀭􀁽􀀯􀀨􀀩􀁾􀁤􀀬􀀮􀁉􀀺􀁾􀁟􀁟􀁟􀀠'.-1 f.. "Z -􀀵􀀢􀁾􀀠:c: \lb i h1.,IJ/-l!. /)T-W"' ..J 􀁬􀀲􀀱􀁊􀁾􀀠-I-􀁾􀀠r.-24 HA. 72 􀁈􀁲􀀮􀁾􀀧􀀠􀁾􀀭􀁅􀁌􀁘􀁘􀀭􀁏􀀢􀀧􀁎􀁌􀀮􀀮􀁕􀀭􀁓􀀢􀀭􀁔􀀽􀀢􀀭􀁩􀁓􀁐􀁅􀁃􀁉􀁁􀁌􀀠DETECTION LIMITS (5 48 HR. 96 Hr. _' CONTRACT NO. Standard _ 'ConlaC1 US Prior S02317MOl SPECIAL REPORTING REQUIREMENTS REQUIREMENTS (Specify) to Sending SampleOther QA/QC Level 􀁾􀁉􀁡􀁮􀁤􀀧􀁲􀁤􀀠0 ClP 0 FAX 0 CUSTODY RECORD Relinquished By: 􀁾􀀠􀁃􀁾􀁁􀁉􀁎􀁏􀁆􀁃􀁕􀁓􀀱􀀰􀀰􀁙􀁒􀁅􀁃􀁏􀁒􀁏􀁎􀁏􀀮􀁏􀀩􀀠􀁜􀁜􀁏􀁾􀀱􀀩s:l ANALYSIS REQUest: "i (CHECK APPROPRIATE BOX) 0 􀁾􀀠􀁾􀀠 􀁾􀀠0 S 􀁾􀀠0 􀁾􀀠􀁾􀀠􀁾􀀠0 􀁾􀀠􀁾􀀠 􀁯􀁾􀀠Pi3 􀁾􀀺􀀺􀀻􀀠􀁾􀀠ill zg 􀁾􀁾􀁾iii 0 0 zOaj0 § ;;l 􀁾􀀠0 a: J!! 0 fl 􀁾􀀠Ii}<1J E i ffi" § .::. 0 fi! 􀁾􀀠0 0 0 0 􀁾􀀠􀁾􀀠􀁾􀀠It-;:; 0 g § -' 11"'-:1' 􀁪􀀭􀀭􀀭􀀭􀁾􀀫􀀠􀁪􀀭􀁟􀁾􀀠-􀁾􀀭􀁾􀀻􀀺􀀠'--1 􀁾􀀭􀀭􀀭􀀭􀀭􀁾􀀠 --cz. -􀀭􀁾􀁾􀀠􀁲􀀮􀁾􀁬􀁉􀀭􀁲􀁣􀁬􀀦􀁴􀀠..... 􀁾􀀠rJ!f'-!I-􀁾􀁉􀁉􀀽􀀠r-r-􀁉􀀭􀀭􀀭􀀭􀁾􀀠t c--I-I 􀁉􀀭􀁾􀀭􀀬􀀠\ 1PrJ 7"/O&s:' I) LAS USE ONLY Storage Localion 􀁾􀀠􀁾􀀠WORK 0i'lDER #: LAB WORK RELEASE #: Received By: o Received By: Dale Time IReceived By 􀁬􀁡􀁢􀁏􀀢􀀧􀁴􀁯􀁲􀁹􀁾􀀬􀀠1 \ 1'1/0 I cJ 􀁾􀀠"'!ay Bill 􀀣􀁾􀁾􀁾􀀠Cooler Temp: 1'00 pageJof? OTHER [] I􀁾􀀭􀁲􀁯􀀭􀁜􀀭􀀭􀀭􀀭􀁾􀀢􀀭􀁾􀀧􀀭􀀭􀀭􀀭􀀱􀀭􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠􀁾􀀠 g 0 0 􀁾􀀠0 1,* 8 􀁾􀀠!il ,,; D.s::: ;;l 0 􀁾􀀠􀁾􀀠􀁾􀀠 " 􀁾􀀠-'g >-, 􀁾􀀠0 J SHIP SAMPLES BACK TO: SPL INCORPORATED. 8680 Interchanae Drive. 􀁈􀁯􀁵􀁳􀁴􀀭􀁯􀁮􀀭􀀮􀀭􀀽􀁔􀀭􀀺􀀭􀀺􀁘􀀭􀀽􀀷􀀺􀀺􀀭􀀺􀀷􀀰􀀺􀀭􀀺􀁃􀀵􀀴􀀧􀀭􀀭􀀭􀀽􀀭􀁐􀁨􀀺􀀭􀀺􀀭􀀺􀀺􀀨􀀷􀀺􀀺􀀭􀀱􀀭􀀽􀀳􀁜􀀭􀀭􀀽􀀧􀀶􀀶􀁾􀀰􀀭� �􀀹􀀰􀀱􀀠Fax: (713\ 660-8975 Ph: 1-000·969·6775 I EXXON COMPANY, USA. CHAIN OF CUSTODY RECORD NO. 01\\03?S:age 􀁾􀁦􀁾􀀠ANALYSIS REaUEST: OTHER . If)􀁾L I'􀁾_" (CHECK APPROPRIiUE BOX)··rExxon Engineer: ur nllf111 Phone: . ... 00 -0 . Consultant Co. Name: Contact: 0 II! . 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UJ VI'}( 01 I') 111!11 //, Standard _ 'ContactUS Prior S02317M01 SPECIAL REPORTING REQUIREMENTS (Specify) LI\ll USE ONLY Lot # I Siorago Location Other to Sending Sampl$ . ......... _----_. 􀀭􀁾􀀠 Slandard 0 CLP 0 􀀺􀀺􀁾􀁉􀀠,I r/.x 0 0 FAX C-a-¥ WJREPORT WORKORDER.#_:__...___ LAB 􀁗􀁏􀁒􀁋􀁟􀀺􀁒􀁟􀀺􀀬􀁾􀁅􀀺􀁌􀀺􀁅􀀺􀁁􀀮􀀬􀁓􀀺􀀬􀀢􀁅􀀺􀀧􀀣􀀺􀀧􀀭___--j 􀁒􀁥􀁬􀁩􀀢􀀷􀁈􀁾􀁾􀁾􀁾􀀠 . 􀁊􀀯􀀯􀁒􀁴􀀯􀁬􀀯􀀯􀀮􀀮􀁔􀀻􀁾􀀯􀀠Received By: CUSTODY Rannquist ad BY: v '/D'1Ie Time Received By: RECORD I,I Relinquished By: Date Time Received By 􀁌􀁡􀀬􀀮􀀿􀁯􀁲􀁡􀁴􀁯􀀬􀀺􀁾􀀠n \' 19/01 (OcCI Way Bill D: nTA'II\'ll!,IlVJL. Cooler Temp: L-___________ ... , .. _ ......_"". 􀀭􀁾􀀭􀀢􀀧...􀁾􀀮􀀭􀀬_-.-.􀁟􀀭􀁟􀀭􀀢􀀭􀁾􀀭􀀬-..􀀭􀀬􀁾􀀭􀁾􀀭􀁾􀀭􀁾􀀭􀁾􀀭􀁾􀀭􀀮􀁔􀀭􀁾􀀭􀁾􀀭􀁍􀀭􀁮􀀭􀁮-,.-,.-..-.-••-.-\_'n--...;,-._-u_-'-.-..'-n-n=T:::v-=,-:- -,n'·."AL-="-:--h-''=7'=''''--'A"Rn.nQni--F,w-17131 660-8975 ...) Ph: 􀀱􀀭􀀸􀀰􀀰􀂷􀀹􀀶􀀹􀁾􀀶􀀷􀀷􀀵􀀠 EA Engineering, Science, and Technology APPENDIXC Waste Profiles and Disposal Documentation F:\Pro}\Ex:wn\sdM-0275\Reports\TEA Tank Excavation Report ALLIED WASTI! GENERATOR WASTE PROFILE SHEET Page lof2 Requested Disposal Facility: Waste Profile # an Allied Waste Company AWl Sales Rep: I. Generator Information Date: Generator Name: ExxonMobil Generator Site Address: 4191 Beltline Road CHy: Addison County: Dallas IState: TX Zip: 75244 State ID/Reg No: 0026323 State ApprovallWaste Code: (If appncablel SIC COde: Generator Mailing Address (if different): ExxomMobii P.O. Box 4552 City: Houston r:n..nh.. Hams IState: TX Zip: 77210-4552 Generator Contact Name: Dale L. Gomm Phone Number: 713-656-9219 IIa. Transporter Information Transporter Name: Alliance Trucking Transporter Address: 2010 Century ctr. Blvd. City: hving Phone Number: 972-445-1772 IFax Number: 713-656-9191 ....􀁾􀁾􀀭􀀭􀀭􀀭Transporter Contact Name: Jeff Clay State: TX Zip: 75062 state Transportation Number: lib. Billing Information Bill To: Exxon Mobil IContact Name: Dale L. Gomm Billing Address: P.O. Box 4552 City: HOU Istate: TX Izip: 77210 IPhone Number: Same III. Waste Stream Information Name Name of Waste: Soil containing unleaded gasoline Process Generating Waste: UST removal Type of Waste o iNDUSTRIAL PROCESS WASTE or IZJ POLLUTION CONTROL WASTE Physical state: [8l SOLID o SEMI-SOLID o POWDER [J LIQUID o OTHER: Method of Shipment: IZJ BULK o DRUM o BAGGED o OTHER: Estimated Annual Volume: [8l CUBIC YARDS: 150 o TONS: o GALLONS o OTHER: Frequency: [8l ONETIME o DAILY o WEEKLY o MONTHLY o OTHER: Special Handling Instructions: IV. Representative Sample Certification Is the representative sample collected to prepare this profile and laboratory analysis. . coll""ted in accordance with U.S. EPA 40 CFR 261.20(c) 'delines or uivalent rul Sample Date: 11-8-01 Type of Sample: IZJ COMPOSITE SAMPLE 􀁾􀁙􀁅􀀺􀁓􀀠orONO Laboratory: SPL 􀀭􀀽􀀽􀀮􀀺􀀽􀀧􀀢􀀢􀀢􀀧􀀭􀀮􀀺􀀺􀀮􀀮􀀺􀀮􀀮􀀮􀀽􀀭􀁾􀁾􀁟...._ ..... 􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀧􀀭􀀮􀀺􀀺􀀮􀀮􀀽􀀮􀀺􀀮􀀽􀀮􀀺􀀮􀀺􀀮􀀮 􀀮􀁣􀀮􀀻􀀮􀁣􀀮􀀮􀀮􀀮􀀺􀀮􀀺􀀺􀀽􀀺􀀺􀀮􀀺􀀺􀀮􀀺􀀮􀀮􀀺􀀮􀀺􀀮􀀮􀀮􀀺􀁣􀀮􀀺􀀮􀀮􀀺􀀮􀀮􀀮􀀺􀀮􀀺􀀮􀀮􀀺􀀭􀀧􀀭􀀽􀀭􀀭􀀧􀀽􀁾􀀻􀀬􀀮􀀮􀀺􀀺􀀮􀀫􀀭􀀭􀁾􀁟􀁟􀁉􀀠Sampler's Employer: EA Engineering • Sampler's Name (printed): Mark S. Lach Signature: RI=V 1 GENERATOR WASTE PROFILE SHEET (continued) Page 2 of2 Waste Profile # V. Physical Characteristics of Waste Chll:racteristic Components % by Weight (raIlge) 1, Clay soil 99 2. BTEX and TPH 1 3. 4. 5. Color Odor (describe) i Free Liquids % Solids I pH: Flash Point Phenol . 0 YES or r2J NO 17 (Illinois) Tan Slight hydroicarbon . Content % 100 NAOF NAppm Attach Laboratorv AnalvtiealRe1J{Jrt (andlor Matorial Safetv Dato Sheet! Inc/udinll Required Parameters Provided for this Profile Does this waste or generating process contain regulated concentrations of the following Pesticides andlor Herbicides: o Yes or r2J Noi Chlordane, Emlrin, Heptachlor (and it epoxides), Lindane, Methoxychlor, Toxaphene,2,4-D, or 2,4,S-TP Silvex as ! defmed in 40 CFR 261.331 Does this waste or genemting process cause it to exceed OSHA exposure limits from high levels afHydragen Sulfide ar o Yes or r2J No 􀁾􀁧􀁥􀁮Cyanide as defined in 40 CFR 261.231 Does this waste contain regulated concentrations ofPolychlorinated Biphenyls (PCBs) as defmed in 40 CFR Part 7611 o Yes or r2J No Does this waste contain regulated concentrations oflisled llszardous wastes defined in 40 CFR 261.31, 261.32, 261.33, o Yes or r2J Noincluding RCRA F-Listed Solvents?Does this waste contain regulated concentrations of2,3,7,8-Tetrachlorodibenz:cd scraping. Executed on this 26th Day of October, 2001. (Signature) By: Brent McClure Title: Vice President Company: Sunbelt Industrial Services Nov 16 01 lUlboa USFlLTER RECOVERY SERVICES (SOU11IWES1), INC. OFF·SPECIFICATION PRODUCT MANIFEST Vlwmdl Water Transport, Inc. 1657'Commerce Dr., Suite lOB South Bend; IN 46628 ' , 􀁁􀁄􀁄􀁾􀁔􀁉􀁏􀁎􀁁 􀁌INFORMATION: Emergt1)cy 􀁃􀁯􀁮􀁴􀁡􀁣􀁾􀀠Clifum or Chemtre¢ (800) 424-9300 ",' , ' North Aljlerican Emergency Response Guide No. '128, Placard .s i'131llllllJiqle UGlUid (lJNt993), Mllterlals is Off-Spedficaticn Fuel Product; See for additional information. CBRTlPJCATION: I hereby declare the CO[Ite!lts of /his consignment are fuUy and 'COl"ately described above by proper .hipping name and are classified. paclred. marked and labeled, and are in all respeclS in propu condition for transport by highways according to applicable international and national governmental regulations. I cortiiy Ulllt the material removed from Ibe nbove premises i, not bazardou, waSte as identified in 40 CFR Part 261. and does not contain PCB', as ideatilied in 40 CPR Part 761.1 the service times and are correct Is this debris defined under 40 CFR280? (J Yes DATE TREATMENT FACILITY o BIIJ_n..._ Factljty 44t5 EastG....wood Baytown, TX 11520 􀁅􀁐􀁁􀁉􀁄􀀴􀀺􀁔􀁉􀁭􀁬􀁩􀀸􀀰􀁾􀀲􀀱􀀠State Rna, TX 751 W EPA!D 1I:TXll988059291 Stat. Reg. I/: lOO95 Canary copy 􀁾􀀠Transponcr Green Copy -OencmtQ"S lit Copy Nov 16 01 lO:5Ba p . .r.u 􀀭􀀭􀀭􀀭􀀭􀀭􀁾􀀭􀀺􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀢􀀠< .... . " I US FILTER RECOVERY SERVICES (SOUTHWEST), INC; . [Fi;Ud Type: UST 0 . PST Ell I ,'; .OFF·SPECIFICATION PRODUCT MANIFEST ." • 4 _"....􀁾􀀠..r" . • Wvendi Water Transporf;,liie. 1657 Commerce Dr., Suite lOB South Bend, IN 46628 ' PHONE (800) 355-2383 STATE .STATE REGIS1lRA1'IONSIU6469,. U.S. EPA tD. it INROOOO22798 u.s. D.O.T. REGISTRATION It 828559 or ChemlreC (BOO) 424·9300 . as FiammalJ,le Uquid (UN1993). Materials is Off-Specification Fuel Product, See GENERATORS CERTIFICATION: I hereby declare tbe content, of this consignment are fully and accurately described above by proper 'hipping name and are classified; packod, marked and labeled, and are in all respects in proper condition for tnm'pcrt by highways according to applicable international and national governmental regulations. . . Icertify !hat the material removed [rom the above premises is not haumloos waste as identified in 40 CPR Part 261. and does not contain PCB', as identified in 40 CFR Part 761. !he service times and . Unit No. 3 6J .:ll. '1L-'-__-􀁟􀁾􀁟􀀠. Arrival TlltIe: SIGNATURB -..􀁾􀀮􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭􀀭VATE o Baytown Tnatmenll'llcllity 4415 East G_wood BaylDVln, TJ( 17520 EPA lD t. TXD9!8089421 8m!!! Reg. II: 81059 UI!l348 Coraiam.Tnatmenl Fdty 2124 31 White Copy -Cienerator Original Pink Copy 􀁾􀀠Design3ted F3cility . Canary Copy -Transporter Green Copy -􀁾􀁥􀁲􀁡􀁲􀁯􀁮􀁳􀀠Itil Cupy BHS017 􀁄􀁔􀀨􀁾􀁣􀁶􀀮􀀠9.001 TEXAS NATURAL RESbuRCE CONSERVATION COMMISSION Petroleum Storage Tank Division, MC 137 P.O. Box 13087 Austin, Texas 78711-3087 Please type orprint (Form designed for use on elitel12 -pitch typewriter,) tNSTRUCTIONS ON REVERSE StDE. 1. 􀁇􀁥􀁮􀁥􀁲􀁡􀁴􀁯􀁾􀁳􀀠LPST to No. or ST to No. 2. Page 1 of PETROLEUM-SUBSTANCE WASTE MANIFEST 􀁾􀀱􀀰􀀠􀁬􀁟􀁾􀀺􀀬􀀠3. Generator's Narile, Contact Person, and Mailing Address A. State Manifest Document No. 􀀭􀀻􀀺􀀭􀀻􀀭􀁜􀀺􀁜􀀭􀁾􀀮􀁉􀁎􀀠7>.f! ion;;. i"-',-;PH )RATJ' )1"·;"r 􀁬􀀬􀁤􀁾􀀠(r(\!fhil R.;!. h:.T-i 27i,i i .: 􀀧􀁾􀀠187832 PO H·.!...: 􀁉􀁾􀀠<., 􀀻􀀬􀀻􀁾􀀠􀁴􀁬􀀧􀀭􀀢􀀧􀁾􀀼􀀢􀁬􀀧􀁾􀁄􀀮􀀠L\ -: 􀁾􀀮􀀺􀀠I \) B. Generator's Facility ID No. 4. Generator's Phone ( ) Generator's Fax ( ) .. . . .. I '" 􀀻􀂷􀀬􀂷􀁮􀁾􀀢􀂷􀀧􀀢􀀠I '" ,...-. .,,, , 5. Generator's Facility Name, Contact Person, and Physical Address 􀀡􀁾􀁸􀁾􀂷􀀺􀁮􀁎􀁴􀁜􀂷􀁦􀁏􀁂􀁉􀁌􀀠n:s 􀁣􀀺􀁾􀀨􀁊􀀻􀀠􀀻􀁾􀀮􀀯􀁄􀀬􀁾􀀺􀀡􀁾􀀠·.....􀁊� �􀀮􀁬􀁲􀀱􀁾􀀡􀁮􀀠C. Generator's Tank Owner 10 No. q1􀁾i 􀀻􀁾􀀬􀁤􀁴􀀱􀁭􀁾􀀠• _, 1 .. ...,...,,r:"O'...ltM 'fl. [.'\ 6. Generator's Facility Phone ( ) Generator's Fax ( ) _1 . 􀁾􀀬􀀢􀀺􀀮􀀧􀀠c'!. . 􀁾􀀬􀀠7. Transporter 1Company Name and Address D. Transporter's Phone 􀁁􀁮􀁪􀁾􀁉􀁩􀁬􀁌􀀨􀀺􀀻􀀠􀀧􀁦􀁲􀁵􀀨􀀬􀁾􀁊􀁨􀀿􀀠􀀨􀁾􀀻􀀯􀁽􀀩􀁟􀁗􀁜􀀧􀁉􀁔􀁴􀀻􀀺􀀠20] () I." 􀁴􀀺􀁮􀁾􀁵􀁲􀁹􀀠􀀨􀁜􀀾􀀬􀁬􀁊􀁾􀀨􀀻􀁬􀀠 l;j'. d Contact Person: 􀁛􀁬􀀢􀁜􀀺􀁉􀁈􀁾􀀺􀀠TX 􀁲􀁾􀁯􀀨􀀩􀀺􀀠.rdrC!.( 8. Transporter 2 Company Name and Address E. Transporter's Phone Contact Person: 9. Designated Facility Name and Site Address F. Facility's Phone ',l:,-;:;I.;-􀁴􀀬􀀧􀀱􀀢􀁮􀀺􀀺􀀱􀁆􀁾􀁔􀁬􀁥􀁈􀁉􀀠UUld1W !:.).,.!) _'I 􀁾􀀮􀀭'\ 􀁪􀀧􀀺􀁾􀀠l 1':)OD.:\ 􀀡􀂷􀁾􀀼􀀻􀀺􀁊􀁲......􀀩􀁾􀁜􀁾􀀠St. J.;:",:isv;f!::._ 􀀮􀁾..... 􀁾􀀢􀀧􀁏􀀶􀀧􀀭􀁃􀁾􀀡􀀱􀁴􀁡􀁣􀁴􀀠Person: 10. Facility 10 Number 􀁉􀁏􀁾􀀠r, n " \\􀁾􀁬􀁬􀁬􀁩􀁾􀀧􀀠􀁾􀂷􀁩􀁲􀀺􀁮􀀬􀀮􀁜􀀠11. Waste Description (including Proper Class, and 10) 12. Containers 13. Totat Quantity 14. Unit 15. Waste Code a. -"::',', I 􀀢􀀨􀁖􀀡􀁾􀀠'!Y 'T'O 􀀡􀁉􀁾􀁤􀀬􀀮􀀮􀀮􀀧􀀭􀁜􀀬􀀠􀀡􀁾􀀮􀀬􀀺􀀠1􀀢􀀺􀀧􀁊􀁾􀀬􀀧􀀠lhn,· 1<;"" 􀁾􀀠􀀧􀀮􀁌􀀮􀁾􀀠􀀠b. G. Additional Description for Materials Listed Above 􀀺􀂷􀂷􀁛􀀨􀁊􀁾􀁆􀀠16. Special Handling Instructions and Additional Information j\! . 11-.iI: GENERATOR'S CERTIFICATION: I hereby declare the contents of this consignment are fully and accurately described above by shipping name and are classified, packed, marked, and labeled, and are in all respect in proper condition fortransport by highway according to applicable federal and state regulations. . -􀁾􀀠-. ... ., """ r' , __ . 􀁾􀀮􀁾􀁾.. ..' ., ,h I',' ,'" .1-;,....,1 􀀺􀀧􀀺􀀧􀀧􀀩􀁽􀁾􀀧􀀨􀁬􀀡􀀠􀁐􀁲􀁩􀁮􀁴􀁥􀁤􀁦􀁔􀁹􀁰􀁥􀁾􀁎􀁡􀁭􀁥 􀀠.• _. 􀁾􀁬􀀮􀀠􀀬􀀻􀀬􀁾􀀠..... ;:," r , ' .. ", ','. , .,. ,􀁓􀁩􀁧􀁮􀁾􀀭􀀧􀀠􀀬􀁾􀀠¥ate;617. . /..,/'{".'vld f__ 􀀮􀂷􀀬􀁾􀂷􀂥􀀢􀀬􀀢􀀢􀀢􀀠i:..... r 1-...... 1.. r" 􀁾􀀻􀁮􀁮􀀧􀀠-;;k./iY' /____.. !lr II . ",-C V, t Transporter 􀀱􀀮􀁾􀁫􀁮􀁯􀁷􀁬􀁥􀁤􀁧􀁥􀀢􀀺􀀱􀁥􀂷􀁮􀁴􀁯􀁦􀀠Receipt of Materials I'>(ature.///, Date 􀁐􀁲􀁩􀁮􀁴􀁥􀁤􀁦􀁔􀁙􀁰􀁥􀀧􀂥􀁾􀀠􀁉􀁦􀀧􀁾􀀠j'\ 􀀯􀁾􀀠I , G:f􀁾􀀠􀀯􀁲􀀺􀀷􀀧􀀻 􀁾􀀠\.....{. " V \ '.:?.-?' 􀀯􀀰􀁣􀀲􀁾􀁤􀁲􀀺􀀻􀀺􀀠. /, 19. Transporter 2 Acknowledgement of Receipt of Materials Sigl1atDle Date PrintedfTyped Name l/, .' 20. Discrepancy Indication Space 21. FacilityOwner/Operator: Certification of receipt of petroleum-substance wastes covered by this manifest except as noted in Item 20. PrintedfTyped Name Signature Date ,, .. TNRCC-0332 (05-05-94) While -Onglnal Yellow-STFaciitly Pmk-Transporter Green· Generators first copy TEXAS NAlURAl ResOURCE CONSERVATION COMMISSION Petroleum Storage Tank Division, MC 137 P.O. Box 13087 AusUn, Texas 78711·3087 Please type orprint. (Form designed lor use on eHtel12 ·pilch typewriter.IiP,·Jr!! I, 􀁩􀁾􀀿􀀠Dr: '0..􀀻􀀱􀀩􀀬􀁾􀀠INSTRUCTIONS ON REVERSE SIDE. 1. Genera""'s LPST ID No. or ST ID No. 2. Pagel of PETROLEUM-SUBSTANCE WASTE MANIFEST 3. Generator's Name, Contact Person, and Mailing Address F.,X\UN 0·tOnH, 􀀨􀁙􀁾􀁋􀁴􀁊􀁕􀁒􀀧􀀻􀁔􀁈}N(U'11r: 1.}<;)tl:W, 􀁒􀁾􀀨􀁬􀀠I·:t· i -: 􀁾􀁾􀀬􀀠1-\) Hi':.. "1';;'.1 Htrl1StPfL 'IX 􀀷􀀺􀁾􀁾􀁩􀁴􀀧􀀠4. Generatots Phone ( Ganeralots Fax ( 5. Generatots Faclnty 􀁎􀁡􀀧􀀻􀀻􀁾􀀮􀀠􀁃􀁾􀁩􀁾􀁃􀁴􀀧􀁰􀀮􀁲􀁮􀁯􀁮􀀮􀀠and Physical Address 􀁦􀁘􀁘􀀨􀀩􀁾􀀴􀁾􀀧􀁦􀁏􀁈􀁬􀁉􀀬􀀠k.':'\ ;:,-0r-\'TJn:e dll·;:;· 􀁾􀁾􀁾􀁰􀁥􀁾􀀺􀀠10. Facility ID Number t:. \ .luie 􀀬􀁥􀀼􀁩􀁴􀁾􀁬􀀠11. Was'e Description (Including Proper Clas" and ID) 12. Containers 13. TolalQuanlity 14. Unit 15. Waste Code 􀁡􀁾􀁴􀁮􀁬􀀠􀀡􀀮􀀮􀁾􀁯􀁮􀁲􀀮􀁩􀁲􀁬􀁮􀁵􀀡� �􀀠un!e.:ae-n g(i::>olltlt! IS-yd, b. G. Additional Description far MaterialS Usled Above "NONE 16. Special Handling Inslrucllons and Addillanallnlarmation NONE GENERATOR'S CERTIFICATION: I hereby declare the contents 01 \his consignment are fully and accurately descnbed above by shipping name and are classified, packed, marl;(;N i\I('iBfI· : 􀂷􀁬􀀢􀁾􀁻􀀠.I'GRAT1( :·i\:t"r,Jt:::: \·.;;1-(itW Kill h:T ....... I .j 187831:. ,I -Pt l Dol,'", 􀂷􀀮􀁨􀁾􀁾􀁾􀀧􀀠f· k,!\;-;-h.:".o_ 􀁾􀀭􀀾􀀻􀀠--, 􀁾􀀠i {.; B. Generalol's Facility 10 No. 4. 􀁇􀁥􀁮􀁥􀁲􀁡􀁴􀁯􀁾􀁳Phone ( ) 􀁇􀁥􀁮􀁥􀁲􀁡􀁴􀁯􀁾􀁳Fax ( ) Generator's Facility 􀁎􀁡􀁾􀀬􀁪􀀬􀀠􀁃􀀧􀁯􀁲􀁩􀁴􀁡􀁾􀀺􀁐􀁾􀁲􀁳􀁯􀁮􀀮 􀀠and Physical Address ..i .!, 􀁮􀀧􀁬􀀡􀀧􀀭􀁾􀀺􀁪􀀠.'} O. fx:Xf )N'1\'f(;BH, R S ,i-f}] '7(., [)ttk, l1J,)'l"UH: C. 􀁇􀁥􀀢􀀢􀁲􀁡􀁴􀁯􀁾􀀮Tank OWner ID No. 􀁾􀀠I􀁾􀀩􀀠i B-et1lmi'. , .Ad.jittun. T\· 6. Generator's Facility Phone ( ) 􀁇􀁥􀁮􀁥􀁲􀁡􀁴􀁯􀁾􀀮Fax ( ) .. .",-1.. 7. Transporter 1 Company Name and Address D. 􀁔􀁲􀁡􀁮􀁳􀁰􀁯􀁲􀁴􀁥􀁾􀁳Phone AlhlHlCi* 'ihKking 􀁩􀀧􀀺􀁮􀀲􀀧􀁾􀀠􀁾􀁾􀀵􀂷􀀱􀀷 􀀷􀀲􀀠20 I fI C,;ntury C-􀁾􀁈􀁫􀁩􀁾􀀠Hh:d Contact Person: 􀁉􀁲􀁮􀀺􀁵􀁾􀀮􀀠TX 􀁾􀂷􀀢􀀧􀀮􀁮􀁻􀀩􀀲􀀠􀀻􀁾􀁴􀁲􀀨􀀧􀁨􀁬􀁜􀀧􀀠B. 􀁾Transporter2 Company Name and Address E. Transporter's Phone Contact Person: 9. De.signaled Facility Name and Site Address F. Facility's Phone 􀁜􀁖􀁾􀁬􀁾􀁨􀀺􀀠􀁍􀁩􀁕􀁐􀁗􀁾􀁈􀁨􀀻􀁧􀁦􀀠Li:\!1·_1HlI 􀁻􀁵􀀧􀀻􀀡􀀱􀀳􀁴􀀵􀁾􀀵􀀴􀀲􀀱􀀠􀀡􀁦􀁾􀁑􀁮􀁁􀀠􀁒􀁾􀁬􀀡􀁬􀁲􀀨􀁬􀁡􀁤 􀀠􀁓􀁾􀀠. L('WLSl'lif:.:, ';;., 􀁾􀀧􀀭􀀻􀀨􀁫􀀧􀁊􀀠Contact Person: 10. Facility 10 Number i (i) 􀀧􀁜􀀭􀁩􀁾􀀠L; '\1\1uidu;;",jl.! 11. Waste Description (including ProparClesa, and ID) 12. Containers 13. TolalQuantity 14. Unit 15, Wasta Code a. 􀁾􀀺􀀬􀀩􀀻􀁴􀀠􀀬􀀧􀁣􀀭􀀮􀁾􀀻􀁴􀀺􀀡􀁩􀁾􀀧􀀺􀀱􀁈􀁔􀀠fll!l,·'·-"{,-, 1 􀀺􀀬􀀮􀁾.. \11'1," I, •.',4, b. G. Additional Description lor Materials Listed Above :..j( Jh!!·· 16. Special Handling Instructions and Additional Inlonnation l..:{ 􀁉􀁍􀁊􀁾􀀧􀀠GENERATOR'S CERTIFICATION: I hereby declare the contents of this consignment are fully and accurately described above by shipping name and are classified, packed, marked, and labeled, and are in all raspaC! in proparcondition lor transport by highway according to applicable federal and state ragulations. ., , , . PrintedIType'd Narli'e " '-"" , " , .. "'f1 , , ; : . 􀁖􀀺􀁾􀀧􀀠!-',:.J 11, ( 􀁾􀀠􀁾􀀠􀁓􀀡􀀺􀀮􀁴􀀮􀀡􀀡􀀮􀀮􀀧􀁬􀁬􀀮􀁵􀀮􀀢􀁊􀁉􀁾􀀢􀀺􀀧􀀮� �􀁊􀀠_' 􀁾􀀠, " 00Z17. 􀁉􀁧􀁮􀁡􀁾􀂣􀀭" 􀀬􀀭􀁾􀀬􀁩􀀬􀁬􀀠t.:T"..<-Ti><> 􀁦􀁾􀀢􀀠r",.j",. ;,-,"In, 􀀬􀁾􀀼􀀭􀀯􀀠.-//, ;:& ,-/1 18. Transporter 1 Acl..􀁤􀁴􀁬􀁩􀁟􀁾􀀮􀁦􀀧􀀱􀁬􀀮􀀠TX 6. Generator'sFacilityPhone ( ), . Generator's Generator's Fax ( ) ,," 7. Transporter 1 􀀮􀀧􀁾􀀮􀀠D. Transporter's Phone !Mli:mcc-Tn1d.ing 􀀧􀀨􀁾􀀷􀀲􀀩􀀠􀀢􀀧􀀴􀀮􀁾􀀱� �􀁾􀀧􀀺􀀧􀁾􀀠21310 ('cnt!ny 􀁃􀀨􀁾􀁮􀁬􀀨􀀬􀁊􀀠Hkd Contaci Person: kVUifl rs 7;;·002 jell {:h1: 8. Transporter2 Company Name and Address E. 􀁔􀁲􀁡􀁮􀁳􀁰􀁯􀁲􀁴􀁥􀁾􀁳Phone Contact Person: 9. DeSignated Facility Name and Site Address F. Facility's Phone 􀁲􀁖􀁡􀀮􀀬􀀢􀀬􀀡􀁾􀀠􀁮􀀻􀀮􀁛􀁡􀀮􀁲􀁬􀁾􀁬􀀿􀀬􀁾􀁈􀁶􀀡􀀭􀁮􀁴􀀠L...ndtiU {\}-:2.i 􀁾􀀱􀁩􀀻􀁾􀀵􀀭􀁴􀀿􀀻􀀠fd)l1:\ 􀁦􀀨􀀻􀀱􀁩􀁉􀁲􀁯􀁾􀁩􀁬􀁩� �Sl . L{!w;:;:\iJJ<:. T:': 􀀻􀁾􀀬􀁮􀀰􀀧􀁜􀀠ContaCI Person: 10. Facility 10 Number !(1: .).B [J. 􀁾􀁜􀁖􀁩􀁵􀁩􀀮􀀻􀀻􀀻􀁨􀀬􀀻􀀬􀀮􀁬􀁊􀀠11. Wasle I ' Ii, I 􀀧􀁮􀁲􀁮􀁾􀀠Proper (010« .nO 10) 112. 13. 􀁔􀁾􀀧􀁯􀁬􀁮􀀬􀀠"hh. •14. 􀁕􀁮􀁾􀀠15. 􀁗􀁢􀀢􀁡􀁦􀀧􀁍􀁾􀀠a. 􀁾􀀬􀀬􀀬􀁉􀀠! 􀀢􀁾􀁫􀀬􀀬􀀬􀀧􀀮􀀧􀁲􀀬􀀠. ,I, ''''' '.'ds b. G. IDescriplion ; Listed Above ,'1(1:;£ 16. Special Handling Instructions andAdditionallnformalion NON;' GENERATOR'S CERTfFICATION, I hereby declare the contenls of this consignmenl are fully and accuralely 􀁤􀁥􀁳􀁣􀁾􀁢􀁥􀁤above by shipping name and are classified. packed, marked, and labeled, and are in all respect in 􀁰􀁾􀁰􀁥􀁲condition fortransport by highway according to applicable federal and state " 'c. , . .... ,. , 'c'',,.". "c' .,. .-" 􀂷􀀮􀁾􀁙􀁮􀁾􀁺􀀻􀁾􀁔􀀠/1/-;6117. ,..nmOOI I ypea 􀁎􀁾􀀢􀀧􀀮􀀠''ovid C, ,," ,>" 1;,;1,., c;;"'''' , 18. " 􀀬􀀬􀀢􀁾􀀮􀀬􀁪􀀮􀀻􀀠fo"􀁮􀀢􀀢􀁾􀀺􀀺􀁾􀀠􀁾􀀻􀀾􀀺􀀠.,g ,w. '\)\ Signatu;? . Dale ..':?:,,/.,/.." 􀁾􀀠􀁾􀀻􀀻􀀻􀁕􀀣􀀠//lJ /19. Transporter2 Signature Date PrinledITypedNarne 20, Discrepancy Indication Space 21. Facility Owner/Operator: Certification of receipt of wastes covered by this manifest except "In Ilem20. PrinledITyped Name Signature Date TNRCC-0332 (05-05-94) While· Original Yellow· STFacUlty Pmk· Transporter Green· Generator's firslcopy i TEXAS NATURAL RESOURCE CONSERVATION CoMMISSION Petroleum Storage Tank Dillision, MC 137 P,O. Box 13087 " /Austin, Texas78711-3087 ,. , ,." . Please type orprint, (Formdesignedforuseonelitelt2-pitchty pewriter.>--r;;, 􀀬􀀬􀀮􀀮􀁖􀁾􀀠I)) I, INSTRUCTIONS ON REVERSe SIDE. 1, Generator's LPST 10 No. or ST ID No, 2. Pagel of PETROLEUM-SUBSTANCE WASTE MANIFEST . , , " , , 3, Generator's Name, Con1act Person, and Mailing Address A. State Manifest Docurnant No. EX 􀁜􀁇􀀺􀁾􀀠:>,,1. 􀀻􀁾􀁻􀁌􀀠l' J.,lRP{);·:.·\'i f('J\ 'i lak! \,.J(IHl!fl. r.:llt j..."-T¥12':U : ' ') 187824... P{; HI',\: ,t':-5: H'..'1i.l.,:-h·J:.1".\ 􀁩􀁾􀀬􀀧􀀺􀀠In 6. 􀁇􀀮􀁮􀁥􀁲􀁡􀁬􀁯􀁾􀁳􀀠Facility 10 No. 4. 􀁇􀁥􀁮􀁥􀁲􀁡􀁴􀁯􀁾􀁳Phone ( ",)",,, "-' III 􀁇􀁥􀁮􀁥􀁲􀁡􀁴􀁯􀁾􀁳Fax ( .J ,,. " .... 5. Generator's Facility Name, Contact Person, and Physical Address EXX()Nil.l{",I!jlL ft/S tl.. 􀀰􀀲􀀭􀀻􀀬􀁲􀀮􀀮􀀧􀁄􀁾􀁫􀀠(:-U1HUI ·J1'!1 􀁾􀁊􀁥􀁊􀁬􀀡􀀱􀁮􀁥􀀠C. Generator's Tank Owner 1D No. 􀁾􀀬􀁜􀁤􀁬􀁡􀁩􀀭􀀮􀀮􀁜􀀩􀁲􀁌􀀠TX6, 􀁇􀁥􀁮􀁥􀁲􀁡􀁬􀁯􀁾􀁳Facility Phone ( LA 􀁇􀁇􀀮􀁮􀁥􀁲􀁡􀁬􀁯􀁾􀁳􀀠Fax ( ) 􀀧􀀡􀀱􀀱􀀯􀀢􀁾􀀠7. Transporter 1 Company Name and Address D. Transporter's Phone All!all"'l' 'li'ud;ing (:J ':'2 ! 􀁾􀁴􀀧􀁬􀀵􀁾I '1:'2 21)1 () Century ('􀁾􀁬􀁬􀁫􀀺􀀠i!iI',1 Contact Person: irVin!,!, r.{ 􀀺􀀻􀁾􀁏􀁶􀀲􀀠JdrCltt\o 8. Transporter 2 Company Narna and Address E. 􀁔􀁲􀁡􀁮􀁳􀁰􀁯􀁲􀁴􀁥􀁾􀁳Phone Contact Person: 9. Designated Facility Name and Site Address F. Facility's Phone BF!-H.3:";'[ \sl.lnl.:n.., i...o.IadfiU ,::'l.-!l 􀁮􀁈􀁲􀀮􀀧􀁟􀁴􀀴􀁾􀀧􀀢� �􀁆􀁾􀀬􀀨􀀺􀂷􀀭􀁴􀀢􀀠􀀺􀁦􀀻􀀺􀁾􀀵􀁴􀁾􀁬􀀬􀀱􀁾􀀠rx ;'v{;::5 Contact Person: FacHit)' ID Number 24: -􀀮􀀩􀀮􀁾􀀠􀁝􀁻􀁻􀀧􀁻􀁬􀁜􀁈􀁾􀀠D"i1n-:I10, 11. Waste Descriplion (including Proper Class, and 10) 12, Containers 13, Tolal Quantity 14. Unit 15, Waste Code 􀁡􀁾􀁾􀁩􀁜􀁬􀀡􀀠'.:-H. f'( ";'., 2Ji) 4. Generalor's Phone ( ) Generator's Fax ( 5. Generalor's Facility NatriJ, Cb'1lla'bt 􀁾􀁾􀁲􀁳􀁯􀁮􀀬􀀠and Physical Address f.X"XONr..1'OBH. R"S 􀀶􀁾􀁜􀁲􀀺􀀠"5 Tl;d-.' 􀁪􀀮􀁝􀁾􀀧􀁭􀁦􀀮􀁩􀁬􀀠·n (t1 Bdilint .Addi:'.ofl. 􀁔􀀺􀂷􀁾􀀠6. Generator's Facility PhOne ( ) 7. Transporter 1 Company Name and'Ad'dress Alli.l1n..'t; 􀁔􀁮􀁴􀁜􀀬􀀧􀁊􀁪􀁮􀁾􀀠1010CellflU,' 􀁃􀁾􀁮􀁫􀁲􀀠B!YG frving. TX 75(1()': 8. Transporter 2 Company Name and Addres. 9. Designated Facility Name and and Site Addre•• an 􀂷􀁬􀁬􀁡􀁾􀁾􀁜􀀮􀀺􀀧􀀮􀀧􀀠... 􀂷􀀻􀀮􀀻􀁾􀁲􀁊􀁥􀁷􀀩􀀮􀀠􀁌􀁾􀁬􀁈􀁤􀁦􀀡􀀱􀀱􀀠.!:':'vit)tl. }i,,:.I,.·.j T\. '"'i'J(f"\\ 10. Facility ID Number :,J i· 􀁾􀀠11. Wast. Descripllon 􀁾􀁮􀁣􀁬􀁵􀁤􀁩􀁮􀁧􀀠Proper Class, and ID) O. Additional Description lor Materials Lisled Above Generator's Fax ( 12. Containers 13. A. Slate Mani!esl Dacumenl No. 􀀡􀀧􀀮􀁾􀀠18.7823 B. Generator's Facility ID No. C. GenerStor's Tank Owner ID No. D. Transporters PhOne 􀁻􀁾􀀷􀀲􀁊􀀠..􀁈􀁾􀁬T.t2 Contact Person: it'Q(ill" E. Transporters Phone Contact Person: F. Faclllly'. Phone t 􀀱􀁾􀁾􀀩􀀠􀁴􀀾􀁾􀀧􀀮􀀠􀁾􀂷􀁩􀁾􀀺􀁻􀀻􀀠Contact Person: l{PIl.Hi;:' j),m;d Total Quantity 14. Unit 15. Waste Code '20 .>•.􀁾􀀢􀀠_... 􀀻􀀮􀀮􀁩􀁉􀁾􀁬􀀡􀀬􀀺􀁲􀀮􀀠..... ______________􀁾􀀮_______________-1 16. Spacial Handling Instructions and Addltiona"n!onnalion -".. GENERATOR'S CERTIFICATION: I hereby declare Ihe contents 01 this conslgnmenl are luliy and accurately described above by shipping name end are classifiedl packed, marked, and labeled, and are in all respect in proper condition for transport by highway according to applicable federal and stale re1JulaUons. " 111. Transporter 1 Acknowledgennentof Receipt 01 Materials 􀁐􀁲􀁩􀁾􀁾􀁥􀁾􀁾􀀬􀁎􀁡􀀧􀀻􀀡􀁥􀀠,Mv,'d./' '',I'.__0 ..."-,....': ""'/:...../􀀯􀀯􀀯􀀻􀁴􀀡􀀯􀀯􀁖􀀧􀁾􀀠􀀮􀀭􀁾􀀠,/;".,-'l/..,r-9 19. Transporter2 Acknowledgamentof ReceiPt of Materials PrintedITypadName 20. Discrepancy Indication Space //;;;:61 \ Date .,i\ 􀀬􀁾􀀠Signature v'" Date 21. FacilityOwnerlOperator: Certification of receipt of petroleum-substance wastes covered by this manifest except as noted in Item 20. PrintedlTypod Name Signature Date TNRC= (Q5.05-94) White -Onglnal Yellow -STFacility Pink -Transporter Gr6en -Generator's first copy TEXAS NATURAL ReSOURCE CONSERVATION COMMISSION Petroleum Storage Tank Division, MC 137 P.O. Box 13087 Austin, Texas 78711-3087 ';1 . /! '. i \ -j ;,; 􀁾􀀠'"I Please type orprint (Form designed for use on elilel12 -pilch Iypewriter)---r-iF"-INSTRUCTIONS ON REVERSE SIDE 1. Generator's LPST to No. or ST iO No. 2. Page 1 of PETROLEUM·SUBSTANCE WASTE MANIFEST ' .. -', .. 3. Generator's Name. Contact Personl and Mailing Address A. State Manifest Document No. f.:\X<'Jr,' \fi ;;:;;, I .{ 'F r'i +:..:\'fji 􀀻􀁲􀀢􀁾􀀠;-'!.ik' \,)!lHti, hJn " l , .. 􀁾􀀧􀀭; 􀀮􀁾􀀡􀀠187825>i'{ 1 H ' 􀀬􀁾􀀠􀀮􀀧􀀻􀀮􀁾􀀺􀀠i·:1...􀁵􀁊􀁾􀀬􀀬􀀻􀁬􀁉􀀮􀀬􀀠';'\ ' :.: ;tl -_.... B. Generalor's Facility 10 No. 4. GeneratorsPhone ( ) ... Generator's Fax ( I ' . ..;------,.;-, 5. Generator's Facility Name. Contact Person, and Physical Address 􀁾􀁾􀀬􀁜􀀮􀁜􀁕􀀻􀁜􀁉􀁾􀀧􀁁􀀺􀀩􀁈􀀱􀁌􀀠}(:::: 􀀢􀀭􀀺􀀧􀀻􀁾􀀭􀀢􀀢􀀠Uitk '-<'EO£! i l":l\ iJd,1;",. C. Generator's Tank Owner ID No. :';,\14,,,-,·)1. ;'\ 6. Generator's Facility Phone ( ),., ., Generator's Fax ( ) 􀁾􀀬􀀬􀀺􀀠.It, 7. Transporter 1 Company Name and Address O. Transporter's Phone ..-... 􀁕􀁩􀀢􀁈􀁾􀀮􀀬􀁲􀀻 􀀠􀁔􀀻􀁵􀂷􀂷􀁴􀁪􀁮􀁾􀀡􀀠􀁩􀀭􀀺􀀮􀀺􀀺􀀲􀁾􀀠-i,t;, l :' :-. 2:tjifj 􀁾􀀠􀂷􀁾􀁮􀁴􀁩􀀻􀁲􀂷􀀧􀀠i '1-::1!h') Bh,: 􀁃􀁐􀁾􀁾􀀹􀁴􀁅􀁾􀁲􀁳􀁯􀁮􀀺􀀠in'J11;2 "t\ 5(h-,: ".J < t. _,I" 8. Transporter 2 Company Name and Address E. Transporter's Phone Contact Person: 9. Designated Facility Name and Site Address F. Facility's Phone 1:,: 􀁩􀀭􀁩􀁬􀁾􀀬􀂷􀀮􀁇􀀻􀀻􀀠􀀧􀀬􀀮􀀡􀁴􀀮􀁨􀀺􀁾􀀻􀀮􀀻􀀺􀀠l..:ut•.HW (.:>.JJ 􀁄􀁩􀁦􀀺􀀭􀁾􀀲..:·:"" \. ".-j:;." It;.:: ... :, 1"\ ""'!'....... Contact Person: ". 􀁴􀁜􀀮􀀬􀀢􀁮􀁲􀁾􀀡􀀺􀀺􀀧􀀠1 :,1; 􀁦􀁲􀀬􀀭􀁾􀀻􀀠10. Facility 10 Number .j t 11. Waste De.coption (including Proper Class. and 10) 12. Containers 13. Total Quantity 14. Unit 15. Waste Code __􀁾􀀮􀀠7.":'] 􀀬􀀺􀀬􀀬􀀧􀂷􀀺􀀮􀀺􀀡􀀼􀀡􀀧􀁮􀁮􀁾􀀭􀀧􀀠􀂷􀀮􀀬􀁩􀁤􀁾􀀬􀀬􀀺􀂷􀀮􀁾􀀺􀀺􀀬􀁻􀁪􀀠􀀻􀁾􀀨􀁉􀀺􀀬􀁁􀀧􀀻� �􀀧􀁌􀀮􀀺􀀬􀀠_.. 00 " i 􀁾􀁾􀀮􀀠b. G. Additional Description for Materials Usted Above 􀁾􀁜􀀺􀀬􀀠':.J, 16. Special Handling Instructions andAdditionallnformatlon , 􀀻􀁬􀀭􀀺􀀧􀁾􀁾􀁌􀀠GENE;:RATOR'S CERTIFICAnON: I hereby declare the contents ofthis consignment are fully and accurately described above by shipping name and are classified, packed, marked, and labeled, and are In all respect in proper condition fortransport by highway according 10 applicable federal and slate regulations. lh tl" 1111,1,'1 􀀮􀀻􀀺􀀺􀁾􀁬􀀻􀂷􀁤􀀠fl"' ,').-:!! i'-I; !.. "."cn"\. '"tn! ! 'dO ' "',IL-t'i. I (,I d1tUroH.,:':ii.;•. )H 􀀻􀀬􀁢􀁴􀁾􀀮􀀮􀁩􀀠:.'lr·:·:{;!:1 : ,.(¥lbY'/' . Y/!'c://.. -􀁾􀀬􀀮􀀮􀀮􀀮􀀭􀀭􀀭18. Transporter 1 Acknowledgement of Receipt 01 Materials Signature; /') Date PrintedlTyped Name􀁊􀀼􀁾􀀠<., :; /. .' ? , " ... /"" /􀁾􀀿􀀠/1>'-/*1' ,( L. 􀁾􀀧􀀬􀀻􀀧􀀠. ,(..-. 􀁾􀁾􀀯􀀢􀀧􀀠􀁾􀀠/;:p/"-/; --J , c. /19. Transporter2 Acknowledgement of Receipt of Materials signature Date PrintedlTypadName 20. Discrepancy Indication Space 21. FacilltyOWnerlOperalor. CertlficaUon of receipt of 􀁰􀁥􀁴􀁲􀁯􀁬􀁥􀁵􀁭􀁾􀁳􀁵􀁢􀁳􀁬􀁡􀁮􀁣􀁥wastes covered by this manifest except as noted in Item 20. PrinledfTypedName Signalll," Dele TNRro= (OS-IlS·94) ..White -Onglnal ..Yellow· STFacility Pmk -Transpotfar G"'en Genera/ot's first copy EA Engineering, Science, and Technology APPENDIXD Photographic Documentation F;\Proj\Exxon\sdM-0275\Repons\TEA Tank Excavation Repon Texas. Photo 1. Rinsing ofempty UST, Exxon 6-0275, 4191 Belt Line Photo 3. UST properly labeled for off site transport and destruction, Exxon 6-0275, 4191 Belt Line Road, Addison, Photo 4. View ofthe excavation following removal ofthe UST,Texas. Exxon 6-0275, 4191 Belt Line Road, Addison, Texas, EA Engineering, Science, and Technology APPENDIXE Release Determination Report F:\Pro}\Exxon\sdNi-0275\Reports\TEA Tank Excavation Report RELEASE DETERMINATION REPORT FORM Owners and operators must report releases by phone to the appropriate TNRCC Region Office within 24 hours of conlinnation. The owner and operator should use this form to comply with the reporting requirements in Title 30, Texas Administrative Code 0334.77(b). Suhmit the completed form within 20 days after release confirmation. EXCEPT IN EMERGENCIES. THE TNRCC WD..L INITIATE ACTION ON TIllS CASE ONLY WHEN THE COMPUTED FORM (pages 6 through 15) IS SUBMITI'ED wrrn ATTACHMENTS TO BOTII THE APPROPRIATE TNRCC REGIONAL OFFICE AND TO THE CENTRAL OFFICE IN AUSTiN (PST Division, MC137. P,O, Box 13087. Austin. Texas 78711), DO NOT MODIFY TIllS FORM IN ANY WAY, Complete an applicable blanks, Incomplete forms will be returned without review, All proposals for the next appropriate corrective action activity must be submitted by a CAS and PM in the format outlined in the guidance document entitled Preapproval for Correclive Action Activities (RG-III), SUMMARY Based on the infonnation obtained during this release detennination and by comparing the contaminant levels to the stated action levels, check one of these four items as appropriate: TIlis was a suspected release. No contamination was detected due to this suspected release. ! This site is an LPST site. Contaminant levels exceed action levels (or one of the other criteria applies). I I II' This site is not an LPST site, Contaminant levels do not exceed action levels (and none of the other criteria applies), This site Is not an LPST site, No contamination was detected (and none of the other criteria applies), IF THIS SITE IS AN LPST SITE. COMPLETE THE REMAINDER OF THIS FORM (except Section B). If this site is not an LPST site, stop here and complete Sections A, C, and G (and Section B ifapplicable) of the attached form. Check here ifthis site is an existing LPST case and this Release Determination Report i, being submitted only as the tank removal-fiom-service documentation. Answer the foDowing questions In this Summary Section If tbis is is an LPST case and if the CAS and PM sign the form in Section G. This section is to be completed hy a CAS and PM only. If the form is completed by someone other than a CAS and PM, leave the rest of this Summary Section blank and go 10 Section A. Is this case eligible for reimbursement of necessary corrective actions'? YES NO Ifnot. appropriate corrective action in accordance with applicable rules and guidance Ill3y continue withoul,pecific direction or approval from the PST Division, however, coordination with the PST Division is recommended. Ifthe site is eligible for reimbursement, aU corrective action activities, with the exception ofNAPL recovery and emergency abatement activities. must be prcapproved prior to initiation. The next appropriate step for this site, ifit is an LPST sire, is (check one only): Case closure Ifchecked, attach Sile Closur. Request Form (TNRCC-0028). Please be sure the site meets all requirements for closure prior to submitting the Site Closure Request Form. Are there costs associated with case closure? 0 YES 0 NO If YES. and if the site is eligible for reimbursement. attach a cost proposal and workplan with the Sile Closure Request FOrni. Risk·Based Assessment The risk-based assessment is needed only when the existing assessment data is not an adequate basis for site c1oSW"C. Pie... critically evaluate the need for additional assessment before selecting this option, Refer to pamphlet RG-175 for guidance on conducting the risk-based assessment. Attach a detailed workplan and proposal if the site is eligible for reimbursemenL A proposal must be submitted with this form if the RP is financially able to undertake necessary corrective actions, Corrective aelion other than risk-based assessment Attach a detailed workplan and proposal if the site is eligible for reimbursement and the RP is financially able to undertake necessary corrective actions. A. GENERAL INFORMATION LPST ID No.: rid i TNRCC Region: 4 Priority: (If known) (see pages 13-15) Facility ID No,: 0026232 Required onIess one one of the following applies: Cbeck here if tank registralion is not required for this site (per 30 TAC 0334,7). and check one of the fullowing as applicable: the tank(s) are partially excluded or exempted from jurisdiction under 30 TAC Cbapter 334, Specify type or usage of tank(s): these tanks were permanently removed from the ground before May 8, 1986 (provide date ofremoval ): these tanks remained in the ground but were emptied, cleaned, and filled with inert substance hefore Janoary I, 1974 (provide date of activities: ); TNRCC-0621 (8-1-96) Page 1 of 16 --------A. GENERAL INFORMATION these tanks were out of operation, their existence was unknown, and they were permanently removed from service within 60 days of their discovery (provide date of discovery: . Provide method of discovery: Prior to this investigatIon. was this site ever an LPST site? v YES or NO If yes, provide LPST ID number: 10.:1218, 􀀱􀀰􀀹􀀱􀀰􀀴􀀱􀁾􀁑􀁴􀁨􀀠closed1 Tank Owner: Exxo.n Mobil ComorotiOtl Tank Owner Mailing Address: 􀁐􀀮􀁏􀀮􀀸􀁯􀁸􀀴􀁾􀀲􀀠Room /I lIT· 127Q Tank Owner City: Hous.ton 􀁓􀁴􀁡􀁴􀁥􀀺􀁾􀀠Zip: 􀁚􀁚􀀲􀀱􀀰􀀭􀀴􀀵􀁾􀀲􀀠 Tank Owner Contact Pemon: l2ale l. Gomm Phone: (71:1.19.5.6·9219 Fax no.: (7131656·9121 Tank Operator (if different from tank owner): __.. Tank Operator Mailing Address: Tank Operator ("Iv' State:__ Zin: Tank Operator Contact Person: Phone: Fax no.; Land Owner (if different from tank owner and operator): Land Owner Mailing Land Owner City: State: Zin: Land Owner Contact Person: Phone: Faxnn.: IfIbis site is an LPST site, which of these parties will oversee the the corrective actions at this site? vTankOwner Tank Operator LandOwner Other (not the contractor or consultant): Name: Exxon Mobil Corporation _ ______M ___Address: P.O. 80):455.2, Room # KT-1270 ...􀁾.._ City: Houl.tan State: TexJJS Zip: 7721Q·4:i.5.2 Contact person: I2lJitt GOI1l1!' Phone: 713-(i56-9219 Fax: ZlJ-(i56-9191 A representative of the party overseeing the corrective action must sign this fonn in Section G. Please note that no matter which party Conducts I corrective action, the tank owner and the tank operator are jointly responsible for the necessary corrective actions. i Facility Name: Exx.QU B&. 6-0275 Facility Physical Address: 4121lleltIine Road @Mldwa! Road Facility City: AddiS!l!l County: Dallas County Code: 57 INDICATE TYPE OF RELEASE: (ebeek one) Suspected v Confirmed but below action levels (not an LPST site) Confirmed and above .ction levels (LPST site) No evidence ofcontamination (all results below detection limits) Please refer to flowchart and Title 30 Texas Administrative Code, 0 334.71 ·334.77 for descriptions and procedures for suspected and confirmed releases. Were copies of this COMPLETED form (excluding pages I through 5) and appropriate attaduneots, including a proposal (ifRP is financially able), sent to both the TNRCC Central Office and to the Region Office? 0 YES V NO (IF COPIES ARE NOT SENT TO BOTH OFFICES, THIS DOCUMENT WILL BE RETURNED WITHOUT REVIEW). i TNRCC.0621 (8·1·96) Page20f 16 A. GENERAL INFORMATION lndicate number of tanks currently and formerly located at this site (attach pages as necessary): Type ruST!ASn Product Type Size C!ll!p!Ox. gall Current: 􀁾􀀨􀁕􀁓􀁔􀀡􀁁􀁓􀁮􀀠P roduct Type Size (approx. gall Date Removed from Service Former: Plus Unleaded Regular Unleaded Supreme Unleaded Diesel 10,000 .allon /0, GOO gallon 8,000 gallon 􀁾􀁏􀀢􀁏􀁏􀁏􀀠gallon 10126/01 1026//01 10126101 10126/01. B. SUSPECTED RELEASE INFORMATION Complete only this section and sectioIlS E through G as appropriate when the situation of a suspected release has occurred and it was documented that a release had not occurred. i Dale suspected 􀁲􀁾􀁬􀁥􀁡􀁳􀁥􀀠discovered:___________Reason release 􀁳􀁵􀁳􀁰􀁥􀁣􀁴􀀻􀁤􀀺􀁟􀁾_____􀁾____􀁾________ 􀁉􀁾􀀽􀀽􀀽􀀽􀀽􀀮􀀽� �􀀻􀀽􀀽􀁾􀀽􀀻􀀺􀀺􀀽􀀺􀀻􀀻􀀺􀀻􀀻􀀺􀀻􀀺􀀻􀀻􀀻􀀺􀀺􀀺􀀺􀀮􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀻􀀻􀀽􀀽􀀽􀀻􀀽􀀮􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀽􀀭􀁾􀁉􀀬Date suspected release reported to TNRCC: Reported 10: Possible sOUIce(s) of release: (check all that apply) Tanks: 0 USTs ASTs Piping Overfills/spills 0 Unknown Other: Type of suhstanee(s) suspected released: (check all that apply) 0 Gasoline 0 Diesel Used Oil Aviation Gasoline I Jet Fuel (type: ) Alcohol-blended fuel (Type nod percentage of alcohol:___________) Other: (be specific) Were USTIAST system tank and/or line tightness tests performed? 0 YES or 0 NO (check one) If yes, attach test data and results. Did the tests indicate that all tanks and piping were tight? YES or X NO (cheek one) If No, specify the poruon of the tank system(s) that were fouod not to be tight: 10,QQO gallon diesel UST Were any repairs conducted on the tank system(s)'! YES or 0 NO (check one) ffyes, describe type(s) and location of repairs: Diesel and accumulated groundwater was removed from the UST am! the USTwas temporarily put out ofservice pending a decision as to whether ornot to permanently mmQ}'€ orrepair the UST Were tightness tests perfOl1Ded after repairs were conducted? YES or 0 NO (check one) If yes. attach test data and results. Did the tests indicate that the repaired items were tight? YES or NO If No. specify the portion of the tank system(s) that were found not to be tight: The damaged diesel UST has not been repaired pending a decision to remove i1. Were any soil confirmation samples collected? 0 YES or NO (check one) If yes, were all potential source areas investigated? YES or NO If samples were collected, attach descriptions of sample locations, collection methods. and laboratory results. i Were any groundwater confirmation samples collected? YES or 0 NO (check one) If yes, were all potential source areas Investigated? YES or NO Ifsamples were collected. attach descriptions of sample locations, collection methods, aquifer name, and lahoratory results. (Groundwater sampling is not required at this point unless there is reasonahle suspicion of imp"!.) C. CONFIRMED RELEASE INFORMATION -, Date release confirmed: 11/05/01 Date release reported 10 TNRCC: NA Reported 10: NA Is this the fin;t release from a UST or AST discovered at this site? YES v NO Is there any other contamination or potential impacts to human health from any source other than the tank systems at this site? oYES v NO Ifyes, indicate type and location of contamination:__________________._________ TNRCC-0621 (8-1-96) Page 3 of 16 ! ! i ! Reported to TNRCC by: NI;, Representing: NA -' Method of release discovery: V' Samples collected during tank removal-from-service activities Impact to utility line Samples collected during other tank system construction activities Impact to surface water Samples colleeted during release detennination investigation Impact to water well Other: Method of release confirmation: (check all that applyJ V' Soil samples Groundwater samples Surface water sample o Documentation ofpresence ofNAPL Source(sJ of release: (check all that apply J Tanks: USTs ASTs Piping Overfills/spills V' Unknown Other: Substance(s) released: (check all that apply) V' Gasoline II'Diesel Used Oil Aviation Gasoline Alcohol-blended fuel (Type and percentage of alcohol: ) Jet Fuel (type; ) Other: (be specificl______, Amount of product released: 􀀡􀀮􀁉􀁮􀁫􀁮􀁯􀁾􀀠Chemical Abstract Service registry #: (for hazardous substances) Were any soil confinnation samples collected? V' YES or NO (check one) Ifyes, attach descriptions of sample locations, collection methods and laboratory results, Type of native soil: (check one) V' Clay or silt Sand,gravelorrock Were any groun'dwater confirmation samples collected? YES or V' NO (check one) If yes, attach descriptions of sample locations, collection methods, aquifer namej and laboratory results. Known Iropact(s): (check all that apply) V' Soil OW Surface Water Subsurface Utilities -type: Buildings WaterweUs Other sensitive receptors: Was the land owner (if different from the tank owner) notified of the contamination? V' YES or NO (check one) IfYes, attach copy oftheletter which provided the notification, IfNo, documenllltion that notification was provided must be submitted within 30 days from the date the impact is discovered, Possibly Threatened: (check all that apply) V' GW Surface Water Subsurface Utilities -type: Buildings Water wells Other sensitive receptors: Was NAPL detected (graater than 0,01 feet)? YES or V' NO (check one) Ifyes, describe how and where it was detected, the thickness detected, and the recovery actions taken: : TNRCC-Dli21 (8-1-96) Page 4 ofl6 D. AlIATEMENT MEASURES Were abatement measures initiated to stop the release or to recover the released substance? YES Or NO (check one) If yes, describe the II. abatement andlor recovery measures taken and the dates and duration ofthe activities: NA il Were UST/AST system tank andlor line tightness tests performed? Did the testS indicate that all tanks and piping were tight? YES be tight:NA or YES or NO (cbeck one) Ifyes, attach test results. NO If No, specify the portion of the tank system(s) that were found not to il Were any repairs conducted on the tank system(s)" NA YES or NO (check one) lfyes, describe type(s) and location of repairs: Were tighmess tests performed afrer repairs were conducted? YES or NO (check one) If yes, attach test results. Did the tests indicate that the repaired items were tight? YES or NO If No, specify the portion of the tank syslem(s) thaI were found not to be 􀁴􀁩􀁧􀁨􀁴􀀺􀁎􀀢􀀬􀁁􀀬􀀭􀀭􀁟􀁾___� �􀁟􀁾_________________􀁾___ ! ! E. FIRE/OTHER OFFICIALS Were any other officials notified? YES NO (check one) If Yes, indicate: Name Renresenting: phone number Date!s) Notified Were any directives issued by the fire Of other officials? YES NO If Yes. describe directives and actions taken in response to the direcuve:__ F. WASTE DISPOSITION Indicate the status of all wastes and other materials generated: Iw of waste 􀀨􀁾􀁩􀁬􀀠waterl };!roouct} Ouantity 􀁃􀁵􀁾􀁴􀁬􀁯􀁾􀁯􀁮􀀠Method and JQgtion of disposal or treatment Fiberglass l!!iI..s 4 Scrae.rzgd Dis/losed 􀁯􀁛􀁢􀁾􀀠S.unbelt lndustrial 􀁾􀁦􀀮􀀮􀁲􀁶􀁩􀁣􀁥􀁳􀀠w..Bi!Jse 􀁗􀁡􀁴􀁾􀁲􀀯􀁷􀁡􀁴􀁥􀁲􀀠14,850 gal C.Qrsicana, TX DislZ!l.sgd o(};rt. U.S. t:.ilter 􀁾􀀬􀁯􀁶􀁥􀁡s.c.rvices SQtlLF{ll Mg,l€rigl 60 vdl IIQJ.co, TX 􀁄􀁩􀁾􀁦􀀡􀀮􀁑􀁳􀁥􀁤􀀠at b't. llllied Wasle I BFl &2.i1.L£il/Material 140 vdsJ Ferris! TX Disoosed o[by Waste Managemgjl : ! , i I TNRCC·0621 (S·t·%) Page 5 of 16 I ________ __ G. REPORT PREPARATION PM Slgnature:---... .. Date: c..._.., 0: ) r:J/AND CAS Representative: Roger W. Place CAS Reg No.: 0127 Exp. Date: 12106103 By my signature affixed below. I certify that I am the duly authorized representative of the Correction Action SpeCialist named and that I have personally reviewed the site investigation results and other relevant information presented herein and considered them to be in accordance with accepted standards/practices and in compli . the applicable TNRCC published rules. guidelines and the laws of the State of Texas. Further, that the information presented herein is co 􀁾􀁩􀁤􀁥􀁲􀁥􀁤􀁾􀁭􀁰􀁬􀁥􀁴􀁥􀀧􀀺􀁴􀀽􀀼􀀻and representative of the conditions discovered during the site investigation. I acknowledge that if) intentionally or 􀁫􀁮􀁯􀁾􀀠ngly 􀁭􀁾􀁳􀁥st s, representations, or certifications in this report,) may be subject to i administrative, civil, andlor criminal penal t;:i 􀁾􀀠I Silll1ature of CAS Representative: 􀁲􀀺􀁾􀀠'.. A.... Date: Ii'" Iro /Ol i ff the CAS or On·Site Supervisor does 􀁮􀁾􀁬􀁥􀁴􀁥and sign this form, provide the following infurmatlon oII the person who has prepared the furm: Name: Company: Telephone No.: FAX No,: Signature: Date: Name of Tank Owner or Operator contact: Dille Gomm. f:rmn Mobil Corporation Telephone No.: 17131656-9219 FAX No.: (1130 656·9191 By my signature affixed below, ) certify that I have reviewed this report for accuracy and completeness of information regarding points of contact and the facility and storage tank system history and status. [ aCknowledge that if) intentionally or knowingly make false statements. representations. or certifications in this report related to the contact information, and the facility and storage tank system history and status information. I may be subject to administtative. civil. and/or criminal penalties. I attest that I have reviewed this report for accuracy and completeness. [underntand that) am responsible for addressing this matter. Signature: Date: A Licensed On·Site Supervisor may complete and sign this form when the supervisor is acting in an approved capacity for tank removal·from· service or tank system repair activities. Licensed 􀁏􀁮􀁾􀁓􀁩􀁴􀁥􀀠Supervisor: lLP Reg. No.: Exp.Date:.. Company: Telephone No.: FAX No.: Based on the results of the site investigation and the additional infonnation presented herein. I certify that the site investigation activities perfonned either by me, or under my direct supervision. including subcontracted work, were conducted in accordance with accepted industry standards/practices and further. that all such tasks were conducted in compliance with applicable TNRCC published rules, guidelines and the laws of the State ofTexas. I have reviewed the information included within this report. and consider it to be complete, accurate and representative of the conditions discovered during the site investigation. ) acknowledge that if [ intentionally or knowingly make false statements, representations, or certifications in this report, ) may be subject to administrative, civil, andlor Climinal penalties. Signature: Date: OR Project Manager: T0d4 Fralee PM Reg. No.: 01237 Exp. Date: 6I2l{Q3 Company: EA.Engineerill&1 3,cience. and. Technology Telephone No.: (9721481·1420 FAX No.: (972124l·7220 Based on the results of the site investigation and the additional information presented herein, ) certify that the site investigation activities performed either by me. or under my 'direct supervision. including subcontracted work. were conducted in accordance with accepted industry standards/practices and further, that all such tasks were conducted in compliance with applicable TNRCC published rules, gnidelines and the laws of the State ofTexas, I have reviewed the information incJuded within this report. and consider it to be complete. accurate and representative of the conditions discovered during the site investigation. I acknowledge that if) intentionally or knowingly make false statements, representations. or 􀁣􀁥􀁲􀁴􀁩􀁦􀁩􀁾􀁡􀁴􀁩􀁯􀁮􀁳􀀠in this 􀁲􀁥􀁾􀁾administrative, administrative, civil, andlor Climinal penalties. /,."d Vc Company: E4 E.ng.iBft:.rinll, 􀁾􀁥􀁮􀁣􀁥􀀬􀀠€m4 􀁔􀁾􀁣􀁨􀁬􀁬􀁯􀁬􀁯􀁥􀀮􀁹􀀮􀀠Telephone No,: (972,484·,420 .. ... FAX No.: (9721 21Z·Z220􀀭􀀭􀀭􀀭􀁾 WOMACK, McCLISH & WALL, P.C. A'TTORNEYS AT LAw DANNY M. WOMACK 180 I LAVACA. SUITE I 20 JOHN MCCUSH * AUSTIN. TEXAS 7870 I SUE WALL PHONE (512) 474·9875 DAN FOSTER FACSIMILE: (512) 474'9694 EMAIL WMC@WOMACKMCCLlSH.COM • BOAtIa C(RJIFJU) IN CM!. 'TmAI. .010 CMI. APPEU..A'Tt tAw BY'nIC 􀁾SV Addison, Texas 75001-9010 PI ff'ei. FI/It.. J?e q .f'􀁾􀀠T1ttJ-1-?:!iRe: Fuel Storage Tanks -Midway Road and Belt Line Road Dear Mr. Jalbert: Exxon/Mobile has asked that we respond to your June 6th letter regarding the Exxon Tiger Mart located at the intersection of Midway Road and Belt Line Road in Addison. As you recall, one of the store's underground storage tanks was recently damaged by contractors working within the Town's right-of-way. Your letter requests a written response outlining Exxon's intended course of action regarding the existing tanks and the Town's request that the curb and pavement be setback in compliance with the previously approved site plan. We wish to assure you that Exxon is working diligently toward a resolution of these matters. Discussioris regarding the . tanl